• Title/Summary/Keyword: P-Method

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Determination of 25 EDs in Frog and Fish Tissue by GC-MS (SIM)

  • Shin, Ueon-Sang;Shin, Ho-Sang
    • Bulletin of the Korean Chemical Society
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    • v.24 no.4
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    • pp.413-420
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    • 2003
  • A gas chromatography/mass spectrometric assay method was developed for the simultaneous determination of neutral and bacis twenty-five disruptors $(ED_S)$ in frog and fish. Afther homogenization and sonication of 5 g of sample, purification was achieves in one step with a solid phase extraction procedure using silica gelflorisl. Eluton was performed with 50mL of acetone : n-hexane (1 : 9) solution. The eluate was concentrated to approximately 10uL and dissolves with 100 uL of hexane and analyzed by GC-MS (SIM). The peaks had good chromatographic properties and the extraction of these compounds from sample also gave relatively high recoveries with small variatoins. Detection limits were 0.1 ng/g for 4-nitrotoluene, benzophenone, hexachlorobenzene, atrazine, malathion, o,p-DDT, o,p-DDT and permethrin, and 0.2 ng/g for heptachlor epoxide, γ-chlordane, α-chlordane, p,p'-DDE, p,p'-DDD, cypermethrin and fenvalerate, and 0.3 ng/g for trifluralin, metribuzin, alachlor, dieldrin and p,p'-DDT, and 0.5 ng/g for heptachlor, aldrin and parathion, and 0.7 ng/g for endrin, and 0.8 ng/g for nitrofen. The recoveries were between 33 and 109%. The method was used to analyze twenty-five frogs and forty-six fishes fishes samples caught from various regions in Korea. Benzophenone was detected at concentration of up to 17.2 ng/g in frog or fish. Heptachlor, aldrin, γ-chlordane, p,p'-DDE, p,p'-DDD, endrin and o,p-DDD were detected at concentrations of 0.7-12.5 ng/g in frog or fish. Also significant leveles of dieldrin (up to 22.5 ng/g) were observed. The developed method may be valuable to be used to the national monitoring project of EDS in biota samples.

A Sclable Parallel Labeling Algorithm on Mesh Connected SIMD Computers (메쉬 구조형 SIMD 컴퓨터 상에서 신축적인 병렬 레이블링 알고리즘)

  • 박은진;이갑섭성효경최흥문
    • Proceedings of the IEEK Conference
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    • 1998.10a
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    • pp.731-734
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    • 1998
  • A scalable parallel algorithm is proposed for efficient image component labeling with local operatos on a mesh connected SIMD computer. In contrast to the conventional parallel labeling algorithms, where a single pixel is assigned to each PE, the algorithm presented here is scalable and can assign m$\times$m pixel set to each PE according to the input image size. The assigned pixel set is converted to a single pixel that has representative value, and the amount of the required memory and processing time can be highly reduced. For N$\times$N image, if m$\times$m pixel set is assigned to each PE of P$\times$P mesh, where P=N/m, the time complexity due to the communication of each PE and the computation complexity are reduced to O(PlogP) bit operations and O(P) bit operations, respectively, which is 1/m of each of the conventional method. This method also diminishes the amount of memory in each PE to O(P), and can decrease the number of PE to O(P2) =Θ(N2/m2) as compared to O(N2) of conventional method. Because the proposed parallel labeling algorithm is scalable, we can adapt to the increase of image size without the hardware change of the given mesh connected SIMD computer.

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Multivariate pHd analysis (다변량 pHd 분석)

  • 이용구
    • The Korean Journal of Applied Statistics
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    • v.8 no.1
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    • pp.61-74
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    • 1995
  • These days, many kinds of graphical methods have been developed, and it is possible to get information directly from data. Especially, R-code (Cook and Weisberg, 1994) make it possible to draw various kinds of two and three dimensional plots, and to rotate the axis of the plots. But the maximum dimensional of the plot is three, so we can not draw plot of one response variable with more than three explanatory variables. Li(1991, 1992) has developed a method to reduce the dimension of the explanatory variables, so it is possible to draw lower dimensional plots to get information of the full explanatory variables. One of the dimension reduction method developed by Li is pHd. In this paper, we have tried to apply the pHd method for the model with multivariate response.

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Preparation and Luminescence Properties of Y(P,V)O4:Eu3+ Phosphor using Impregnation Method (함침법에 의한 Y(P,V)O4:Eu3+ 형광체의 합성 및 발광특성)

  • Han, Cheong-Hwa;Kim, Soo-Jong
    • Journal of the Korean Ceramic Society
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    • v.48 no.6
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    • pp.565-570
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    • 2011
  • The $Eu^{3+}$ doped $Y(P_x,V_{1-x})O_4$ (0 ${\leq}$ x ${\leq}$ 1) phosphors were synthesized by solid-state and impregnation method and investigated as potential red-emitting phosphors for a plasma display panel(PDP). The optimal substitution proportion of P for V was determined to be 60 mol%, for $Y(P_x,V_{1-x})O_4$ doped with 8 mol% $Eu^{3+}$. The VUV PL spectra and SEM for the synthesized phosphors were measured and compared against those of a commercial red-emission phosphor. The $Y(P_x,V_{1-x})O_4$:$Eu^{3+}$ phosphors exhibited strong red at around 592, 618 and 698 nm. The emission intensity and particle size of the phosphors were controlled by preparation conditions.

Adaptive control for pH systems (pH공정의 적응제어)

  • 성수환;이인범;이지태
    • 제어로봇시스템학회:학술대회논문집
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    • 1996.10b
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    • pp.457-460
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    • 1996
  • An adaptive pH control is developed to manipulate the nonlinearities and time-varying properties of pH systems. In this research, we estimate two adjustable parameters by using the recursive least squares method and a nonlinear PI controller is used to control pH systems based on the estimated two parameters.

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A Study on the Maternal Perception of Her Newborn Baby (신생아에 대한 산모의 감지도에 관한 연구)

  • 박영숙;변희재
    • Journal of Korean Academy of Nursing
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    • v.14 no.1
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    • pp.50-59
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    • 1984
  • The purpose of this study was to evaluate the maternal perception of her newborn and identify the risk of mother-infant relationship. Broussard's Neonatal Perception Inventories were completed by 113 mothers on the first or second postpartum day (Time I ) while they were still in the University Hospital. These inventories were again administered when the infants were approximately one month of age (Time Ⅱ). The data was analyzed by S.P.S.S. program and the results were as follows: 1) There were differences between the mothers' exportations of the average baby and perceptions of their babies at Time I and Time Ⅱ (p<0.01). 2) The maternal perception of her newborn at Time I was not related with the education, the parity, the experience of abortion, the type of delivery and the sex of baby but related with the method of feeding (p<0.05). 3) The maternal perception of her newborn at Time Ⅱ was not related with the education, the parity, the experience of abortion, the type of delivery and the method of feeding but related with the sex of baby (p<0.05). 4) The changes of maternal perception between Time I and Time Ⅱ were not related with the education, the parity, the experience of abortion, the method of delivery and the sex of baby but related with the method of feeding (p<0.1). 5) The maternal perception of the newborn was not correlated with the age and the duration of labor.

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In-situ Calibration of the Hydroperoxyl Radical Using an Immobilized TiO2 Photocatalyst in the Atmosphere

  • Kwon, Bum-Gun
    • Bulletin of the Korean Chemical Society
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    • v.29 no.4
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    • pp.785-789
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    • 2008
  • The present study is the first report of utilizing $TiO_2$ photocatalyst to analytically calibrate the hydroperoxyl radical ($HO_2\;^{\cdot}$). An in-situ calibration method of $HO_2\;^{\cdot}$ is proposed for air monitoring by using an 2-methyl-6-(pmethoxyphenyl)- 3,7-dihydroimidazo-[1,2-a]pyrazin-3-one (MCLA)-chemiluminescence (CL) technique. In this method, $HO_2\;^{\cdot}$($pK_a$ = 4.80) is produced by the ultraviolet (UV) photolysis of immobilized $TiO_2$ using a constant flow rate of air equilibrated water, in which $HO_2\;^{\cdot}$ is controlled by using various lengths of knotted tubing reactor (KTR). The principle of the proposed calibration is based on the experimentally determined halflife ($t_{1/2}$) of $HO_2\;^{\cdot}$ and its empirically observed pH-dependent rate constant, $k_{obs}$, at a given pH. The concentration of $HO_2\;^{\cdot}$/$O_2\;^{\cdot}$− is increased as pH increases. This pH dependence is due to the different disproportionative reactivities between $HO_2\;^{\cdot}$/$O_2\;^{\cdot}$− and $HO_2\;^{\cdot}$/$O_2\;^{\cdot}$−. Experimental results indicate the practical feasibility of the approach, producing very promising method.

HV-SoP Technology for Maskless Fine-Pitch Bumping Process

  • Son, Jihye;Eom, Yong-Sung;Choi, Kwang-Seong;Lee, Haksun;Bae, Hyun-Cheol;Lee, Jin-Ho
    • ETRI Journal
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    • v.37 no.3
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    • pp.523-532
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    • 2015
  • Recently, we have witnessed the gradual miniaturization of electronic devices. In miniaturized devices, flip-chip bonding has become a necessity over other bonding methods. For the electrical connections in miniaturized devices, fine-pitch solder bumping has been widely studied. In this study, high-volume solder-on-pad (HV-SoP) technology was developed using a novel maskless printing method. For the new SoP process, we used a special material called a solder bump maker (SBM). Using an SBM, which consists of resin and solder powder, uniform bumps can easily be made without a mask. To optimize the height of solder bumps, various conditions such as the mask design, oxygen concentration, and processing method are controlled. In this study, a double printing method, which is a modification of a general single printing method, is suggested. The average, maximum, and minimum obtained heights of solder bumps are $28.3{\mu}m$, $31.7{\mu}m$, and $26.3{\mu}m$, respectively. It is expected that the HV-SoP process will reduce the costs for solder bumping and will be used for electrical interconnections in fine-pitch flip-chip bonding.

CPT-based lateral displacement analysis using p-y method for offshore mono-piles in clays

  • Kim, Garam;Park, Donggyu;Kyung, Doohyun;Lee, Junhwan
    • Geomechanics and Engineering
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    • v.7 no.4
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    • pp.459-475
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    • 2014
  • In this study, a CPT-based p-y analysis method was proposed for the displacement analysis of laterally loaded piles. Key consideration was the continuous soil profiling capability of CPT and cone resistance profiles that do not require artificial assumption or simplification for input parameter selection. The focus is on the application into offshore mono-piles embedded in clays. The correlations of p-y function components to the effective cone resistance were proposed, which can fully utilize CPT measurements. A case example was selected from the literature and used to validate the proposed method. Various parametric studies were performed to examine the effectiveness of the proposed method and investigate the effect of property profile and its depth resolution on the p-y analysis. It was found that the calculation could be largely misleading if wrongly interpreted sub-layer condition or inappropriate resolution of input soil profile was involved in the analyses. It was also found that there is a significant influence depth that dominates overall load response of pile. The soil profile and properties within this depth range affect most significantly calculated load responses, confirming that the soil profile within this depth range should be identified in more detail.