• 제목/요약/키워드: Pure lead

검색결과 174건 처리시간 0.025초

BeO를 확산원으로 한 사파이어의 향상처리 (Sapphire Enhancement with BeO Powder Source)

  • 송오성;김상엽
    • 한국산학기술학회논문지
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    • 제6권2호
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    • pp.105-109
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    • 2005
  • 보석용 사파이어의 색향상 Be처리를 정량화하기 위해서 BeO를 확산 원으로 하여 알루미나(${Al_2}{O_3}$)분말과 $5{\sim}50wt%$ 범위에서 혼합하여 탄소발열체로 대기 중에서 $1800^{\circ}C$에서 100시간동안 순수한 단결정 사파이어 기판을 확산시켰다. 조성에 따라 처리된 사파이어를 육안검사, 색좌표검사, 표면조도의 변화검사를 실시한 결과, $Be^{2+}$ 원소는 알려진 바와 같이 순수한 사파이어에서는 발색원소로 작용하지 않았고 국부적인 회색의 원인이 되었다. 조성증가에 따라 확산양의 증가에 따라 급격히 Lab지수에서 광택지수(L)가 감소하였으며 표면조도가 증가하는 특징이 있었다. 기존에 알려진 블루사파이어의 오렌지 사파이어로의 향상을 위해서는 처리 후 표면조도가 작아서 재연마를 생략할 수 있는 5% 이하 BeO의 저조성 범위에서 순수한 커런덤이 아닌 $Fe^{3+}$ 성분이 많은 원석의 채용이 필요함을 확인하였다.

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열경화성 에폭시 기지의 흡습탄성 거동에 관한 분자동역학 전산모사 (A Molecular Dynamics Simulation Study on Hygroelastic behavior of Thermosetting Epoxy)

  • 권선영;이만영;양승화
    • Composites Research
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    • 제30권6호
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    • pp.371-378
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    • 2017
  • 본 연구에서는 대표적인 열경화성 재료인 에폭시 기지의 흡습탄성 거동을 예측하기 위해 분자동역학 전산모사를수행하였다. 고분자 복합재가 오랜 시간 동안 흡습환경에 지속적으로 노출될 경우, 거시적 물성의 저하가 발생하기 때문에 복합재의 내구설계 측면에 있어 흡습노화 현상에 대해 분자스케일적으로 접근하는 방법은 매우 중요하다. 본 연구에서는 $EPON862^{(R)}$ 수지와 아민계 Triethylenetetramine (TETA) 경화제로 비정질 에폭시 분자모델을 구성하였으며, 각각 30과 90%의 가교 상태에서 수분 흡수 유무에 따른 물성변화를 관찰하였다. 건조상태의 에폭시와 수분이 4 wt% 포함된 에폭시 단위셀에 대한 평형 및 비평형 앙상블 전산모사 과정을 통해, 에폭시의 수분팽창계수, 응력-변형률 선도 및 탄성계수 그리고 침투된 수분의 수지 내 확산계수를 예측하였다. 또한 흡습된 구조와 그에 따른 물성변화의 상관관계를 규명하기 위해, 자유체적 변화 및 흡습에 따른 에폭시 수지의 비결합 포텐셜 에너지 변화를 관찰하였다.

전열촉진관군의 순수냉매 강제대류비등 (Forced Convective Boiling of Pure Refrigerants in a Bundle of Enhanced Tubes)

  • 김내현;정호종;조진표;최국광
    • 대한기계학회논문집B
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    • 제25권12호
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    • pp.1831-1843
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    • 2001
  • In this study, convective boiling tests were conducted for enhanced tube bundles. The surface geometry consists of pores and connecting gaps. Tubes with three different pore sizes (d$_{p}$ = 0.20, 0.23 and 0.27 mm) were tested using R-123 and R-l34a for the following range: 8 kg/m$^2$s G 26 kg/m$^2$s, 10 kW/m$^2$ q0 40 kW/m$^2$and 0.1 $\chi$ 0.9. The convective boiling heat transfer coefficients were strongly dependent on heat flux with negligible dependency on mass flux or quality. For the present enhanced geometry (pores and gaps), the convective effect was apparent. The gaps of the present tubes may have served routes for the passage of two-phase mixtures, and enhanced the boiling heat transfer. The convective effect was more pronounced at a higher saturation temperature. More bubbles will be generated at a higher saturation temperature, which will lead to enhanced convective contribution. The pore size where the maximum heat transfer coefficient was obtained was larger for R-l34a (d$_{p}$ = 0.27 mm) compared with that for R-123 (d$_{p}$ = 0.23 mm). This trend was consistent with the previous pool boiling results. For the enhanced tube bundles, the convective effect was more pronounced for R-134a than for R-123. This trend was reversed for the smooth tube bundle. Possible reasoning is provided based on the bubble behavior on the tube wall. Both the modified Chen and the asymptotic model predicted the present data reasonably well. The RMSEs were 14.3% for the modified Chen model and 12.7% for the asymptotic model.model.

Fly ash의 NaOH 용융처리에 의한 고순도 Na-P1 Zeolite의 합성 (Synthesis of Highly Pure Na-P1 Zeolite by NaOH Fusion Treatment of Fly Ash)

  • 최충렬;이동훈;이인중;신동현;김장억;박만
    • 한국환경농학회지
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    • 제24권3호
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    • pp.232-237
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    • 2005
  • This study was conducted to elucidate the effects of NaOH fusion treatment on Na-P1 zeolite synthesis from fly ash and to evaluate its optimal condition. NaOH fusion treatment of fly ash led to Na-P1 zeolite with shorter reaction time and higher quality compared that of simple hydrothermal method. Mixed zeolite phases of Na-P1 and hydroxy sodalite were formed by the fusion treatment below $450^{\circ}C$, whereas only Na-P1 zeolite was formed above $550^{\circ}C$. Ratio of NaOH/fly ash, reaction times, fusion temperature and solid/liquid ratio strongly affected the kind and crystallinity of the zeolite formed. The CEC of Na-P1 zeolite formed at the optimum reaction conditions of NaOH/fly ash ratio 0.9 and solid/liquid ratio $1/5.0{\sim}1/7.5$ after NaOH fusion treatment at $550^{\circ}C$ for 2 hours was about $398cmol^+kg^{-1}$ which was 40% higher than those of control products. Therefore, it is clear that NaOH fusion treatment of fly ash in open system could lead to Na-P1 zeolite with high purity.

Bar effects on the central SF and AGN activities in the SDSS galaxy sample

  • Kim, Minbae;Choi, Yun-Yung;Kim, Sungsoo S.
    • 천문학회보
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    • 제41권1호
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    • pp.35.3-36
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    • 2016
  • We explore the role of bars in AGN-galaxy co-evolution using a volume-limited face-on late-type galaxy sample with $M_r$ < -19.5 and 0.02 < z < 0.055 selected from SDSS DR7. In this study, we investigate how $SFR_{fib}$ as a proxy of gas contents at galactic center (over 1~1.5 kpc bulge scale) and central stellar velocity dispersion, ${\sigma}$, of host galaxies are connected to the bar presence and AGN activity. We find that galaxies are distributed in three distinct regions over the $SFR_{fib}-{\sigma}$ space and the behaviors of their bar fraction ($f_{Bar}$) are clearly different for each region. Galaxies at the AGN dominant region tend to be gas-deficient as $f_{Bar}$ increases and bars are more frequently found in fully-quenched late-type galaxies at the quiescent region, suggesting that bars speed up of the consumption of gas by SF and lead a sudden decline in the central gas. Overall, the bar effects on the AGN activity are positive over the same space except for quiescent galaxies with ${\sigma}$ > $170km\;s^{-1}$. Most significant bar effect on the AGN activity occurs in the less massive galaxies having sufficient gas, whereas the effect on galaxies at the AGN dominant region with higher the AGN fraction is relatively small. We suggest that the bar affect both central SF and AGN activities, but differently for central gas amount and BH (or bulge) mass of galaxies. We also investigate the AGN-bar connection with only pure AGNs and then confirm that they give marginally the same results.

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Establishment of an easy Ic measurement method of HTS superconducting tapes using clipped voltage taps

  • Shin, Hyung-Seop;Nisay, Arman;Dedicatoria, Marlon;Sim, KiDeok
    • 한국초전도ㆍ저온공학회논문지
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    • 제16권2호
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    • pp.29-32
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    • 2014
  • The critical current, $I_c$ of HTS superconducting tapes can be measured by transport or contactless method. Practically, the transport method using the four-probe method is the most common. In this study, a simple test procedure by clipping the voltage lead taps have been introduced instead of soldering which reduces time and effort and thereby achieving a much faster measurement of $I_c$. When using a pair of iron clips, $I_c$ value decreased as compared with the measured one by standard method using soldered voltage taps and varies with the width of the clipped specimen part. However, when using a pure Cu clip, both by clipping and by soldering voltage taps give a comparable result and $I_c$ measured are equal and close to the samples specification. As a result, material to be used as voltage clip should be considered and should not influence the potential voltage between the leads during $I_c$ measurement. Furthermore, the simulation result of magnetic flux during $I_c$ measurement test showed that the decrease of $I_c$ observed in the experiment is due to the magnetic flux density, $B_y$ produced at the clipped part of the sample by the operating current with iron clips attached to the sample.

Compression Strength Size Effect on Carbon-PEEK Fiber Composite Failing by Kink Band Propagation

  • Kim, Jang-Ho
    • KCI Concrete Journal
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    • 제12권1호
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    • pp.57-68
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    • 2000
  • The effect of structure size on the nominal strength of unidirectional fiber-polymer composites, failing by propagation of a kink band with fiber microbuckling, is analyzed experimentally and theoretically. Tests of novel geometrically similar carbon-PEEK specimens, with notches slanted so as to lead to a pure kink band (without shear or splitting cracks), are conducted. The specimens are rectangular strips of widths 15.875, 31.75. and 63.5 mm (0.625, 1.25 and 2.5 in and gage lengths 39.7, 79.375 and 158.75 mm (1.563, 3.125 and 6.25 in.). They reveal the existence of a strong (deterministic. non-statistical) size effect. The doubly logarithmic plot of the nominal strength (load divided by size and thickness) versus the characteristic size agrees with the approximate size effect law proposed for quasibrittle failures in 1983 by Bazant This law represents a gradual transition from a horizontal asymptote, representing the case of no size effect (characteristic of plasticity or strength criteria), to an asymptote of slope -1/2 (characteristic of linear elastic fracture mechanics. LEFM) . The size effect law for notched specimens permits easy identification of the fracture energy of the kink bandand the length of the fracture process zone at the front of the band solely from the measurements of maximum loads. Optimum fits of the test results by the size effect law are obtained, and the size effect law parameters are then used to identify the material fracture characteristics, Particularly the fracture energy and the effective length of the fracture process zone. The results suggest that composite size effect must be considered in strengthening existing concrete structural members such as bridge columns and beams using a composite retrofitting technique.

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예비보육교사가 인식한 '영유아'에 대한 은유 분석 (Metaphor Analysis of 'Children' Perceived by Pre-service Childcare Teachers)

  • 김경미
    • 한국콘텐츠학회논문지
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    • 제22권4호
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    • pp.458-467
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    • 2022
  • 본 연구는 예비보육교사들이 인식한 영유아에 대한 의미를 은유분석 방법을 통해 알아보고자 하였다. 이를 위해 경기도 소재 대학에서 보육학을 전공하는 예비보육교사 288명 대상으로 2021년 5월 4주부터 6월 2주까지 자료를 수집하였다. 연구 결과, 영유아에 대한 의미는 '돌봄이 필요한 존재', '환경에 영향받는 존재', '개성을 지닌 존재', '소중하고 귀한 존재', '기쁨을 주는 존재', '미래를 이끌어갈 존재', '맑고 순수한 존재', '교사·부모를 성장시키는 존재'로 범주화되었다. 예비보육교사들은 8가지 범주 중에서 영유아를 '돌봄이 필요한 존재'로 인식한 경향이 가장 높게 나타났고, 138개 은유 표현 중에서는 '새싹', '씨앗', '꽃', '도화지', '스펀지', '거울' 순으로 표현한 것이 높게 나타났다. 이를 통해 예비보육교사들이 가진 영유아에 대한 인식을 보다 폭넓게 이해할 수 있었으며, 향후 예비보육교사 양성과정에서 개선 및 지원해야 할 방안을 마련하는데 기초자료로 활용할 수 있을 것이다.

A novel barium oxide-based Iraqi sand glass to attenuate the low gamma-ray energies: Fabrication, mechanical, and radiation protection capacity evaluation

  • Al-Saeedi, F.H.F.;Sayyed, M.I.;Kapustin, F.L.;Al-Ghamdi, Hanan;Kolobkova, E.V.;Tashlykov, O.L.;Almuqrin, Aljawhara H.;Mahmoud, K.A.
    • Nuclear Engineering and Technology
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    • 제54권8호
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    • pp.3051-3058
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    • 2022
  • In the present work, untreated Iraqi sand with grain sizes varied between 100 and 200 ㎛ was used to produce a colored glass sample that has shielding features against the low gamma-ray energy. Therefore, a weight of 70-60 wt % sand was mixed with 9-14 wt% B2O3, 8-10 wt% Na2O, 4-6 wt% of CaO, 3-6 wt% Al2O3, in addition to 0.3% of Co2O3. After melting and annealing the glass sample, the X-ray diffraction spectrometry was applied to affirm the amorphous phase of the fabricated glass samples. Moreover, the X-ray dispersive energy spectrometry was used to measure the chemical composition, and the MH-300A densimeter was applied to measure the fabricated sample's density. The Makishima-Makinzie model was applied to predict the mechanical properties of the fabricated glass. Besides, the Monte Carlo simulation was used to estimate the fabricated glass sample's radiation shielding capacity in the low-energy region between 22.1 and 160.6 keV. Therefore, the simulated linear attenuation coefficient changed between 10.725 and 0.484 cm-1, raising the gamma-ray energy between 22.1 and 160.6 keV. Also, other shielding parameters such as a half-value layer, pure lead equivalent thickness, and buildup factors were calculated.

The Effects of Daily Melatonin Gavage on Reproductive Activity in the Male Syrian Hamsters

  • Jeon, Geon Hyung;Kim, Hyeon Jeong;Park, Jinsoo;Lee, Sung-Ho;Cheon, Yong-Pil;Choi, Donchan
    • 한국발생생물학회지:발생과생식
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    • 제24권4호
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    • pp.263-275
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    • 2020
  • The proper administration of melatonin has well been documented to induce testicular regression in seasonal breeding animals. The subcutaneous injections of melatonin in the afternoon, not in the morning, consistently occurred testicular involution in the male Syrian (golden) hamsters whose reproductive activity is regulated by the photoperiod. But the effects of daily melatonin via gavage have not been estimated. Golden hamsters housed in long photoperiod (LP) were divided into 5 groups: the control animals housed in LP or in short photoperiod (SP) and animals treated daily with low (15 ㎍), middle (150 ㎍), and high dosages (1,500 ㎍) of pure melatonin by using gavage in the evening for 8 weeks. As results, LP control animals had large testes and SP controls displayed small and entirely regressed testes. The animals treated with various dosages of melatonin showed collectively degenerating effects on the weights of testes, epididymides, and seminal vesicles in the middle and high dosage groups, with the individual differences as well. The high dosages induced testicular regression in more proportion than the middle dosages did. The low dosage had large testes like the LP control animals. The small and inactive testes shown in some animals of both middle and high groups presented the complete regression as those of the animals maintained in SP. These results strongly suggest that the administrations of melatonin lead to testicular involution in the male golden hamsters when it is administered through gavage.