• 제목/요약/키워드: Out-of-Phase Mode

검색결과 211건 처리시간 0.026초

Rapid Determination of Chlorostyrenes in Fish by Freezing-Lipid Filtration, Solid-Phase Extraction and Gas Chromatography-Mass Spectrometry

  • Kim, Min-Sun;Park, Kwang-Sik;Pyo, Hee-Soo;Hong, Jong-Ki
    • Bulletin of the Korean Chemical Society
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    • 제29권2호
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    • pp.352-356
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    • 2008
  • An analytical method has been developed for measuring chlorostyrenes in fish tissue sample. Extraction of chlorostyrenes from fish tissue was carried out by ultrasonication using acetone/n-hexane (5:2, v/v) mixture. Most of the lipids in the extract were eliminated by freezing-lipid filtration, prior to solid-phase extraction (SPE) cleanup. During freezing-lipid filtration, about 90% of the lipids extracted from the fish samples were easily removed without any significant losses of chlorostyrenes. For purification, SPE using Florisil was used for the rapid and effective cleanup. Quantification was performed using gas chromatography-mass spectrometry in the selected ion monitoring mode. Spiking experiments were carried out to determine the recovery, precision, and limits of detection (LODs) of the method. The overall recovery was above 80% in the spiked fish tissue sample at 10 and 100 ng/g levels, respectively. The detection limits for chlorostyrenes were ranged from 0.05 to 0.1 ng/g. This developed method is demonstrated to give efficient recoveries and LODs for detecting chlorostyrenes spiked into fish tissue with high lipid content.

Holographic phase gratings in back- and frontlights for LCD's

  • Bastiaansen, C.W.M.;Heesch, C. van;Broer, D.J.
    • 한국정보디스플레이학회:학술대회논문집
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    • 한국정보디스플레이학회 2006년도 6th International Meeting on Information Display
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    • pp.421-421
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    • 2006
  • The light and energy-efficiency of classical liquid crystal displays is notoriously poor due to the use of absorption-based linear polarisers and colour filters. For instance, the light efficiency of PVAL polarisers is typically between 40 and 45 % and the colour filters have a typical efficiency below 35 % which results in a total light and energy-efficiency of the display below 10 %. In the past, a variety of polarizers were developed with an enhanced efficiency in generating linearly polarized light. Typically, these polarizers are based on the polarisationselective reflection, scattering or refraction of light i.e. one polarisation direction of light is directly transmitted to the LCD/viewer and the other polarization direction of light is depolarised and recycled which results in a typical efficiency for generating linearly polarized light of 70-85 %. Also, special colour filters have been proposed based on chiral-nematic reactive mesogens which increase the efficiency of generating colour. Despite the enormous progress in this field, a need persists for improved methods for generating polarized light and colour based on low cost optical components with a high efficiency. Here, the use of holographic phase gratings is reported for the generation of polarized light and colour. The phase grating are recorded in a photopolymer which is coated onto a backor frontlight for LCDs. Typically the recording is performed in the transmisson mode or in the waveguiding mode and slanted phase gratings are generated with their refractive index modulation at an angle between 20o and 45o with the normal of the substrate. It is shown that phase gratings with a high refractive index modulation and a high efficiency can be generated by a proper selection of the photopolymer and illumination conditions. These phase gratings coupleout linearly polarized light with a high contrast (> 100) and the light is directed directly to the LCD/viewer without the need for redirection foils. Dependent on the type of phase grating, the different colours are coupled-out at a slightly different angle which potentially increases the efficiency of classical colour filters. Moreover, the phase gratings are completely transparent in direct view which opens the possibility to use them in frontlights for LCDs. Holographic polarization gratings posses a periodic pattern in the polarization state of light (and not in the intensity of light). A periodic pattern in the polarization direction of linearly polarized light is obtained upon interference of two circularly polarized laser beams. In the second part of the lecture, it is shown that these periodic polarization patterns can be recorded in a linear photo-polymerizable polymer (LPP) and that such an alignment layer induces a period rotation in the director of (reactive and non-reactive) liquid crystals. By a proper design, optical components can be produced with only first order diffraction and with a very high efficiency (>0.98). It is shown that these diffraction gratings are potentially useful in projection displays with a high brightness and energy efficiency

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유한한 Bandwidth를 갖는 비선형 불규칙 파열에서의 Threshold Crossing Rate, 위상분포와 파군특성 (Threshold Crossing Rate, Phase Distribution and Group Properties of Nonlinear Random Waves of finite Bandwidth)

  • 조용준
    • 한국수자원학회논문집
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    • 제30권3호
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    • pp.225-233
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    • 1997
  • 부체의 장주기동요, 연안구조물과 계류선의 파괴 등과 같은 역기능으로 인해 파군현상의 정확한 해석은 시급한 과제라 하겠다. 본고에서는 연안계에서 발생하는 파랑과 가장 근접한 비선형불규칙 파랑계를 산정하여 해안구조물의 피로거동에 지대한 영향을 미치는 파군당 파랑의 수와 해안구조물의 first excursion failure mode를 결정하는 high run에서의 파랑수를 중심으로 파군현상을 해석하였다. 해석과정에 mapping technique과 유의파경사를 perturbation parameter로 섭동이론이 사용되었다. 해석결과 Gaussian wave계에서 균등분포하는 것으로 알려진 위상함수는 평균값 주위에 집중분포하였고, 그 정도는 비선형성이 증가할수록 심화되었다. threshold crossing rate의 경우 비선형성이 심화될수록 평균해수위보다 큰 쪽으로 분포형이 이동하였으며 파군당 파랑수와 high run에서의 파랑수도 비슷한 경향을 보여 최근 설치범위가 심해쪽으로 확대되는 해안구조믈의 경우 피로거동에 대한 보강이 요만된다.

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식품중 발기부전 치료제 및 유사물질 함량에 관한 조사연구 (A Study on Contents of Anti-impotence drug/drug-like compounds in Food)

  • 홍해근;방선재;박광희;이인숙;박민정;박정화;김종찬
    • 환경위생공학
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    • 제22권3호
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    • pp.89-96
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    • 2007
  • To determine 8 anti-impotence drug/drug-like compounds such as sildenafil, vardenafil, tadalafil, homosildenafil, hydroxyhomosildenafil, aminotadalafil, pseudovardenafil and hongdenafil in foods, simultaneously, high performance liquid chromatography(HPLC) and liquid chromatography-mass spectrometry (LC/MS) were used. The HPLC/UV analysis was performed on a column of capcellpak $C_{18}$ with 0.1% sodium-1-hexansulfonate in 0.2M ammonium formate/acetonitrile as a mobile phase. Mass spectra of the compounds by LC/MS were investigated with SCAN mode(Mass range and Fragment voltage) and SIM(Selected Ion Monitoring) mode (Ion target and Fragment voltage). The results follow as; 1. The HPLC/UV analysis was detected from 5 out of 63 samples. The content of sildenafil was in the range of 32.80 ppm ${\sim}$ 60.13 ppm from 4 out of 5 samples. The contents of sildenafil, vardenafil, homosildenafil were in the range 47.14 ppm from 1 out of 5 samples. 2. The conformed result of LC/MS was equal of detected from 5 out of 63 samples in HPLC/UV analysis. An easily available, simultaneous determination of 8 standards in adulterated health related foods was established by using a combination of LC/MS methods.

트랙터의 전자유압식(電子油壓式) 히치 제어(制御) 시스템에 관한 연구(硏究)(II) -견인력제어(牽引力制御)- (Electronic-hydraulic Hitch Control System for Agricultural Tractor -Draft Control-)

  • 유수남;류관희;윤여두
    • Journal of Biosystems Engineering
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    • 제14권4호
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    • pp.229-241
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    • 1989
  • The purposes of this study were to develop an electronic-hydraulic draft control system for tractor implements, to investigate the control performance of the system and the possibility of adaptation to the conventional tractor. Experiments were carried out to investigate the responses of the system to the step and sinusoidal inputs in draft control. The effects of control mode, hydraulic flow rate, reference deadband, and proportional constant on control performance of the system were investigated. Moreover, the effects of filtering signals from draft sensor were also investigated. The following conclusions were derived from the study; 1. In draft control, there were hunting problems in controlling the implement without filtering the draft signals. Filtering was performed by a control program of electronic controller and the control performance and stability of the system were improved significantly. 2. For the draft control system operated on on-off control mode, draft was controlled within ${\pm}27-{\pm}55kg_f$ to the reference draft when the hydraulic flow rates were 5-15 l/min. For the draft control system operated on PWM control, draft was controlled within ${\pm}27kg_f$ to the reference draft regardless of hydraulic flow rates. 3. In the frequency responses of the draft control system, control performance on PWM control mode was not better than on on-off control mode because of characteristics of hydraulic valve and drafe sensor. As the hydraulic flow rates increased for the system operated on on-off control mode, the corner frequency of amplitude attenuation increased, but the corner frequency of phase-angle change remained nearly the same. But, the system was unstable beyond the frequency of 3.1 rad/s. 4. The electronic-hydraulic hitch control system developed in this study showed superior control performance, stability and convenience compared to conventional mechanical-hydraulic hitch control system. It is considered to be a superior replacement for the conventional mechanical-hydraulic hitch control system.

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자기부상열차용 선형유도전동기의 회생 제동 특성 해석 (Regenerative Braking Characteristics of Linear induction Motor for MAGLEV)

  • 박승찬;이원민;김정철;박영호
    • 한국철도학회:학술대회논문집
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    • 한국철도학회 2008년도 춘계학술대회 논문집
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    • pp.1866-1870
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    • 2008
  • In this paper, electric braking performances of linear induction motor(LIM) designed for propelling the MAGLEV are presented. Regenerative braking is carried out from 110km/h to 20km/h, and plugging which converts the direction of travelling magnetic field is carried out in the low speed region below 20km/h. It is important to reduce attractive force which can affect the magnetic levitation load during regenerative braking or plugging operation mode. So in this paper the braking performances are analyzed by finite element method. As a result, braking force, attractive force, phase current, voltage to frequency patterns and its magnetic fields of braking LIM are presented.

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A Voltage Regulation System for Independent Load Operation of Stand Alone Self-Excited Induction Generators

  • Kesler, Selami;Doser, Tayyip L.
    • Journal of Power Electronics
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    • 제16권5호
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    • pp.1869-1883
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    • 2016
  • In recent years, some converter structures and analyzing methods for the voltage regulation of stand-alone self-excited induction generators (SEIGs) have been introduced. However, all of them are concerned with the three-phase voltage control of three-phase SEIGs or the single-phase voltage control of single-phase SEIGs for the operation of these machines under balanced load conditions. In this paper, each phase voltage is controlled separately through separated converters, which consist of a full-bridge diode rectifier and one-IGBT. For this purpose, the principle of the electronic load controllers supported by fuzzy logic is employed in the two-different proposed converter structures. While changing single phase consumer loads that are independent from each other, the output voltages of the generator are controlled independently by three-number of separated electronic load controllers (SELCs) in two different mode operations. The aim is to obtain a rated power from the SEIG via the switching of the dump loads to be the complement of consumer load variations. The transient and steady state behaviors of the whole system are investigated by simulation studies from the point of getting the design parameters, and experiments are carried out for validation of the results. The results illustrate that the proposed SELC system is capable of coping with independent consumer load variations to keep output voltage at a desired value for each phase. It is also available for unbalanced consumer load conditions. In addition, it is concluded that the proposed converter without a filter capacitor has less harmonics on the currents.

비선형부하에 의해 발생한 전원 전류의 고조파를 제거하기 위한 단상 병렬형 Active Power Filter의 구현 (The Realization of a Single-Phase Parallel Active Power Filter to Eliminate Harmonics of Source Current Generated by Nonlinear Loads)

  • 장목순;이후찬;김상훈;박종연
    • 대한전기학회:학술대회논문집
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    • 대한전기학회 2006년도 제37회 하계학술대회 논문집 A
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    • pp.220-221
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    • 2006
  • This paper presents a single-phase parallel active power filter with an analog control circuit to eliminate for harmonic source currents generated by nonlinear loads. The proposed system removes the harmonic source currents by injecting a compensation current that is 180' out of phase with the load harmonic current. The detection of the load harmonics is realized by a simple new structure, referred to the Notch Filter with GIC (Generalized Impedance Converter), which has higher Q than existing harmonic detecters and a simpler structure. The compensation current is obtained using the proposed harmonic detection circuit, DC-Link voltage, and output current of the full-bridge inverter controlled current mode PWM controller. The operation of the proposed system is verified experimentally.

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Slip-Mode Frequency Shift 단독운전 검출 기법의 정상상태 전력 품질 개선 (Design of Modified Slip-Mode Frequency Shift Islanding Detection Method for Power Quality Improvement)

  • 김동욱;김성민
    • 전기전자학회논문지
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    • 제22권3호
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    • pp.539-547
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    • 2018
  • 계통 연계형 인버터는 단독운전 조건에서 반드시 전력 공급을 차단해야 한다. 이러한 이유로 분산 발전 시스템은 단독운전을 검출 기능을 반드시 가지고 있어야 한다. 분산 발전용 인버터에 적용되는 일반적인 방법 중에는 Slip-Mode frequency Shift (SMS) 단독운전 검출 기법이 있다. SMS 기법은 계통 전압의 주파수에 따라 무효 전력을 공급하여 단독운전 조건에서 계통 주파수를 허용 범위 밖으로 이동시키는 방법이다. SMS 기법은 안정적으로 단독운전을 검출할 수 있으며, 계통 전류에 고주파를 인가하지 않는다는 장점이 있으나, 무효 전류를 인가하기 때문에 계통 역률이 나빠져서 전력 품질의 저하를 가져온다. 본 논문에서는 계통 전원이 연결되어 있는 정상 조건에서 전력 품질 저하가 없는 수정된 SMS 기법을 제안한다. 600W 단상 인버터 실험을 통해 제안된 방법의 유효성을 검증한다.

강한 음향장에 구속된 고압 액적의 연소 (Unsteady Vaporization of Burning Droplet at High Pressure Environments With Linear Acoustic Mode)

  • 김성엽;신현호;윤웅섭
    • 대한기계학회:학술대회논문집
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    • 대한기계학회 2004년도 추계학술대회
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    • pp.1122-1127
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    • 2004
  • an isolated droplet combustion exposed to pressure perturbations in stagnant gaseous environment is numerically conducted. Governing equations are solved for flow parameters at gas and liquid phases separately and thermodynamic parameters at the interfacial boundary are matched for problem closure. For high-pressure effects, vapor-liquid interfacial thermodynamics is rigorously treated. A series of parametric calculations in terms of mean pressure level and wave frequencies are carried out employing a n-pentane droplet in stagnant gaseous air. Results show that the operating pressure and driving frequency have an important role in determining the amplitude and phase lag of a combustion response. Mass evaporation rate responding to pressure waves is amplified with increase in pressure due to substantial reduction in latent heat of vaporization. Phase difference between pressure and evaporation rate decreases due to the reduced thermal inertia at high pressure. In addition to this, augmentation of perturbation frequency also enhances amplification of vaporization rate because the time period for the pressure oscillation is much smaller than the liquid thermal inertia time. The phase of evaporation rate shifts backward due to the elevated thermal inertia at high acoustic frequency.

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