• 제목/요약/키워드: P2X4

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Untersuchungen Zur Herstellung Von Neun Messpraparaten Fur Die Rontgenfluoreszenzspektrometrie (X-線 螢光分析에 있어서의 새로운 試料 調制에 關한 硏究)

  • Park, Yung-Kyu
    • Journal of the Korean Chemical Society
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    • 제11권4호
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    • pp.165-169
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    • 1967
  • Eine neue Methode zur Herstellung von Meßpraparation wird die Bestimmng der Spurenelemente Quecksilber, Kupfer, Blei, Zink, Nickel, Kobalt und Eisen durch Rontgenflureszenzspektrometrie entwickelt. Die Spurenelemente werden aus waßrigen Losungen durch Einleitung von Schwefelwasserstoff mit Aluminiumsulfat als Trager bei pH8 ausgefallt. Die Niederschlage der Metallsulfide werden uber Membranfilter filtriert, mit Gelatine fixiert und ihre Absolutmengen durch Rontgenfluoreszenz analyse bestimmt. Bei der geringen Dicke der auszumessenden Schichten treten Matrixeffekte nicht auf. Durch den Zusatz von Aluminiumsulfat-Trager wird eine gute Reproduzierbarkeit erzielt: Quecksilber, Kupfer, Blei, Zink, Nickel und Kobalt werden bei einer Konzentration von 50 bis 1000 p.p.b. mit einer relativen Standard-abweichung von 5.0% und Eisen bei einer Konzentration von 50∼1000 p.p.d. mit einer relativen Standardabweichung von 6.1% gemessen.

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Syntheses and Characteristics of $Ln_xCa_{2-x}MnO_4$ {Ln=Gd, Nd, Pr, Sm} ($Ln_xCa_{2-x}MnO_4$ 상의 합성과 특성에 관한 연구 {Ln=Gd, Nd, Pr, Sm})

  • Seo, Sang-Il;Lee, Jai-Yeoul
    • Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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    • 한국전기전자재료학회 2000년도 영호남학술대회 논문집
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    • pp.196-199
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    • 2000
  • Since the reports of CMR(colossal magnetoresistance) effects in some single crystal R-P phase $La_{1+x}Sr_{2-x}Mn_2O_7$, considerable researches have been carried out to find optimum composition and to understand the role of dimensionality in the CMR mechanism of this system. In this study, layered perovskite $Ln_xCa_{1-x}MnO_{4}$ (x=0.5, Ln=Pr, Nd, Sm, Gd) phases were synthesized by solid state reaction and their structures were refined by Rietveld method. Electrical and magnetic properties were measured between room temperature and liquid helium temperature and compared with those of two dimensional $La_{1.4}Sr_{1.6}Mn_2O_7$ phase.

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An analysis of Factorial structure of Kinematic variables in Bowling (볼링의 운동학적 분석과 주요인 구조분석)

  • Lee, Kyung-Il
    • Korean Journal of Applied Biomechanics
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    • 제12권2호
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    • pp.381-392
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    • 2002
  • This study attempted to indentify changeability of the factorial structure of kinematic analysis in bowling. Subjects of group composed of three groups : Higher bowers who are national representative bowers with 200 average point and one pro-bowler. Middle bowlers who are three common persons with 170 average points. Lower bowler who are three common persons with 150 average points. Motion analysis on throw motion in three groups respectively has been made through three-dimension cinematography using DLT method. Two high-speed video camera at operating 180 and 60 frame per secondary. T-test factorial structure analysis has been used to define variable relations. It was concluded that : 1. The difference of x1, x2, x4, x8, x9, x11, x12, x13 where significant between two group. 2. The difference of number of spin and angle of the back-hand where statistically significant between two group(p<.001, p<.05) 3. The correlation over r=.5 between the kinematic data x1, x2, x3, x9, x10, x11. In the rotation loading matrix Factor 1 was x1, x2, x9, x10 and Factor 2 relates to x3, x11. 4. In order to obtain the factor score as follow as ; Factor 1 = (0.248)X1 + (0.265)X2 + (-0.074)X3 + (0.259)X9 + (0.259)X10 + (-0.025)X11 Factor 2=(-0.016)X1 + (-0.055)X2 + (0.84)X3 + (-0.013)X9 + (-0.007)X10 + (0.553)X11.

Pericentric Inversion of the X Chromosome in a Male with Azoospermia and in the Family of a Pregnant Female Carrier (무정자증을 보이는 남성과 정상 생식력을 가진 여성의 가계에서 관찰된 X 염색체의 Pericentric Inversion)

  • Lee, Bom-Yi;Ryu, Hyun-Mee;Lee, Moon-Hee;Park, Ju-Yeon;Kim, Jin-Woo;Lee, Joong-Shik;Kim, Hye-Ok;Kim, Min-Hyung;Park, So-Yeon
    • Journal of Genetic Medicine
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    • 제5권2호
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    • pp.139-144
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    • 2008
  • We report on two cases of pericentric inversion of X chromosome. The cases were found in a 40-year-old man with azoospermia and in a family of a 38-year-old pregnant woman. The first case with 46,Y,inv(X)(p22.1q27) had concentrations of LH, prolactin, estradiol, and testosterone that were within normal ranges; however, FSH levels were elevated. Testis biopsy revealed maturation arrest at the primary and secondary spermatocytes without spermatozoa. There were no microdeletions in the 6 loci of chromosome Y. For the second case, the cytogenetic study of thepregnant woman referring for advanced maternal age and a family history of inversion X chromosome was 46,X,inv(X)(p22.11q27.2). The karyotype of her fetus was 46,X,inv(X)(p22.1q27). Among other family members, the karyotypes of an older sister in pregnancy and her fetus were 46,X,inv(X)(p22.11q27.2), and 46,Y,?inv(X), respectively. The proband's father was 46,Y,inv(X)(p22.11q27.2). All carriers in the family discussed above were fertile and phenotypically normal. In addition, the ratio of inactivation of inv(X) by RBG-banding was discordant between the two sisters, with the older sister having only 4.1% of cells carrying inactivated inv(X) while the proband had a 69.5% incidence of late replicating inv(X). Therefore, we suggest that the cause of azoospermia in the first case might be related to inversion X chromosome with positional effect. Also, the family of the second case showing normal phenotype of the balanced inv(X) might be not affected any positional effect of genes.

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Synthetic study of Zeolites from Some Glassy Rocks (I) L Low-Temperature Hydrothermal Synthesis of Zeolites Na-P, Na-X, and Na-A (유리질 암석으로부터 제올라이트 합성에 광한 연구 (I) : Na-P, Na-X 및 Na-A 제올라이트의 저온 수열 합성)

  • 노진환
    • Journal of the Mineralogical Society of Korea
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    • 제3권1호
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    • pp.7-17
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    • 1990
  • 화산 유리질 암석을 출발 물질로 사용하여 저온 ($80^{\circ}C$)에서 수열 처리하여 Na-P Na-X 및 Na-A 제올라이트를 합성하였다. 합성과정은 (1) 유리질 분말 시료와 알칼리 용액과의 용해.변질 반응에 의한 1차적인 Na-P의 합성 방식과 (2) 여기서 잔류된 규산질 모액에 Al(OH)3나 NaAlO2의 수용액을 공급하여 보다 고순도의 Na-P, Na-X 및 Na-A를 효과적으로 합성할 수 있었다. 원암의 암상과 조성은 제올라이트들의 화학 조성과 순도 및 백색도같은 물리적 특성에는 영향을 주지만, 합성된 제올라이트의 광물종을 규제하는 주된 요인은 아닌 것으로 해석된다. 합성된 제올라이트의 광물상은 반응 용액의 pH, Al(OH)4 및 Na+에 대한 농도 조건에 주로 의존되는 경향을 나타낸다. 또한 화산 유리질 암석을 제올라이트 합성원료로 활용하는 데에 있어서 (2)와 같음 합성 방안이 보완적으로 시행되면 그 생산성과 효율성을 제고시킬 수 있을 것으로 여겨진다.

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A NOTE ON CLARKSONS INEQUALITIES

  • Cho, Chong-Man
    • Bulletin of the Korean Mathematical Society
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    • 제38권4호
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    • pp.657-662
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    • 2001
  • It is proved that if for each n, $1\leqp_n\leq2 \;and \;the(p_n, p’_n)$ Clarkson inequality holds in each Banach space X$_{n}$ then the (t, t’) Clarkson inequality holds in ($\sum^\infty_{n=1}\; X_n)_r, \;the \ell^r-sum \;of\; X_n’s,\; where\; 1\leqr<\infty,\; t=min{p, r, r’} \;and \;p = \;inf{p_n}.$ The (p, p’) Clarkson inequality is preserved by quotient maps and a new proof of a Takahashi-Kato theorem stating that the (p, p’) Clarkson inequality holds in a Banach space X if and only if it holds in its dual space $X_*$ is given.n.

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Local Structure Refinement of the $BaFe_{1-x}Sn_xO_{3-y}$ System with Fe K-Edge X-Ray Absorption (XANES/EXAFS) Spectroscopy

  • 김민규;곽기섭;로권선;여철현
    • Bulletin of the Korean Chemical Society
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    • 제18권7호
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    • pp.743-749
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    • 1997
  • Local structure refinement of the BaFe1-xSnxO3-y system (x=0.00-0.50) has been carried out with Fe K-edge x-ray absorpion spectroscopic studies. It is found out that the Fe ions are placed in two different symmetric sites such as tetrahedral and octahedral sites in the compounds by comparison with Fe K-edge x-ray absorption near edge structure (XANES) spectrum of the γ-Fe2O3 compound as a reference. Small absorption peaks of dipole-forbiden transitions appear at a pre-edge region of 7111 eV due to the existence of Fe ions in the tetrahedral and octahedral sites. The peak intensity decreases with the substitution amount of Sn ion. Three different absorption peaks of 1s→4p dipole-allowed transition appear on the energy region between 7123 and 7131 eV. The peaks correspond to 1s→4p main transition of Fe ions in tetrahedral and octahedral sites and 1s→4p transition followed by the shakedown process of ligand to metal charge transfer. The bond distances between Fe ions in the tetrahedral site and nearest neighboring oxygen atom (Fe-4O), and those in octahedral site (Fe-6O) are determined with the extended x-ray absorption fine structure (EXAFS) analysis. Two different interatomic distances increase with the substitution amount of Sn ion and also the bond lengths of Fe-4O are shorter than those of Fe-6O in all compounds.

Production, Nitrogen and Phosphorus Absorption by Macrohydrophytes (대형수생식물의 물질생산과 질소와 인의 흡수량)

  • 문형태;남궁정;김정희
    • Korean Journal of Environmental Biology
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    • 제17권1호
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    • pp.27-34
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    • 1999
  • In order to obtain necessary data for the use of hydrophytes to improve water quality of artificial lakes, production and nutrients absorption by some macrohydrophytes were investigated in a small water course at Woongcheon, Chungnam Province. The maximum above-ground standing biomass of Phragmites communis, Typha angustifolia and Zizania latifolia stand were 3,504 g/m$x^2$, 2,834 g/m$x^2$ and 3,125 g/m$x^2$, respectively. Estimated below-ground standing biomass of each stand were 9,671 g/m$x^2$,5,158 g/m$x^2$ and 5,813 g/m$x^2$, respectively. Concentration of nutrients in each organ was different among plant species. Maximum amount of standing nitrogen was the highest in the reed stand and that of standing phosphorus was the highest in the cattail stand. Amount of maximum standing nutrients are 2795.6 kgN/ha and 42.5 kgP/ha for the reed stand, 1,413 kg N/ha and 24.8 kgP/ha for the cattail stand and 1.901.1 kgN/ha and 38.4 kgP/ha for the wild rice stand, respectively. According to our investigation, it is concluded that reed, cattail and wild rice are suitable for water quality improvement of artificial lakes through nutrients absorption.

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THE RULE OF TRAJECTORY STRUCTURE AND GLOBAL ASYMPTOTIC STABILITY FOR A FOURTH-ORDER RATIONAL DIFFERENCE EQUATION

  • Li, Xianyi;Agarwal, Ravi P.
    • Journal of the Korean Mathematical Society
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    • 제44권4호
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    • pp.787-797
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    • 2007
  • In this paper, the following fourth-order rational difference equation $$x_{n+1}=\frac{{x_n^b}+x_n-2x_{n-3}^b+a}{{x_n^bx_{n-2}+x_{n-3}^b+a}$$, n=0, 1, 2,..., where a, b ${\in}$ [0, ${\infty}$) and the initial values $X_{-3},\;X_{-2},\;X_{-1},\;X_0\;{\in}\;(0,\;{\infty})$, is considered and the rule of its trajectory structure is described clearly out. Mainly, the lengths of positive and negative semicycles of its nontrivial solutions are found to occur periodically with prime period 15. The rule is $1^+,\;1^-,\;1^+,\;4^-,\;3^+,\;1^-,\;2^+,\;2^-$ in a period, by which the positive equilibrium point of the equation is verified to be globally asymptotically stable.

Studies on the Quality of Silage from Domeestic Herbage I. Effects of water , corn starch and glucose as additives on Kudzu ( Puerarie thunbergii Bentham ) silage (야초 사일리지의 품질향상에 관한 연구 I. 칡 사일리지 제조에 있어서 물, 전분, 포도당 첨가효과)

  • Kim, Dae-Jin;Leem, Wan
    • Journal of The Korean Society of Grassland and Forage Science
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    • 제7권3호
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    • pp.162-167
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    • 1987
  • This experiment was conducted to determine the effect of the feeding value for the wild legumes silage-making with additives. The chopped Kudzu (Puerarie thunbergii Bentham) of wild legumes was ensiled by the conventional method in the small experimental silo of 2 liters. The additives used in the present experiments were water (8%),water (8%) plus corn starch (3%) and water (8%) plus glucose (3%). These additives as well as that of control without additive were set up and these silage were compared with the conventional corn silage. The fermentative qualities and the characteristic of fiber (neutral detergent fiber, NDF; acid detergent fiber, ADF; acid detergent lignin, ADL) of silage produced was determined by chemical analysis, and dry matter digestibility (DMD) was evaluated by pepsin-cellulase technique. The results obtained are summarized as follows: 1 The weight of Kudzu silage was lost under the 10% for all the treatments. 2 In degree of pH for the Kudzu silages with glucose, starch, control and water treatments were high 3.80,4.04,4.57 and 5.34, respectively.

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