• 제목/요약/키워드: Nano-processing

검색결과 551건 처리시간 0.028초

유리렌즈 성형용 금형의 ta-C 보호 필름 제조에 관한 연구 (Processing of ta-C Protective Films on Mold for Glass Lens)

  • 오승근;김영만
    • 한국표면공학회지
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    • 제44권5호
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    • pp.213-219
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    • 2011
  • Recently aspheric lenses are widely used for superpricision optical instruments, such as cellular phone camera modules, digital cameras and optical communication modules. The aspherical lenses are processed using mold core under high temperature compressive forming pressure. It is imperative to develop superhard protective films for the life extension of lens forming mold core. Especially ta-C films with higher $sp^3$ fractions receive attentions for the life extension of lens forming mold and, in turn, the cost reduction of lenses due to their suprior high temperature stability, high hardness and smooth surfaces. In this study ta-C films were processed on WC mold as a function of substrate bias voltage using FVA (Filtered Vacuum Arc) method. The processed films were characterized by Raman spectroscopy and nano-indentation to investigate bonding nature and hardness, respectively. The film with maximun 87% of $sp^3$ fraction was obtained at the substrate bias voltage of -60 V, which was closest to ta-C film. ta-C films showed better high temperature stability by sustaining relatively high fraction of $sp^3$ bonding even after 2,000 glass lens forming applications.

Glycothermal법을 이용한 나노 사이즈 BaTiO3분말의 제조 (Preparation of Nano-size BaTiO3 Powders Using Glycothermal Method)

  • 김병규;임대영;노준석;조승범
    • 한국세라믹학회지
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    • 제39권7호
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    • pp.642-648
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    • 2002
  • 본 연구에서는 TiCl$_4$를 가수분해 시켜 제조한 비정질의 titanium hydrous gel과 Ba(OH)$_2$.8$H_2O$를 출발물질로 사용하였으며, 반응용매로써 1,4-butanediol과 distilled water를 이용하여 나노 사이즈 BaTiO$_3$분말을 제조하였다. 용매로써 사용된 1,4-butanediol과 distilled water의 부피비에 따라 입자의 크기를 조절할 수 있으며, 습식화학법의 단점이었던 분말의 응집을 최소화 시킬 수 있다. 그리고 22$0^{\circ}C$의 비교적 낮은 반응온도에서 분산성이 우수하고, 입도분포가 좁은 약 50~200nm의 barium titanate 나노 분말을 제조하였다.

Development of Poly(methyl methacrylate)-Clay Nanocomposites by Using Power Ultrasonic Wave

  • Ryu, Joung Gul;Lee, Jae Wook;Kim, Hyungsu
    • Macromolecular Research
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    • 제10권4호
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    • pp.187-193
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    • 2002
  • Several methods have been used to synthesize polymer-clay nanocomposites. In-situ polymerization with clay belongs to a classical way to develop nano-structured materials, while melt intercalation is being recognized as another useful approach due to its versatility and environmentally benign character. In this research, we prepared polymer-clay nanocomposites based on the poly (methyl methacrylate) and organically modified montmorillonite via two-stage sonication process. According to the unique mode of power ultrasonic wave, the sonication during processing led to enhanced breakup of the clay agglomerates and reduction in size of the dispersed phase. Optimum conditions to form stable exfoliated nanocomposites were studied for various compositions and conditions. It was found that a novel attempt carried out in this study yielded further improvement in the mechanical performance of the nanocomposites compared to those produced by the conventional melt mixing process, as revealed by DMA, XRD and TEM. And rheological properties of nanocomposites were measured by ARES. As a result, sonicated PMMA-clay nanocomposites exhibits enhanced properties such as storage modulus and thermal stability than that of neat PMMA.

미세유체 바이오칩을 이용한 DNA 마이크로어레이 Hybridization 향상 (Enhancement of DNA Microarray Hybridization using Microfluidic Biochip)

  • 이현호;김용상
    • KSBB Journal
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    • 제22권6호
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    • pp.387-392
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    • 2007
  • DNA 마이크로어레이는 바이오칩의 발전에서 가장 주목받으며 발전하고 있는 분야로서 이에 대한 연구가 점차 확장하고 있다. DNA나 RNA 등 유전자의 매우 느린 확산속도를 극복하기 위하여 마이크로플루딕 바이오칩이 DNA 마이크로어레이에 적용되는 최근의 학술적인 사례들을 연구, 비교하였다. DNA 마이크로어레이에 적용된 미세유체 바이오칩은 상당수가 효율적인 hybridization을 달성하기 위한 믹싱 시스템이 많이 보고되었으며, 이 총설에서는 그에 대한 분석을 수행하여 유전자 hybridization 강화를 이룬 시스템에 대한 최근 동향을 가늠할 수 있게 하였다. 특별히 PDMS를 이용한 마이크로 펌프의 적용 등, 앞으로의 미세유체 DNA 마이크로어레이 발전가능성과 모델링의 한계점 등을 정리 분석해 보았다.

Synthesis and characterization of polyamide thin-film nanocomposite membrane containing ZnO nanoparticles

  • AL-Hobaib, A.S.;El Ghoul, Jaber;El Mir, Lassaad
    • Membrane and Water Treatment
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    • 제6권4호
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    • pp.309-321
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    • 2015
  • We report in this study the synthesis of mixed matrix reverse osmosis membranes by interfacial polymerization (IP) of thin film nanocomposite (TFNC) on porous polysulfone supports (PS). This paper investigates the synthesis of ZnO nanoparticles (NPs) using the sol-gel processing technique and evaluates the performance of mixed matrix membranes reached by these aerogel NPs. Aqueous m-phenyl diamine (MPD) and organic trimesoyl chloride (TMC)-NPs mixture solutions were used in the IP process. The reaction of MPD and TMC at the interface of PS substrates resulted in the formation of the thin film composite (TFC). NPs of ZnO with a size of about 25 nm were used for the fabrication of the TFNC membranes. These membranes were characterized and evaluated in comparison with neat TFC ones. Their performances were evaluated based on the water permeability and salt rejection. Experimental results indicated that the NPs improved membrane performance under optimal concentration of NPs. By changing the content of the filler, better hydrophilicity was obtained; the contact angle was decreased from $74^{\circ}$ to $32^{\circ}$. Also, the permeate water flux was increased from 26 to 49 L/m2.h when the content of NPs is 0.1 (wt.%) with the maintaining of lower salt passage of 1%.

Application of a Dynamic-Nanoindentation Method to Analyze the Local Structure of an Fe-18 at.% Gd Cast Alloy

  • Choi, Yong;Baik, Youl;Moon, Byung M.;Sohn, Dong-Seong
    • Nuclear Engineering and Technology
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    • 제49권3호
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    • pp.576-580
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    • 2017
  • A dynamic nanoindentation method was applied to study an Fe-18 at.% Gd alloy as a neutron-absorbing material prepared by vacuum arc-melting and cast in a mold. The Fe-18 at.% Gd cast alloy had a microstructure with matrix phases and an Fe-rich primary dendrite of $Fe_9Gd$. Rietveld refinement of the X-ray spectra showed that the Fe-18 at.% Gd cast alloy consisted of 35.84 at.% $Fe_3Gd$, 6.58 at.% $Fe_5Gd$, 16.22 at.% $Fe_9Gd$, 1.87 at.% $Fe_2Gd$, and 39.49 at.% ${\beta}-Fe_{17}Gd_2$. The average nanohardness of the primary dendrite phase and the matrix phases were 8.7 GPa and 9.3 GPa, respectively. The fatigue limit of the matrix phase was approximately 37% higher than that of the primary dendrite phase. The dynamic nanoindentation method is useful for identifying local phases and for analyzing local mechanical properties.

폐수처리를 위한 제올라이트 막의 최근 연구에 대한 총설 (Recent Progress in Zeolite Membrane for Wastewater Treatment: A Review)

  • 이주엽;라즈쿠마 파텔
    • 멤브레인
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    • 제32권4호
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    • pp.227-234
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    • 2022
  • 폐수는 석유 정제 산업에서만 방출되는 것이 아니고 아니라 가죽, 섬유, 페인트, 목재, 염료 가공 산업에서 또한 방출된다. 이런 산업 폐수는 중금속과 질소화합물 등 수질오염물질을 포함하고 있으며 화학적 산소요구량(COD)이 높다. 안전한 처리를 위해 폐수에서 각종 오염물질을 걸러내는 방식이 있지만 막 기반 기술은 고효율, 저비용으로 가장 효율적인 방법 중 하나이다. 다양한 막 중에서, 제올라이트 막은 가성비로 주목을 받고 있으며 많은 연구를 거쳤다. 본 리뷰논문은 i) 폐수처리, ii) 미세여과막, iii) 중공사막, iv) 초여과막의 순서로 폐수처리를 위한 제올라이트 막의 최근 진척을 중점으로 다루고 있다.

초전도 자속고정 특성 향상을 위한 $ZrO_2$ 나노점의 형성 연구 (Formation of $ZrO_2$ nanodots for the enhanced flux pinning properties in high $T_c$ superconducting films)

  • 정국채;유재무;김영국;이혜문
    • 한국초전도ㆍ저온공학회논문지
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    • 제10권1호
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    • pp.15-18
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    • 2008
  • To achieve high transport current without degradation under magnetic field, it is essential to artificially generate the pinning sites at which moving magnetic flux can be pinned. In this work, $ZrO_2$ nanodots were formed on the substrate surface using electro-spray deposition method. On top of the nanodots, the extended and effective pinning centers can be created. The positively charged Zr precursor solution was sprayed out from the needle using the corona discharge phenomena. Then, the sprayed precursor was deposited onto the negatively charged substrate surface followed by the heat treatment under the controlled atmosphere. Using the electrostatic force among the charged particles of precursor, evenly distributed and nano-sized dots were formed on the substrate surface. The size and density of the nanodots were studied by Atomic Force Microscopy. Also discussed are the effect of the deposition time and solution concentration on the size and density of the nanodot and processing variables in electro-spray method for the effective flux pinning centers in the superconducting films.

얼굴 영상 기반의 심박수 추정을 위한 딥러닝 모델의 경량화 기법 (Lightweight Deep Learning Model for Heart Rate Estimation from Facial Videos)

  • 황규태;박명근;이상준
    • 대한임베디드공학회논문지
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    • 제18권2호
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    • pp.51-58
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    • 2023
  • This paper proposes a deep learning method for estimating the heart rate from facial videos. Our proposed method estimates remote photoplethysmography (rPPG) signals to predict the heart rate. Although there have been proposed several methods for estimating rPPG signals, most previous methods can not be utilized in low-power single board computers due to their computational complexity. To address this problem, we construct a lightweight student model and employ a knowledge distillation technique to reduce the performance degradation of a deeper network model. The teacher model consists of 795k parameters, whereas the student model only contains 24k parameters, and therefore, the inference time was reduced with the factor of 10. By distilling the knowledge of the intermediate feature maps of the teacher model, we improved the accuracy of the student model for estimating the heart rate. Experiments were conducted on the UBFC-rPPG dataset to demonstrate the effectiveness of the proposed method. Moreover, we collected our own dataset to verify the accuracy and processing time of the proposed method on a real-world dataset. Experimental results on a NVIDIA Jetson Nano board demonstrate that our proposed method can infer the heart rate in real time with the mean absolute error of 2.5183 bpm.

자동차 바디용 알루미늄 도어 힌지 페이스 부품의 프레스 성형 최적화에 관한 연구 (A Study on the Optimization of Press Forming of Aluminum Door Hinge Face Parts in Automobiles)

  • 김석중;김민준;최원일;이춘규
    • Design & Manufacturing
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    • 제17권2호
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    • pp.47-54
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    • 2023
  • The research direction of the automobile industry worldwide is speeding up research to improve fuel efficiency through weight reduction as the weight of automobiles increases due to environmental problems, convenience demands, and safety problems. As a way to solve weight reduction, there is a method of improving mechanical properties by improving the development and manufacturing method of lightweight materials with replaceable mechanical properties. Therefore, research on the molding and processing technology of aluminum, which is a lightweight material, is being actively conducted. In this study, aluminum material was applied. By using Autoform S/W, a press forming analysis program, the blank holding force, mold die R, and bead restraint force were selected in three levels, respectively, and the results and optimization of formability and shape freezing were carried out. In this study, aluminum material was applied. By using Autoform S/W, a press molding analysis program, the blank holding force, mold die R, and bead restraint force were selected in three levels, respectively, and the results and optimization of formability and shape freezing were carried out. The optimized results were confirmed by comparative analysis of formability and Spring Back. As a result of the experiment, it was possible to confirm the result value of the Spring Back of the final product according to the tensile change of the material.