• Title/Summary/Keyword: Nano size

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Synthesis and Properties of Ultra-fine (Ti, M1, M2)(CN)-Ni Cermets

  • Kang, Young-Jae;Kang, Shin-Hoo
    • Proceedings of the Korean Powder Metallurgy Institute Conference
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    • 2006.09a
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    • pp.644-645
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    • 2006
  • TiC-and Ti(C,N)-based cermets are excellent in semi-and final finishing of work piece during cutting operations. Typical microstructure of the cermets is a core/rim structure. The undissolved Ti(C,N) cores contribute to their high hardness while the rim phases, (Ti,M1,M2)(C,N)-type solid solutions, play great roles in enhancing the toughness. In this paper, various ultrafine pre-mixed MeC-Ni powders were synthesized and the powders were sintered or hot pressed after mixing in order to control the size and volume fractions of core and rim phases in the system. This paper will present the factors determining the microstructure along with mechanical properties.

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Characteristics of Porous YAG Powders Fabricated by PVA Polymer Solution Technique

  • Lee, S.J.;Shin, P.W.;Kim, J.W.;Chun, S.Y.
    • Proceedings of the Korean Powder Metallurgy Institute Conference
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    • 2006.09a
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    • pp.438-439
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    • 2006
  • Pure and stable YAG $(Y_3Al_5O_{12})$ powders were synthesized by a PVA (polyvinyl alcohol) polymer solution technique. PVA was used as an organic carrier for the precursor ceramic gel. The precursor gels were crystallized to YAG at relatively a low temperature of $900\;^{\circ}C$. The synthesized powders, which have nano-sized primary particles, were soft and porous, and the porous powders were ground to sub-micron size by a simple ball milling process. The ball-milled powders were densified to 94% relative density at $1500\;^{\circ}C$ for 1h. In this study, the characteristics of the synthesized YAG powders were examined.

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Synthesis of Ultrafine Zr Based Alloy Powder by Plasma Arc Discharge Process

  • Lee, Gil-Geun;Park, Je-Shin;Kim, Won-Baek
    • Proceedings of the Korean Powder Metallurgy Institute Conference
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    • 2006.09a
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    • pp.420-421
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    • 2006
  • In the present study, ultrafined Zr-V-Fe based alloy powder prepared by a plasma arc discharge process with changing process parameters. The chemical composition of synthesized powder was strongly influenced by the process parameters, especially the hydrogen volume fraction in the powder synthesis atmosphere. The synthesized powder had an average particle size of 50 nm. The synthesized Zr-V-Fe based particles had a shell-core structure composed of metal in the core and oxidse in the shell.

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Fabrication of nanomaterials using an Anodic Aluminum Oxide(AAO) thin film and their properties (AAO template를 이용한 나노 구조의 제조와 특성)

  • Yu, Hyun-Min;Lee, Jae-Hyung;Lee, Jong-In;Jung, Hak-Ki;Jung, Dong-Su
    • Proceedings of the Korean Institute of Information and Commucation Sciences Conference
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    • 2010.05a
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    • pp.814-817
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    • 2010
  • AAO thin films prepared by a two-step anodization process have pores that are uniform in diameter, highly ordered, and perfectly vertical with respect to the plane of the nano template. Further, the pore size and interpore distance can be easily controlled by varying the anodizing voltage and acid electrolyte. When metals are electrochemically deposited in the pores, metal nanowires that are highly ordered and uniform in diameter are formed in each pore.

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Characterization of Poly-Si TFT's using Amorphous-$Si_xGe_y$ for Seed Layer (Amorphous-$Si_xGe_y$을 seed layer로 이용한 Poly-Si TFT의 특성)

  • Jung, Myung-Ho;Jung, Jong-Wan;Cho, Won-Ju
    • Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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    • 2007.06a
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    • pp.125-126
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    • 2007
  • Polycrystalline silicon thin-film-transistors (Poly-Si TFT's) with a amorphous-$Si_xGe_y$ seed layer have been fabricated to improve the performance of TFT. The dependence of crystal structure and electrical characteristics on the the Ge fractions in $Si_xGe_y$ seed layer were investigated. As a result, the increase of grain size and enhancement of electrical characteristics were obtained from the poly-Si TFT's with amorphous-SixGey seed layer.

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Selective Array of Polystyrene Beads by Using Nanometer-Scaled Hydrophilic Thin Film Patterning (나노미터 규격의 친수성 박막 패터닝을 이용한 선택적 폴리스티렌 입자 배열)

  • Kang, Jung-Hwa;Kim, Kyoung-Soeb;Kim, Nam-Hoon;Roh, Yong-Han
    • Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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    • 2007.11a
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    • pp.103-104
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    • 2007
  • Nanometer-scaled polymer beads, such as polystyrene beads, were used as nanometer fabrication materials due to their some advantages such as self-assembled monolayer, nanometer scaled size and excellent compatibility with silicon based devices. Thus, the investigation on these properties of polymer beads was required. It is difficult to control the array of polystyrene beads on silicon substrate. In this study, we investigated the condition of selective array of polystyrene beads on nanometer-scaled hydrophilic surface which was obtained by APS coating. A tilting method was used to array the polystyrene beads selectively on the substrate. The polystyrene beads could be arrayed selectively by this method. From these results, we verified that there are possibilities to fabricate unique tools for the nanometer-scaled electrical devices.

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Manufacturing Process condition and Electrical Characteristics of Bi Series Varistors with ZnO Powder Sizes (ZnO 분말 크기에 따른 Bi계 바리스터의 제조공정조건과 전기적 특성)

  • Jeong, Jong-Yub;Wang, Min-Sung;Kim, Kyoung-Min;Park, Choon-Bae
    • Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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    • 2005.07a
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    • pp.344-345
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    • 2005
  • The characteristics of varistors based on M.Matstuokas with one another ZnO powder (50nm, 100nm, 300nm) have been investigated. The optimum calcination and sintering temperature was also selected for each samples. Varieties of sintering conditions were found according to powder size. As the result of analysises on each operating voltages. We obtained the most high voltage in a sample with 50nm ZnO powder.

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Molecular Interfacial Control and Molecular Morphology Properties of Functionalized Dendrimer Organic Monolayers (기능성 덴드리머 유기단분자막의 분자계면제어 및 분자모폴로지 특성)

  • Shin, Hoon-Kyu;Kim, Doo-Seok
    • Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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    • 2007.06a
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    • pp.365-366
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    • 2007
  • The dendrimer has been well known as a promising macromolecules for a building the organized nanostructure, which of the size can be controlled and which of periphery can be terminated by various functionalities. Currently a variety of research is being carried out in the field of dendrimer / polymer characterization, nano-scale atomic manipulation, and supramolecular nanostructure analysis. We investigated monolayer behavior and its characteristics at the air-water interface by LB method. In this report, we will present the interfacial properties of dendrimer monolayers on various conditions such as the surface-pressure, barrier speed and spreading quantity.

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Preparation of $TiO_2$ Pure Nanoparticles by Vapor-Phase Hydrolysis (기상 가수분해에 의한 순수 $TiO_2$ 초미립자의 제조)

  • Lee, Soo-Keun
    • KOREAN JOURNAL OF PACKAGING SCIENCE & TECHNOLOGY
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    • v.9 no.1
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    • pp.11-18
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    • 2003
  • The pure $TiO_2$ particles have been prepared in vapor-phase hydrolysis of titanium tetraisopropoxide(TTIP). The rate of TTIP hydrolysis was so fast that the overall rate of formation of $TiO_2$ was controlled by the rate of mixing of TTIP and $H_2O$. Thus, the primary $TiO_2$ particles were prepared in nano sizes to form chainlike aggregates due to rapid coagulation. The pure $TiO_2$ particles as prepared were amorphous at the reactor set temperatures below $400^{\circ}C$ and became anatase at the temperatures of $450^{\circ}C$ above while the weak rutile peaks were also observed above $800^{\circ}C$. The actual size of primary particles as prepared were reduced by increasing the reactor set temperature while their crystalline sizes as well as BET sizes increased by post-sintering.

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Pulsed Electrochemical Deposition for 3D Micro Structuring

  • Park, Jung-Woo;Ryu, Shi-Hyoung;Chu, Chong-Nam
    • International Journal of Precision Engineering and Manufacturing
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    • v.6 no.4
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    • pp.49-54
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    • 2005
  • In this paper, micro structuring technique using localized electrochemical deposition (LECD) with ultra short pulses was investigated. Electric field in electrochemical cell was localized near the tool tip end region by applying pulses of a few hundreds of nano second duration, Pt-Ir tip was used as a counter electrode and copper was deposited on the copper substrate in mixed electrolyte of 0.5 M $CuSO_4$ and 0.5 M $H_2SO_4$, The effectiveness of this technique was verified by comparison with ECD using DC voltage. The deposition characteristics such as size, shape, surface, and structural density according to applied voltage and pulse duration were investigated. The proper condition was selected based on the results of the various experiments. Micro columns less than $10{\mu}m$ in diameter were fabricated using this technique. The real 3D micro structures such as micro spring and micro pattern were made by the presented method.