• Title/Summary/Keyword: Powder flowability

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SiAlON 원료분말제조를 위한 분무건조 과립분말의 형상과 크기에 미치는 공정변수효과 (Effect of Process Parameters on the Morphology and Size of Spray-Dried Granule Powder for Fabrication of SiAlON Raw Material)

  • 최재형;이소율;한윤수;이성민;남산;김성원
    • 한국재료학회지
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    • 제27권12호
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    • pp.716-721
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    • 2017
  • SiAlON-based ceramics are some of the most typical ceramic materials used as cutting tools for HRSA(Heat Resistant Super-Alloys). SiAlON can be fabricated using ceramic processing, such as mixing, granulation, compaction, and sintering. Spray drying is a widely-used method for producing a granular powder of controlled morphology and size with flowability. In this study, we report a systematic investigation aimed at optimizing spherical granule morphology by controlling spray-drying parameters such as gas flow and feed rate. Before spray drying, the viscosities of the raw material slurries were also optimized with the amount of dispersant added.

플라즈마 분사 처리에 의한 Cr2O3 조립분말의 구상화에 대한 연구 (Spherodization of Granuled Cr2O3 Fine Ceramic Powder by Plasma Spray)

  • 이동원;이학성;유지훈;왕제필
    • 자원리싸이클링
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    • 제25권6호
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    • pp.92-97
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    • 2016
  • Spray dried $Cr_2O_3$ 분말은 겉보기밀도를 향상시키기 위해 plasma flame에 투입하여 실험을 진행 하였다. 첫번째 고밀도화 공정에서의 분말은 입자내부 공간까지 완전히 용해되어지지 않았으며, 두번째 공정 이후 완전히 용해가 되었다. 두번째 공정 결과 분말 입도는 작아졌으며, 용해 및 표면 연화에 의해 겉보기 밀도와 유동도는 향상이 되었다. 두번째 고밀도화 공정이 후 부분적으로 입자들이 $30{\mu}m$ 이상의 hollow structure을 보여주고 있다. 분말의 이러한 고밀도화는 plasma flame에 의해 응집되어진 응집체내의 열전도율 및 내부 가스압의 관점에서 정량적으로 논의 하였다.

Effect of pumice powder and artificial lightweight fine aggregate on self-compacting mortar

  • Etli, Serkan;Cemalgil, Selim;Onat, Onur
    • Computers and Concrete
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    • 제27권3호
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    • pp.241-252
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    • 2021
  • An experimental program was conducted to investigate the fresh properties, mechanical properties and durability characteristics of the self-compacting mortars (SCM) produced with pumice powder and Artificial Lightweight Fine Aggregate (aLWFA). aLWFA was produced by using fly ash. A total of 16 different mixtures were designed with a constant water-binder ratio of 0.37, in which natural sands were partially replaced with aLWFA and pumice powder at different volume fractions of 5%, 10% and 15%. The artificial lightweight aggregates used in this study were manufactured through cold bonding pelletisation of 90% of class-F fly ash and 10% of Portland cement in a tilted pan with an ambient temperature and moisture content. Flowability tests were conducted on the fresh mortar mixtures beforehand, to determine the self-compacting characteristics on the basis of EFNARC. To determine the conformity of the fresh mortar characteristics with the standards, mini-slump and mini-V-funnel tests were carried out. Hardened state tests were conducted after 7, 28 and 56 days to determine the flexural strength and axial compressive strength respectively. Durability, sorptivity, permeability and density tests were conducted at the end of 28 days of curing time. The test results showed that the pumice powder replacement improved both the fresh state and the hardened state characteristics of the mortar and the optimum mixture ratio was determined as 15%, considering other studies in the literature. In the aLWFA mixtures used, the mechanical and durability characteristics of the modified compositions were very close to the control mixture. It is concluded in this study that mixtures with pumice powder replacement eliminated the negative effects of the aLWFA in the mortars and made a positive contribution.

금속 3D 프린팅 공정 최적화를 통한 H13 공구강 조형체의 기계적 특성 향상 (Mechanical Property Improvement of the H13 Tool Steel Sculptures Built by Metal 3D Printing Process via Optimum Conditions)

  • 윤재철;최중호;이행나;김기봉;양상선;양동열;김용진;이창우;유지훈
    • 한국분말재료학회지
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    • 제24권3호
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    • pp.195-201
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    • 2017
  • In this study, H13 tool steel sculptures are built by a metal 3D printing process at various laser scan speeds. The properties of commercial H13 tool steel powders are confirmed for the metal 3D printing process used: powder bed fusion (PBF), which is a selective laser melting (SLM) process. Commercial H13 powder has an excellent flowability of 16.68 s/50 g with a Hausner ratio of 1.25 and a density of $7.68g/cm^3$. The sculptures are built with dimensions of $10{\times}10{\times}10mm^3$ in size using commercial H13 tool steel powder. The density measured by the Archimedes method is $7.64g/cm^3$, similar to the powder density of $7.68g/cm^3$. The hardness is measured by Rockwell hardness equipment 5 times to obtain a mean value of 54.28 HRC. The optimum process conditions in order to build the sculptures are a laser power of 90 W, a layer thickness of $25{\mu}m$, an overlap of 30%, and a laser scan speed of 200 mm/s.

연소합성법에 의한 Plasma-arc Deposit 용 $Cr_3C_2$ 합성 및 특성에 관한 연구 (Synthesis and Characterization of $Cr_3C_2$ for Plasma-arc Deposit by Combustion Synthesis Process)

  • 장윤식;윤정아;이윤복;박성수;김인술;박흥채;오기동
    • 한국세라믹학회지
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    • 제33권11호
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    • pp.1285-1291
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    • 1996
  • Using Cr2O3 Al and graphite powders as starting materials Cr3C2 was synthesized by combustion synthesis process according to the following reaction : 3Cr3C2 +4C+6Allongrightarrow2Cr3C2 +3Al2O3. The synthesis was conducted at 2 atm in an argon atmosphere. in this study main-product was monolithic phase of Cr3C2 /Cr7C3 mixture and sub-product was slag state of $\alpha$-Al2O3. Single phase of Cr3C2 was obtained when crushed main-product was heat-treated at 120$0^{\circ}C$ for 3h in vacuum state with addition of 2.5wt% C. The obtained Cr3C2 powder can be used as plasma-arc deposit material because the flowability index of powder with the size of 9-50${\mu}{\textrm}{m}$ was 66.

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수중 공동보강용 석고 활용 저 pH형 수중불분리 그라우트에 대한 실험적 연구 (Experimental Study on Low-pH, Anti-washing Grouts Incorporating Gypsum for Reinforcement of Underwater Cavities)

  • 김영상;백정진;김형기
    • 자원리싸이클링
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    • 제27권6호
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    • pp.30-37
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    • 2018
  • 석회암 기반 지반 등에 존재하는 수중공동의 보강을 위해 사용할 수 있는 석고 혼입 저 pH형 수중불분리 그라우트에 대한 기초 실험을 수행하였다. 다양한 종류의 배합을 설계하였으며 이 배합들의 유동성, 강도, 환경영향성을 평가하였다. 유동성은 자연유하, 가압유하의 두 가지 조건에 대해 평가하였다. 강도는 기중 및 수중 주입의 경우에 대해 각각 측정하였다. 환경영향성은 현탁액의 pH 및 현탁물질 농도 두가지로 평가되었다. 석고혼입을 통해 pH를 10 이하로 감소시켰으며, 포틀랜드 시멘트-규사-석고 간의 배합비 및 수중불분리제-유동화제 혼입량의 변화을 통해 모르타르 자유흐름량 7-10 cm, 압축강도 4 MPa 이상의 수중불분리 그라우트 배합을 찾아내었다.

미분시멘트를 사용한 모르터의 품질향상에 관한 연구 (A Study on Quality Improvement of Mortar Using Fine Particle Cement)

  • 이재윤;이충섭;백대현;노동현;한민철;한천구
    • 한국콘크리트학회:학술대회논문집
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    • 한국콘크리트학회 2009년도 춘계 학술대회 제21권1호
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    • pp.327-328
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    • 2009
  • 본 연구는 시멘트 제조공정 중 입도분급을 통하여 채취한 미세입자의 시멘트를 치환한 모르터의 품질향상을 위해 고로슬래그 미분말 및 석고 자극제를 치환한 경우의 실험으로써, 유동성 및 조기강도는 저 하하였으나 28일 일부 압축강도는 증가하는 것으로 나타났다.

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병용계 고유동 콘크리트의 배합요인에 따른 특성 (Properties of the Combined High Flowing Concrete by Mix Design Factors)

  • 권영호;이현호;이화진;하재담
    • 한국콘크리트학회:학술대회논문집
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    • 한국콘크리트학회 2005년도 추계 학술발표회 제17권2호
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    • pp.407-410
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    • 2005
  • This research investigates experimentally an effect on the properties of the combined high flowing concrete by mix design factors. The purpose of this study is to determine the optimum mix proportion of the combined high flowing concrete having good flowability, viscosity, no-segregation and design strength(40.0MPa). For this purpose, trial mixings used belite cement+lime stone powder(LSP) are tested by mix design factors including water-cement ratio($47.9\~54.0\%$), fine aggregate volume ratio($41\~45\%$) and coarse aggregate volume ratio($41\~45\%$). As test results of this study, the optimum mix proportion for the combined high flowing concrete is as followings. Water-cement ratio $51.0\%$, fine aggregate volume ratio $43{\pm}1\%$ and coarse aggregate volume ratio $0.30{\pm}0.05m^3/m^3$ and replacement ratio of LSP $42.7\%$.

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복합섬유 혼입에 따른 고강도콘크리트의 내화 성능 평가 (Performance Evaluation of Fire Resistance of High Strength Concrete by Incorporation of Combined Fiber)

  • 신재경;박종호;정용;문형재;김정진;박순전
    • 한국콘크리트학회:학술대회논문집
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    • 한국콘크리트학회 2010년도 춘계 학술대회 제22권1호
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    • pp.423-424
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    • 2010
  • 본 연구에서는 초고층 건물의 시공을 위하여 유기질섬유와 폴리머분말을 혼합한 복합섬유공법을 활용하여 작업성과 내화성능을 만족시키는 고강도 내화 콘크리트를 개발하고자 하였다. 실험결과 폴리믹스의 경우 폭렬방지 및 내부온도 상승 저감에 효과적인 것으로 나타나 기존의 섬유혼입공법과 유사한 수준의 내화성능을 확보하는 것으로 나타났다.

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간편 배합설계방법을 통한 중간강도 자기충전 콘크리트의 특성 (Properties of Medium Strength Self-Compacting Concrete with Simple Mix design Method)

  • 최연왕;조선규;최욱;김경환;안성일
    • 한국콘크리트학회:학술대회논문집
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    • 한국콘크리트학회 2003년도 봄 학술발표회 논문집
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    • pp.83-88
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    • 2003
  • In this paper, the medium strength self-compacting concrete with simple mix design method was manufactured and investigated about the properties of flowability and strength. Two types of binders like as fly-ash and RP(rock powder) were contained to the SCC in order to obtain the target medium strength of 270-350kgf/$cm^2$. The experimental tests about slump-flow, reaching time to the slump-flow of 50cm, V-funnel and U-box were carried out in accordance with the specified by the Japanese Society of Civil Engineering(JSCE). The mechanical properties such as compressive strength, splitting tensile strength and static modulus of elasticity were checked with the requirements specified by KS.

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