• 제목/요약/키워드: Nanoparticle Dispersion

검색결과 94건 처리시간 0.028초

The Influence of Functionalization of the Fe3O4 Nanoparticle on its Dispersion Property

  • Han, Jin Soon;An, Gye Seok;Park, Bong Geun;Choi, Sung-Churl
    • 한국세라믹학회지
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    • 제55권1호
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    • pp.80-84
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    • 2018
  • In this study, to improve the dispersity of $Fe_3O_4$ nanoparticles, dispersion properties were considered with various types of functionalization of $Fe_3O_4$ nanoparticles. Due to its high surface area, the electrically neutral state of its surfaces, and its magnetic momentum, $Fe_3O_4$ nanoparticles are easily aggregated in solution. In order to prevent aggregation, $Fe_3O_4$ nanoparticles were functionalized with carboxyl and amine groups in the form of a polymer compound. Carboxyl and amine groups were attached to the surface of $Fe_3O_4$ nanoparticles and the absolute value of the zeta potential was found to be enhanced by nearly 40 eV. Furthermore, the morphology and the magnetic property were analyzed for the application of $Fe_3O_4$ nanoparticles as a magnetic fluid.

초음파 분산을 이용한 Epoxy-Organoclay 나노콤포지트 구조적 그리고 유전특성에 관한 연구 (Structural and Dielectric Properties of Epoxy-Organoclay Nanocomposites using Power Ultrasonic Dispersion)

  • 박재준
    • 전기학회논문지
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    • 제57권9호
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    • pp.1572-1578
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    • 2008
  • The effect of the organoclay_10A nanoparticles on the DSC and Structural and Dielectrics Properties(1Hz-1MHz) for epoxy/Organoclay_10A Nanocomposites has been studied. Dielectric properties of epoxy-Organoclay nanocomposites were investigated at 1, 3, 5, 7, 9 filler concentration by weight. Epoxy nanocomposites samples were prepared with good dispersion of layered silicate using power ultrasonic method in the particles. As structural analysis, the interlayer spacing have decreased with filled nanoparticles contents increase using power ultrasonic dispersion. The maximum increase interlayered spacing was observed to decease for above 5wt% clay loading. The other hand, as decrease with concentration filler of the layered silicate were increased dispersion degree of nanoparticles in the matrix. The interesting dielectric properties for epoxy based nanocomposites systems are attributed to the large volume fraction of interfacesin the bulk of the material and the ensuring interactions between the charged nanoparticle surface and the epoxy chains.

Evaluation of dispersion degree of nanoparticles in TiO2/epoxy resin nanocomposites

  • Nam, Ki-Woo;Moon, Chang-Kwon
    • 한국해양공학회지
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    • 제28권4호
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    • pp.338-344
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    • 2014
  • The purpose of this study was to evaluate the dispersion degree of particles using a nanoindentation test for titanium oxide nanoparticles/epoxy resin nanocomposites. Thus, the effects of the particle size and weight fraction, dispersion agent, and position of the sample on the modulus and degree of particle dispersion in the nanocomposites were investigated. As a result, the dispersion degree of large particles was found to be better than that of smaller particles in composites. It could be found that the aggregation or agglomeration of small particles with large surface energy occurred more easily in nanocomposites because of the large specific surface area. The moduli of the upper side of the film-shaped sample obtained from a nanoindentation test were low scattering, while the values for the bottom side were high scattering. Thus, the dispersion situation of the nanoparticles on the upper side of film-shaped samples could be considered to be better than that for the bottom side. This could be concluded due to the non-uniform nanoparticle dispersion in the same sample. The modulus obtained from nanoindentation test increased slightly with the content of nanoparticles and increased with the indented depth for the same sample. The latter is presumably due to the increase in the accumulated particles facing the indenter with the indented depth. The nanoindentation test was found to be a useful method to evaluate the dispersion status of nanoparticles in nanocomposites.

Preparation and characterization of expanded graphite/Ag nanoparticle composites for the improvement of thermal diffusion

  • Hong, Seok Hwan;Lee, Won Gyu
    • Korean Chemical Engineering Research
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    • 제56권3호
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    • pp.410-415
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    • 2018
  • Expanded graphite (EG)/Ag nanoparticle composites were synthesized by the chemical reduction of Ag ions, followed by the addition of expanded graphite into an Ag reducing solution. The prepared composites showed uniform dispersion of Ag nanoparticles on the surface of expanded graphite and exhibited relatively higher thermal conductivities than those of pure expanded graphite. In the case of 10% Ag content in the composite, the thermal conductivity in the thickness direction was 78% higher than the pure expanded graphite. We suggest that EG/Ag nanoparticle composites are a strong candidate for advanced heat spreading material.

Dispersion of Alloy 625 Nanoparticles in Ethanol

  • Lee, Eun-Hee;Lee, Min-Ku;Rhee, Chang-Kyu
    • 한국분말야금학회:학술대회논문집
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    • 한국분말야금학회 2006년도 Extended Abstracts of 2006 POWDER METALLURGY World Congress Part 1
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    • pp.673-674
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    • 2006
  • The influence of several experimental parameters on the formation of stable Alloy 625 nanoparticles dispersion in ethanol was investigated. Several analyzing methods were applied, like transmission profiles measured by Turbiscan, transmission electron microscopy, X-ray diffraction, gas chromatography, and particle size analyzer. The correlation among the increase of particle sizes, caused by nanoparticle coalescence and collision, concentration of dispersant and time was presented and discussed. The optimum conditions for the formation of stable dispersion are evaluated.

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Uniform PMMA-CH3NH3PbBr3 Nanoparticle Composite Film for Optoelectronic Application

  • Kirakosyan, Artavazd;Yun, Seokjin;Choi, Jihoon
    • 한국재료학회지
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    • 제27권6호
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    • pp.307-311
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    • 2017
  • Organometal halide perovskite materials, due to the tunability of their electronic and optical properties by control of composition and structure, have taken a position of significant importance in optoelectronic applications such as photovoltaic and lighting devices. Despite numerous studies on the structure - property relationship, however, practical application of these materials in electronic and optical devices is still limited by their processability during fabrication. Achieving nano-sized perovskite particles embedded in a polymer matrix with high loading density and outstanding photoluminescence performance is challenging. Here, we demonstrate that the careful control of nanoparticle formation and growth in the presence of poly(methyl methacrylate) results in perovskite nanoparticle - polymer nanocomposites with very good dispersion and photoluminescence. Furthermore, this approach is found to prevent further growth of perovskite nanoparticles, and thus results in a more uniform film, which enables fabrication using the perovskite nanoparticles.

불소화 에틸렌 프로필렌 나노 입자 분산액을 이용한 3차원 다층 미세유체 채널 제작 (Fabrication of 3D Multilayered Microfluidic Channel Using Fluorinated Ethylene Propylene Nanoparticle Dispersion)

  • 민경익
    • Korean Chemical Engineering Research
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    • 제59권4호
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    • pp.639-643
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    • 2021
  • 본 연구에서는 3차원 다층 미세유체 디바이스를 제작하기 위한 접착제로서 불소화 에틸렌 프로필렌(fluorinated ethylene propylene, FEP) 나노입자를 연구하였다. FEP 분산 용액을 1500 rpm에서 30초 동안 단순 스핀 코팅하여 기판에 3 ㎛ 두께의 균일하게 분포된 FEP 나노 입자 층을 형성하였다. FEP 나노입자는 300 ℃에서 1시간 동안 열처리 후 소수성 박막으로 변형되었으며, FEP 나노입자를 이용하여 제작된 폴리이미드 필름 기반 미세유체 디바이스는 최대 2250 psi의 압력을 견디는 것을 확인하였다. 마지막으로 기존의 포토리소그래피로 제작하기 어려운 16개의 마이크로 반응기로 구성된 3차원 다층 미세유체 디바이스를 FEP가 코팅된 9개의 폴리이미드 필름을 간단한 1단계 정렬로 성공적으로 구현하였다. 개발된 3차원 다층 미세유체 디바이스는 화학 및 생물학의 다양한 응용을 위한 고속대량 스크리닝, 대량 생산, 병렬화 및 대규모 미세유체 통합과 같은 강력한 도구가 될 가능성이 있습니다.

고갈 가스전에서 CO2 주입성 및 저장성 향상을 위한 알루미나 나노입자의 분산 특성 연구 (A Study on Alumina Nanoparticle Dispersion for Improving Injectivity and Storativity of CO2 in Depleted Gas Reservoirs)

  • 조성학;송차영;이정환
    • 한국가스학회지
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    • 제27권1호
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    • pp.23-32
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    • 2023
  • 본 연구에서는 고갈된 가스전의 사암 저류층 또는 심부 대염수층 내 이산화탄소(CO2) 주입효율 및 저장용량 증진을 위한 주입 첨가제로써 Al2O3 나노유체를 합성하였다. 기반 유체로 탈이온수(deionized water, DIW)와 API Brine의 조성을 참고하여 제조한 염수를 사용하였으며, 양이온성 계면활성제인 CTAB (cetyltrimethyl-ammonium bromide)을 첨가한 Al2O3 나노유체를 이용하여 유체를 합성하였다. 육안관찰, 동적광산란광도계(dynamic light scattering, DLS), 전자투과현미경(transmission electron microscope, TEM), 혼화성 시험(miscibility test)의 방법을 활용한 유체의 분산 안정성 평가 결과, 나노입자 농도가 0.05 wt% 이하 조건에서 70,000 ppm의 염수와 반응 후에도 응집 및 침전되지 않는 안정한 유체를 합성할 수 있음을 확인하였다.