• Title/Summary/Keyword: Powder rheology

Search Result 102, Processing Time 0.024 seconds

Effects of Solder Particle Size on Rheology and Printing Properties of Solder Paste (미세피치 접합용 솔더 페이스트의 솔더 분말 크기에 따른 레올로지 및 인쇄 특성 평가)

  • Jun, So-Yeon;Lee, Tae-Young;Park, So-Jeong;Lee, Jonghun;Yoo, Sehoon
    • Journal of the Microelectronics and Packaging Society
    • /
    • v.29 no.2
    • /
    • pp.91-97
    • /
    • 2022
  • The wettability and rheological properties of solder paste with the size of the solder powder were evaluated. To formulate the solder paste, three types of solder powder were used: T4 (20~28 ㎛), T5 (15~25 ㎛), and T6 (5~15 ㎛). The viscosities of the T4, T5, and T6 solder pastes at 10 RPM were 155, 263, and 418 Pa·s, respectively. After 7 days, the viscosity of the T4 solder paste slightly increased by 2.6% and that of T5 was increased by 20.6%. The viscosity of the T6 solder paste after 7 days could not be measured due to high viscosity. The viscosity variation with solder particle size also affected on the printability of the solder. In the case of the T4 solder paste, printability, slump, bridging, and soldering properties were excellent. On the other hand, T5 showed slight dewetting and solder ball defects. Especially, T6, which the smallest powder size, showed poor printability and dewetting at the edge of solder.

The Physicochemical and Storage Characteristics of Sausage added Mugwort Powder (쑥 분말 첨가 소시지의 이화학적 및 저장 특성)

  • Han, Kyu-Ho;Choi, Il-Shin;Lee, Chi-Ho
    • Food Science of Animal Resources
    • /
    • v.26 no.3
    • /
    • pp.356-361
    • /
    • 2006
  • This study was carried out to investigate the physico-chemical and storage characteristics of sausages added mugwort powder at $4^{\circ}C$ during 13 days. The composition of fresh sausages was as the following : meat 60 % (w/w), lard 20 %, ice 20 %, salt 1.5 %, sugar 0.5 %, phosphate 0.25 %, mugwort 2 % or 5 %. Sausages were divided into three groups; control group mugwort 0 %, Treatment I mugwort 2 % and Treatment II mugwort 5 %. The pH, TBA(thiobarbituric aid) value, VBN(volatile basic nitrogen), rheology, and sensory evaluation were measured. The changes of pH of all groups were slightly decreased with increasing storage days. But, the significant difference of pH changes were not shown between mugwort 2 % (Treatment I) and mugwort 5 % (Treatment II) groups. The changes of TBA values of all treatments increased during storage periods. TBA values of Treatment I and Treatment II groups were significantly (p<0.05) higher than that of the control group. The change of VBN showed trends to increase during storage periods. The change of VBN of Treatment I was significantly (p<0.05) lower than those of the control and Treatment II. Hardness and brittleness of 2 % and mugwort 5 % groups were significantly (p<0.05) higher than that of the control group. Elasticity and cohesiveness of 2 % and Treatment II were significantly (p<0.05) lower than that of the control group. Also, Treatment I was superior to the other groups by the results of sensory evaluation. Therefore, these results suggest that it may be possible to manufacture sausages added 2 % mugwort powder which can help to increase storage periods, and improve quality of sausage.

High Pressure Liquid Jet Technology for Nano Particles Production

  • Mazurkiewicz, Marian;Rhee, Chang-Kyu;Weglinski, Bogumil
    • Journal of Powder Materials
    • /
    • v.15 no.5
    • /
    • pp.411-421
    • /
    • 2008
  • Principles and historical background of high pressure liquid jet (HPLJ) technology is presented in the paper. This technology can be applied, among others, for production of nano particles. This target can be achieved in various type of disintegration systems developed and designed on the base of this technology. The paper describes principles of two examples of such systems: HPLJ-reactor, called also a linear comminuting system, HPLJ- centrifugal comminuting system, which prototypes have been manufactured. A linear mill, being high energy liquid jet reactor, has been developed and tested for micronization of various types of materials. The results achieved so far, and presented in the paper, show its potential for further improvement toward nano-size particle production. Flexibility of adjustment of the reactors and the mechanism of the process allows for the creation of particles with unprecedented rheology. The reactor can be especially suitable to micronize, mix and densify materials with a wide range of mechanical properties for various industrial needs. Presented prototypes of comminution systems generate interesting potentials toward production of nano particles. Their performance, based on up today research, confirms expected high efficiency of materials disintegration, which opens a new challenge for industrial applications. The paper points out benefits and area of possible applications of presented technology.

THE RHEOLOGY OF THE SOFT LINER WITH 4-META

  • Park, Hyun-Joo;Kim, Chang-Whe
    • The Journal of Korean Academy of Prosthodontics
    • /
    • v.40 no.3
    • /
    • pp.269-274
    • /
    • 2002
  • statement of problem The viscoelastic property is the most important and peculiar characteristics of soft liners. But the authorized standard is not certainly established than other dental materials. purpose of study This study is aimed to compare the initial flow of gelation of the modified soft liner with 4-META with that of PMMA soft liners using dynamic method and evaluate the clinical acceptance of the trial materials. materials and method This study consists of 3 groups with the given % of 4-META powder in the Coe soft liquid; 0%, 5%, 10% Each group was tested for 10 times to record the change of G′values during 3 hours. the gelation time was recorded by the oscillating rheometer with parallel plate with 1 rad/sec. results As the results of this study, the gelation time of modified soft liner was elongated by 5 to 6 minutes. conclusion The mean gelation time of modified soft liner could be within the range of clinically acceptable.

Premature Stiffening of Cement Paste Associated with AFm Formation

  • Chung, Chul-Woo;Lee, Jae-Yong
    • Journal of the Korea Institute of Building Construction
    • /
    • v.11 no.1
    • /
    • pp.83-90
    • /
    • 2011
  • The purpose of this research is to investigate the effect of AFm formation on the stiffening process of cement paste. High and low alkali sulfate clinkers were used for the experiments. The flow and stiffening behavior of cement paste was investigated using modified ASTM C403 penetration resistance test and oscillatory shear rheology. X-ray powder diffraction (XRD) was used for phase identification associated with stiffening of the paste. It was found from the results that low alkali clinker mixture produced very strong premature stiffening whereas high alkali clinker mixture did not cause premature stiffening. This is because of the large amount of alkali sulfate present in the clinker. Addition of calcium and sodium chloride to the high alkali clinker mixture caused faster stiffening and set.

Rheological Properties of Binder Pastes for Self-Compacting Concrete

  • Park, Yon-Dong
    • KCI Concrete Journal
    • /
    • v.13 no.1
    • /
    • pp.35-41
    • /
    • 2001
  • This paper investigated rheological properties of binder pastes for self-compacting high performance concrete. Six mixtures of self-compacting concrete were initially prepared and tested to estimate self-compacting property. Then, the binder pastes used in self-compacting concrete were tested for rheological properties using a rotary type rheometer. Binder pastes with different water-binder ratios arid flow values were also examined to evaluate their rheological characteristics. The binders were composed of ordinary Portland cement, fly ash, two types of pulverized blast-furnace slag, and limestone powder. The flow curves of binder pastes were obtained by a rotary type rheometer with shear rate control. Slump flow, O-funnel time, box, and L-flow teats were carried out to estimate self-compacting property of concrete. The flow curves of binder pastes for self-compacting concrete had negligible yield stresses and showed an approximately linear behavior at higher shear rates beyond a certain limit. Test results also indicated that the binders incorporating fly ash are more appropriate than the other types of binders in quality control of self-compacting concrete.

  • PDF

Premature Stiffening of Cement Paste Caused by Secondary Gypsum and Syngenite Formation (False Set)

  • Chung, Chul-Woo;Lee, Jae-Yong
    • Architectural research
    • /
    • v.13 no.1
    • /
    • pp.25-32
    • /
    • 2011
  • The purpose of this research is to investigate the effect of specific hydration reaction on the stiffening process of cement paste. The cement compositions are manipulated to cause specific hydration reactions (secondary gypsum and syngenite formation) responsible for false set, and the relationship between specific hydration reactions and the flow and stiffening behavior of cement paste were investigated using modified ASTM C 403 penetration resistance measurement and oscillatory shear rheology. X-ray powder diffraction (XRD) was used for the phase identification associated with premature stiffening of cement paste. Differential thermal analysis (DTA) and thermogravimetric analysis (TGA) were used for verification of syngenite formation. From the results, both secondary gypsum and syngenite formation caused faster stiffening and set. The amount of syngenite produced during 1 hour hydration was approximately 1 % of total mass of the cement paste, but cement paste with syngenite formation showed significantly accelerated stiffening behavior compared to normal cement paste.

Rheology and Strength Properties Improvement of Recycle Cement by Admixture (혼화재료에 의한 재생시멘트의 레올로지 및 강도특성 개선)

  • 오상균;임승준;김정길
    • Proceedings of the Korean Institute of Building Construction Conference
    • /
    • 2003.05a
    • /
    • pp.89-94
    • /
    • 2003
  • Recently, the study to reduce and recycle industrial waste is underway vigorously in the various fields of industry according to the conservation of environment and resources. In construction work, the disposal problem of its waste and environmental disruption have already been serious all over the world. However the recycle of waste concrete is still at an early stage, recycled aggregate from waste concrete have only used those as subsidiary road fillers. The research institute and the company make the study that it is about the properties of recycled aggregate and those structural capacity since 1990. Through the experimentation last year, we know that strength and fluidity of recycle cement are inferior to normal cement, and admixing aggregate powder deteriorates its strength. The purpose of this study is to search for appropriate heating time and to improve performance of the recycle cement while heating hardened cement which is crushed, we investigate separating aggregate from hardened cement by preheating and improvement of strength and fluidity inrecycle cement which contains admixture.

  • PDF

Ceramic Stereolithography: Additive Manufacturing for 3D Complex Ceramic Structures

  • Bae, Chang-Jun;Ramachandran, Arathi;Chung, Kyeongwoon;Park, Sujin
    • Journal of the Korean Ceramic Society
    • /
    • v.54 no.6
    • /
    • pp.470-477
    • /
    • 2017
  • Ceramic processing to fabricate 3D complex ceramic structures is crucial for structural, energy, environmental, and biomedical applications. A unique process is ceramic stereolithography, which builds ceramic green objects from CAD files from many thin liquid layers of powder in monomer, which are solidified by polymerization with a UV laser, thereby "writing" the design for each slice. This approach directly writes layers in liquid ceramic suspension and allows one to fabricate ceramic parts and products having more accurate, complex geometries and smooth surfaces. In this paper, both UV curable materials and processes are presented. We focus on the basic material principles associated with free radical polymerization and rheological behavior, cure depth and broadening of cured lines, scattering at ceramic interface and their corresponding simulation. The immediate potentials for ceramic AM to change industry fabrication are also highlighted.

Exmination of Rheological Properties on Cement Paste of High-Blaine Blast Furnace Slag Fineness (고미분말 고로슬래그의 치환율 변화에 따른 시멘트 페이스트의 레올로지 성질 검토)

  • Lim, Ji-Hee;Lee, Gun-Cheol;Yoon, Seung-Joe
    • Proceedings of the Korean Institute of Building Construction Conference
    • /
    • 2013.11a
    • /
    • pp.186-187
    • /
    • 2013
  • Recently, high fluidity concrete is becoming more prevalent. High fluidity concrete uses admixture or thickener in order to prevent separation of materials due to increased fluidity, and, especially, BS is becoming more use for reduced heat of hydration and improved long-term strength. This study examined the effect of BS on fluidity of cement paste from a rheological viewpoint. As for BS types, materials equivalent to 1 types of KS F 2563 and the cement mass was substituted by 20, 40, 60, 80%.

  • PDF