• Restorative Dentistry and Endodontics
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• v.37 no.1
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• pp.41-49
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• 2012

Objectives: The internal adaptation of composite restorations with or without resin modified glass ionomer cement (RMGIC) was analyzed non-destructively using Microcomputed tomography (micro-CT). Materials and Methods: Thirty intact human teeth were used. The specimens were divided into 3 groups. In the control group, the cavities were etched with 10% phosphoric acid for 15 sec. Composite resin was filled into the cavity without adhesive. In group 1, light cured glass ionomer cement (GIC, Fuji II LC, GC) was applied as a base. The cavities were then etched, bonded, light cured and filled with composites. In group 2, the cavities were then etched, bonded, light cured and filled with composites without base application. They were immersed in a 25% silver nitrate solution. Micro-CT was performed before and after mechanical loading. One-way ANOVA with Duncan analysis was used to compare the internal adaptation between the groups before or after loading. A paired t-test was used to compare internal adaptation before and after mechanical loading. All statistical inferences were made within the 95% confidence interval. Results: The silver nitrate solution successfully penetrated into the dentinal tubules from the pulp spaces, and infiltrated into the gap between restoration and pulpal floor. Group 2 showed a lower adaptation than the control group and group 1 (p < 0.05). There was no significant difference between the control group and group 1. For all groups, there was a significant difference between before and after mechanical loading (p < 0.05). Conclusions: The internal adaptation before and after loading was better when composites were bonded to tooth using adhesive than composites based with RMGIC.

• The Journal of Advanced Prosthodontics
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• v.7 no.6
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• pp.446-453
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• 2015

PURPOSE. To compare the push-out bond strength of feldspar and zirconia-based ceramic inlays bonded to dentin with different resin cements following simulated aging. MATERIALS AND METHODS. Occlusal cavities in 80 extracted molars were restored in 2 groups (n=40) with CAD/CAM feldspar (Vitablocs Trilux forte) (FP) and zirconia-based (Ceramill Zi) (ZR) ceramic inlays. The fabricated inlays were luted in 2 subgroups (n=20) with either etch-and-bond (RelyX Ultimate Clicker) (EB) or self-adhesive (RelyX Unicem Aplicap) (SA) resin cement. Ten inlays in each subgroup were subjected to 3,500 thermal cycles and 24,000 loading cycles, while the other 10 served as control. Horizontal 3 mm thick specimens were cut out of the restored teeth for push out bond strength testing. Bond strength data were statistically analyzed using 1-way ANOVA and Tukey's comparisons at ${\alpha}=.05$. The mode of ceramic-cement-dentin bond failure for each specimen was also assessed. RESULTS. No statistically significant differences were noticed between FP and ZR bond strength to dentin in all subgroups (ANOVA, P=.05113). No differences were noticed between EB and SA (Tukey's, P>.05) bonded to either type of ceramics. Both adhesive and mixed modes of bond failure were dominant for non-aged inlays. Simulated aging had no significant effect on bond strength values (Tukey's, P>.05) of all ceramic-cement combinations although the adhesive mode of bond failure became more common (60-80%) in aged inlays. CONCLUSION. The suggested cement-ceramic combinations offer comparable bonding performance to dentin substrate either before or after simulated aging that seems to have no adverse effect on the achieved bond.

• Proceedings of the Korean Society of Precision Engineering Conference
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• 2003.06a
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• pp.533-537
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• 2003

Compared to sintered polycrystalline diamond (PCD), the deposited thin film diamond has a great advantage on the fabrication of cutting tools with complex geometries such as drills. Because of high performance in high speed machining non-ferrous difficult-to-cut materials in the field of automobiles industry, aeronautics and astronautics industry, diamond-coated drills find large potentialities in commercial applications. However, the poor adhesion of the diamond film on the substrate and high surface roughness of the drill flute adversely affect the tool lift and machining quality and they become the main technical barriers for the successful development and commercialization of diamond-coated drills. In this paper, diamond thin films were deposited on the commercial WC-Co based drills by the electron aided hot filament chemical vapor deposition (EACVD). A new multiple coating technology based on changing gas pressure in different process stages was developed. The large triangular faceted diamond grains may have great contribution to the adhesive strength between the film and the substrate, and the overlapping ball like blocks consisted of nanometer sized diamond crystals may contribute much to the very low roughness of diamond film. Adhesive strength and quality of diamond film were evaluated by scanning electron microscope (SEM), atomic force microscope (AFM), Raman spectrum and drilling experiments. The ring-block tribological experiments were also conducted and the results revealed that the friction coefficient increased with the surface roughness of the diamond film. From a practical viewpoint, the cutting performances of diamond-coated drills were studied by drilling the SiC particles reinforced aluminum-matrix composite. The good adhesive strength and low surface roughness of flute were proved to be beneficial to the good chip evacuation and the decrease of thrust and consequently led to a prolonged tool lift and an improved machining quality. The wear mechanism of diamond-coated drills is the abrasive mechanical attrition.

• Journal of Radiation Industry
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• v.17 no.4
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• pp.369-375
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• 2023

Radon, a carcinogenic substance generated from soil or building materials, have to be fundamentally blocked from entering indoors. In this study, ethylene vinyl acetate (EVA)/silicone emulsions with excellent mechanical and thermal properties and effective blocking of radon gas were prepared by using radiation technology. As the electron-beam irradiation does increased, a partially crosslinked structure was formed in EVA molecular chain, increasing tensile properties and adhesive strength. The EVA/silicone film showed excellent thermal stability without deformation. In addition, the non-irradiated EVA/silicone film showed a radon blocking rate of about a 75%, while the EVA/silicone film irradiated with 3 and 5 kGy showed an excellent radon blocking rate of over 90% due to the formation of crosslinked structure in the EVA molecular chain. These results indicated that the radiation technology can effectively block radon by forming a partially crosslinked structure of EVA/silicone emulsion to improve tensile property, adhesive strength, and deformation stability.

• Journal of the Korean Society of Propulsion Engineers
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• v.12 no.2
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• pp.40-47
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• 2008

It is known that the adhesive interface testing of the rocket motor using the ultrasonic wave is superior to the other testing methods about the ability to economical detect the defects. But, the signal analysis of the ultrasonic wave takes a lot of time and efforts because the time interval of the transmitted pulse and the received pulse is too short to separate the reflected signals due to the multi-layers of the rocket motor. The ultrasonic testing of rocket motor have only applied to the automatic system about extremely limited areas like the debond in adhesive interface between the motor case and the insulator. In this study the new technique to detect the debond between the liner and the propellant using the property of the resonance and the lamb waves instead of the existing ultrasonic testing was described.

• Proceedings of the Korean Society of Propulsion Engineers Conference
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• 2007.11a
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• pp.55-59
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• 2007

It is known that the adhesive interface testing of the rocket motor which using the ultrasonic wave iS superior to the other testing methods about the economically detectable abiliη of the defects. But, the signal analysis of the ultrasonic wave takes too much time and effort that the time interval of the transmitted pulse and the received pulse is too short to be separated the reflected signals because the structure of the rocket motor is multi-layers. The ultrasonic testing of rocket motor have been only applied with automatic system about extremely limited area like the debond in adhesive interface between the motor case and insulator. In this study the new technique to detect the debond between the liner and the propellant using the property of the resonance and Lamb waves was described as comparing the existence ultrasonic testing.

• The Journal of the Korean dental association
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• v.53 no.12
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• pp.958-966
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• 2015

Objective: Sodium hypochlorite (NaOCl) decreases the bond strength of resin composite. The purpose of this study was to compare the effect of antioxidant and superficial dentin surface removal on the microtensile bond strength of NaOCl-treated dentin. Materials and Methods: Twenty non-carious human third molars were used in this study. The dentin surfaces were treated with 5.25% NaOCl for 10 min, followed either by treatment with 10% ascorbic acid or superficial dentin surface removal. Two-step self-etch adhesive and resin composite were used for restoration. The bonded specimens were subjected to the microtensile bond strength test. Statistical analysis was performed using one-way analysis of variance (ANOVA) and Tukey's test (p < 0.05). Results: The bond strength after removal of the superficial dentin surface following NaOCl irrigation was similar to that in the control group. The group treated with 10% ascorbic acid demonstrated significantly higher bond strength than the other groups. Conclusion: NaOCl irrigation-induced reduction in dentin bond strength could be recovered by either treatment with 10% ascorbic acid or simple removal of the superficial dentin surface.

• Restorative Dentistry and Endodontics
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• v.43 no.2
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• pp.20.1-20.9
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• 2018

Objectives: The aim of this in vitro study was to evaluate the bond strength of 2 universal adhesives used in different application modes to bleached enamel. Materials and Methods: Extracted 160 sound human incisors were used for the study. Teeth were divided into 4 treatment groups: No treatment, 35% hydrogen peroxide, 16% carbamid peroxide, 7.5% carbamid peroxide. After bleaching treatments, groups were divided into subgroups according to the adhesive systems used and application modes (n = 10): 1) Single Bond Universal, etch and rinse mode; 2) Single Bond Universal, self-etch mode; 3) Gluma Universal, etch and rinse mode; 4) Gluma Universal, self-etch mode. After adhesive procedures nanohybrid composite resin cylinders were bonded to the enamel surfaces. All specimens were subjected to shear bond strength (SBS) test after thermocycling. Data were analyzed using a 3-way analysis of variance (ANOVA) and Tukey post hoc test. Results: No significant difference were found among bleaching groups (35% hydrogen peroxide, 16% carbamid peroxide, 7.5% carbamid peroxide, and no treatment groups) in the mean SBS values. There was also no difference in SBS values between Single Bond Universal and Gluma Universal at same application modes, whereas self-etch mode showed significantly lower SBS values than etch and rinse mode (p < 0.05). Conclusions: The bonding performance of the universal adhesives was enhanced with the etch and rinse mode application to bleached enamel and non-bleached enamel.

• Computers and Concrete
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• v.24 no.1
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• pp.37-49
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• 2019

In this study, the shear behaviour of reinforced concrete (RC) beams that were retrofitted using precast panels of ultra-high performance fiber reinforced concrete (UHPFRC) is presented. The precast UHPFRC panels were glued to the side surfaces of RC beams using epoxy adhesive in two different configurations: (i) retrofitting two sides, and (ii) retrofitting three sides. Experimental tests on the adhesive bond were conducted to estimate the bond capacity between the UHPFRC and normal concrete. All the specimens were tested in shear under varying levels of shear span-to-depth ratio (a/d=1.0; 1.5). For both types of configuration, the retrofitted specimens exhibited a significant improvement in terms of stiffness, load carrying capacity and failure mode. In addition, the UHPFRC retrofitting panels glued in three-sides shifted the failure from brittle shear to a more ductile flexural failure with enhancing the shear capacity up to 70%. This was more noticeable in beams that were tested with a/d=1.5. An approach for the approximation of the failure capacity of the retrofitted RC beams was evolved using a multi-level regression of the data obtained from the experimental work. The predicted values of strength have been validated by comparing them with the available test data. In addition, a 3-D finite element model (FEM) was developed to estimate the failure load and overall behaviour of the retrofitted beams. The FEM of the retrofitted beams was conducted using the non-linear finite element software ABAQUS.

• Advances in aircraft and spacecraft science
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• v.4 no.6
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• pp.729-744
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• 2017

This investigation highlights rationale of electrically conductive nano adhesives for its essential application for Electromagnetic Interference (EMI) Shielding in satellites and Lightning Strike Protection in aircrafts. Carbon Nano Fibres (CNF) were functionalized by electroless process using Tollen's reagent and by Plasma Enhanced Chemical Vapour Deposition (PECVD) process by depositing silver on CNF. Different weight percentage of CNF and silver coated CNF were reinforced into the epoxy resin hardener system. Scanning Electron Microscopy (SEM) micrographs clearly show the presence of CNF in the epoxy matrix, thus giving enough evidence to show that dispersion is uniform. Transmission Electron Microscopy (TEM) studies reveal that there is uniform deposition of silver on CNF resulting in significant improvement in interfacial adhesion with epoxy matrix. There is a considerable increase in thermal stability of the conductive nano adhesive demonstrated by Differential Scanning Calorimetry (DSC) and Thermogravimetric Analysis (TGA). Four probe conductivity meters clearly shows a substantial increase in the electrical conductivity of silver coated CNF-epoxy composite compared to non-coated CNF-epoxy composite. Tensile test results clearly show that there is a significant increase in the tensile strength of silver coated CNF-composites compared to non-coated CNF-epoxy composites. Consequently, this technology is highly desirable for satellites and EMI Shielding and will open a new dimension in space research.