• Title/Summary/Keyword: Particulate materials

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Comparative Analysis of Elemental Components in Airborne Particulate Matter by k0-NAA Methods (대기분진의 원소분석에 대한 k0-NAA법의 비교)

  • Chung, Yong-Sam;Moon, Jong-Hwa;Cho, Hyun-Je;Kim, Young-Jin
    • Analytical Science and Technology
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    • v.18 no.1
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    • pp.51-58
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    • 2005
  • A comparison of the analytical data obtained by three $k_0$-NAA software programs was carried out using both the airborne particulate matter collected from an urban site and the certified reference materials of the air filter and urban dust to evaluate the performance of the analysis. The individual $k_0$-NAA standardization methods of three countries, Korea, China and Vietnam which had been modified from the well established $k_0$-program were used for the comparative analysis. The measured concentrations of 30 elements from the two kinds of air samples based on this software were in agreement with each other within about 20% analytical error except for a few elements. By contrast, the results of China and Vietnam were moderately higher than that of Korea due to a systematic error associated with the detection efficiency, gamma peak analysis and geometric effect.

Measurement of the Elemental Composition in Airborne Particulate Matter Using Instrumental Neutron Activation Analys

  • Chung, Yong-Sam;Lim, Jong-Myoung;Moon, Jong-Hwa;Kim, Sun-Ha;Cho, Hyun-Je;Kim, Young-Jin
    • Nuclear Engineering and Technology
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    • v.36 no.5
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    • pp.450-459
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    • 2004
  • For the evaluation of emission sources by air sampling, airborne particulate matter for fine (<2.5 ${\mu}m2$ EAD : $PM_{2.5}$) and coarse partical (2.5-10 ${\mu}m2$ EAD : $PM_{2.5-10}$ fractions were collected using a Gent stacked filter unit low volume sampler and two types of polycarbonate filters. Air samples were collected twice monthly at two regions in and around Daejeon city in the Republic of Korea from January to December 2002. Monthly mass concentration of $PM_{2.5}$ and $PM_{2.5-10}$ were measured and the concentrations of 10 marker elements (Al, Sc, Ti ; Na, Cl ; As, V. Sb, Br, Se) were determined by an instrumental neutron activation analysis. Analytical quality control was corried out using certified reference materials. Enrichment factors were also calculated from the monitoring data to classify the anthropogenic and crustal origins.

Comparison of immunohistochemical analysis on sinus augmentation using demineralized tooth graft and bovine bone

  • Sohn, Dong-Seok;Kim, Ji-Rak;Kim, Hyung-Gyun;Choi, Hyun-Suk;Moon, Yong-Suk
    • Journal of the Korean Association of Oral and Maxillofacial Surgeons
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    • v.47 no.4
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    • pp.269-278
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    • 2021
  • Objectives: The purpose of this animal research was to compare bone regeneration in augmented rabbit maxillary sinuses treated with demineralized particulate human-tooth graft and anorganic bovine bone by immunohistochemical analysis. Materials and Methods: Piezoelectric bilateral sinus augmentation was performed in eight adult rabbits. In the control group, anorganic bovine was grafted in the maxillary sinus following elevation of the sinus membrane. In the experimental group, demineralized human particulate tooth bone was grafted in the sinus. Bone regeneration in augmented sinuses was evaluated by immunohistochemical analysis using various markers of osteoprogenitor cells. Results: The number of bromodeoxyuridine-labeled cells was significantly higher in the experimental group than in the control group at eight weeks. The immunoreactivity of proliferating-cell nuclear antigen was increased slightly in the experimental group relative to the control group at eight weeks. Other bone markers were expressed equally in the two groups. Conclusion: In the rabbit maxillary sinus, higher osteoinduction was correlated with demineralized human particulate tooth bone grafting than with anorganic bovine grafting.

High Temperature Deformation Behaviour of Particulate Reinforced Aluminium Composites (입자분산강화 알루미늄 복합재료의 고온거동에 관한 연구)

  • Gwon, Hyeok-Cheon;Yun, Ui-Park
    • Korean Journal of Materials Research
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    • v.5 no.7
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    • pp.765-774
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    • 1995
  • The hot deformation behaviour of particulate reinforced aluminium 6061 Al composite were investigated by hot compression tests in the temperature range from 623K to 823K with strain rate of 10$^{-3}$ ~5.0 S$^{-1}$ . The effect of reinforced particulate volume fraction, mean diameter on the high temperature flow stress has also been studied. Experimental results showed that the increase in the volume fraction of reinforcement contributed to the rising of yield stress, but the stress above the yield point appeared to be steady state at all volume fractions. The apparent activation energy for deformation was 290KJ/mo1 for unreinforced 6061 Al, 327KJ/mo1 for 6061 Al-20vo1.% SiC composite and 531KJ/mo1 for 6061 Al-20vo1.%A1$_2$O$_3$composite. It appeared that $Al_2$O$_3$reinforced composites was more difficult to hot deform.

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Study on Flow Control of Primitive Structures for Enhancing Particulate Matter Filter Performance (미세먼지 필터 성능향상을 위한 primitive 구조의 유동 제어 연구)

  • J. B. Lee;S. H. Hwang;J. Y. Kim;H. Kim;D. Ahn;S. Y. Jung
    • Transactions of Materials Processing
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    • v.33 no.4
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    • pp.270-276
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    • 2024
  • In order to improve the performance of the PM (Particulate Matter) filter, the TPMS structure was used as a flow controller to control the flow entering the filter. Among various TPMS structures, a primitive structure that is easy to utilize 3D printing technique was selected and the effect of unit cell size was analyzed. In addition, numerical analysis was performed and swirl ratio was analyzed to confirm changes in filter inlet flow characteristics that affect changes in filter performance. Unit cell size is closely related to filter performance, and both PM collection efficiency and pressure drop increase as unit cell size decreases. Through quality factor (QF) comparison, which comprehensively evaluate collection efficiency and pressure drop, it was confirmed that when the unit cell size is 5 mm, PM collection efficiency increases, but the flow controller actually reduces filter performance. QF values are similar for unit cell sizes of 10 and 20 mm, and it is advantageous to select the unit cell size among these two considering collection efficiency and operating costs. The filter's collection performance increases due to the increase in swirl flow caused by the primitive structure, and the filter's collection efficiency increases due to the swirl flow that increases throughout the flow field as the unit cell size becomes smaller.

Barium Ferrite Media for Extremely High Density Recording Applications

  • Yang-Ki Hong;Hong-Sik Jung
    • Journal of Magnetics
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    • v.3 no.3
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    • pp.96-98
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    • 1998
  • In this paper a structurally coupled and magnetically decoupled Ba-ferrite thin film medium is proposed to evade the superparamagnetic limit and reduce media noise. The proposed medium consists of ferrimagnetic Ba-ferrite nano-grains (< 10 nm) and a non-magnetic grain boundary material. Magnetic grains are crystallographically matched with the grain boundary material. Spherical or cubic shaped Ba-ferrite particle is also proposed for above 100 Kfci particulate recording application.

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Development of Internal Dose Assessment Procedure for Workers in Industries Using Raw Materials Containing Naturally Occurring Radioactive Materials

  • Choi, Cheol Kyu;Kim, Yong Geon;Ji, Seung Woo;Koo, Boncheol;Chang, Byung Uck;Kim, Kwang Pyo
    • Journal of Radiation Protection and Research
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    • v.41 no.3
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    • pp.291-300
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    • 2016
  • Background: It is necessary to assess radiation dose to workers due to inhalation of airborne particulates containing naturally occurring radioactive materials (NORM) to ensure radiological safety required by the Natural Radiation Safety Management Act. The objective of this study is to develop an internal dose assessment procedure for workers at industries using raw materials containing natural radionuclides. Materials and Methods: The dose assessment procedure was developed based on harmonization, accuracy, and proportionality. The procedure includes determination of dose assessment necessity, preliminary dose estimation, airborne particulate sampling and characterization, and detailed assessment of radiation dose. Results and Discussion: The developed dose assessment procedure is as follows. Radioactivity concentration criteria to determine dose assessment necessity are $10Bq{\cdot}g^{-1}$ for $^{40}K$ and $1Bq{\cdot}g^{-1}$ for the other natural radionuclides. The preliminary dose estimation is performed using annual limit on intake (ALI). The estimated doses are classified into 3 groups ( < 0.1 mSv, 0.1-0.3 mSv, and > 0.3 mSv). Air sampling methods are determined based on the dose estimates. Detailed dose assessment is performed using air sampling and particulate characterization. The final dose results are classified into 4 different levels ( < 0.1 mSv, 0.1-0.3 mSv, 0.3-1 mSv, and > 1 mSv). Proper radiation protection measures are suggested according to the dose level. The developed dose assessment procedure was applied for NORM industries in Korea, including coal combustion, phosphate processing, and monazite handing facilities. Conclusion: The developed procedure provides consistent dose assessment results and contributes to the establishment of optimization of radiological protection in NORM industries.

Effect of Organic Processing Parameters in Non-aqueous Tape-casting on Dispersion Stability of Barium Titanate-Borosilicate Glass Based Suspensions (비수계 테잎성형공정의 유기공정변수의 변화에 따른 티탄산바륨-붕규산염유리계 현탁액의 분산안정성)

  • Yeo, Jeong-Gu;Choi, Sung-Churl
    • Korean Journal of Materials Research
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    • v.13 no.11
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    • pp.725-731
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    • 2003
  • The effect of organic processing parameters on the dispersion stability of the BaTiO$_3$-based dielectric particles and borosilicate glass particulate suspensions was investigated in a system where organic solvents, dispersant, binder and modifier were used as processing additives in a low temperature cofired ceramic fabrication processes. Two- and three-component organic solvents were used to disperse ceramic particles and it was found the better stability in the particulate suspension prepared in a bi-solvent, which was consists of toluene and ethanol in a non-azeotropic composition. The addition amount of organic additives had a great impact on dispersion in the present investigation. The flow curves of the suspensions prepared with binder and modifier were fitted according to the power-law equation, which indicates that the internal structure of the suspension could be disturbed under the applied shear stress. Finally, the LTCC green tapes were successfully tape-cast based upon the optimum formulation of LTCC suspension and its microstructure was compared with that of the hard-agglomerates.

Application of the full factorial design to modelling of Al2O3/SiC particle reinforced al-matrix composites

  • Altinkok, Necat
    • Steel and Composite Structures
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    • v.21 no.6
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    • pp.1327-1345
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    • 2016
  • $Al_2O_3$/SiC particulate reinforced (Metal Matrix Composites) MMCs which were produced by using stir casting process, bending strength and hardening behaviour were obtained using an analysis of variance (ANOVA) technique that uses full factorial design. Factor variables and their ranges were: particle size $2-60{\mu}m$; the stirring speed 450 rpm, 500 rpm and the stirring temperature $620^{\circ}C$, $650^{\circ}C$. An empirical equation was derived from test results to describe the relationship between the test parameters. This model for the tensile strength of the hybrid composite materials with $R^2$ adj = 80% for the bending strength $R^2$ adj = 89% were generated from the data. The regression coefficients of this model quantify the tensile strength and bending strengths of the effects of each of the factors. The interactions of all three factors do not present significant percentage contributions on the tensile strength and bending strengths of hybrid composite materials. Analysis of the residuals versus was predicted the tensile strength and bending strengths show a normalized distribution and thereby confirms the suitability of this model. Particle size was found to have the strongest influence on the tensile strength and bending strength.

Homogenized Elastic-plastic Relation based on Thermodynamics and Strain Localization Analyses for Particulate Composite (열역학 기반 내부 변수를 이용한 균질화 탄소성 구성방정식 및 입자강화 복합재에서의 소성변형집중)

  • S. J. Yun;K. K. Kim
    • Transactions of Materials Processing
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    • v.33 no.1
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    • pp.18-35
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    • 2024
  • In the present work, the evolution rules for the internal variables including continuum damage factors are obtained using the thermodynamic framework, which are in turn facilitated to derive the elastic-plastic constitutive relation for the particulate composites. Using the Mori-Tanaka scheme, the homogenization on state and internal variables such as back-stress and damage factors is carried out to procure the rate independent plasticity relations. Moreover, the degradation of mechanical properties of constituents is depicted by the distinctive damages such that the phase and interfacial damages are treated individually accordingly, whereas the kinematic hardening is depicted by combining the Armstrong-Frederick and Phillips' back-stress evolutions. On the other hand, the present constitutive relation for each phase is expressed in terms of the respective damage-free effective quantities, then, followed by transformation into the damage affected overall nominal relations using the aforementioned homogenization concentration factors. An emphasis is placed on the qualitative analyses for strain localization by observing the perturbation growth instead of the conventional bifurcation analyses. It turns out that the proposed constitutive model offers a wide range of strain localization behavior depending on the evolution of various internal variable descriptions.