• Title/Summary/Keyword: Multi-probe method

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Preparation and characterization of nanoflake composite multi core-shell SrFe12O19/Fe3O4/PEG/PPy

  • Hosseini, Seyed Hossein;Majidpour diz, Mohammad
    • Advances in materials Research
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    • v.1 no.2
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    • pp.161-168
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    • 2012
  • Nanoflake composite multi core-shell $SrFe_{12}O_{19}/Fe_3O_4$/PEG/Polypyrrole was synthesized by in situ polymerization method. In this paper, the fabrication of $SrFe_{12}O_{19}$ nanoflake is as first core by solgel method. Then fabricated a shell layer from magnetic nanoparticles of $Fe_3O_4$, which synthesized by coprecipitation technique, onto the $SrFe_{12}O_{19}$ nanoflake. Polyethylene glycol (PEG) as a polymer layer and as second shell was coated onto the before core-shell. Than core-shell $SrFe_{12}O_{19}/Fe_3O_4$/PEG was used as template for the preparation of $SrFe_{12}O_{19}/Fe_3O_4$/PEG/Polypyrrole composite. Final composite has a conductive property among $4.23{\times}10^{-2}Scm^{-1}$ and magnetic property about $M_s$=2.99 emu/g. Also final composite in soluble at organic solvent such as DMF and DMSO and has a flake structure. Conductivity and magnetic property respectively determine by four-probe instrument and vibrant sample magnetometer (VSM), morphology and article size determined by FE-SEM, TEM and XRD.

Properties and Preparation of AlNO Multi-layer Thin Films Using DC Magnetron Sputter Method (직류 마그네트론 스퍼터법에 의한 AlNO 복층박막의 제조와 특성)

  • Kim, Hyun-Hoo;Oh, Dong-Hyun;Baek, Chan-Soo;Jang, Gun-Eik;Choi, Dong-Ho
    • Journal of the Korean Institute of Electrical and Electronic Material Engineers
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    • v.27 no.9
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    • pp.589-593
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    • 2014
  • AlNO multi-layer thin films on aluminum substrates were prepared by DC reactive magnetron sputtering method. $Al_2O_3$/AlNO(LMVF)/AlNO(HMVF)/Al/substrate of 4 multi-layer has been prepared in an Ar and ($N_2+O_2$) gas mixture, and $Al_2O_3$ of top layer is anti-reflection layer on double AlNO(LMVF)/AlNO(HMVF) layers and Al metal of infrared reflection layer. In this study, the roughness and surface properties of AlNO thin films were estimated by field emission scanning electron microscopy(FE-SEM). The grain size of AlNO thin films increased with increasing sputtering power. The composition of thin films has been systematically investigated using electron probe microanalysis(EPMA). The optical properties with wavelength spectrum were recorded by UV-Vis-NIR spectrophotometry at a range of 200~1,500 nm. The absorptance of AlNO films shows the increasing trend with swelling ($N_2+O_2$) gas mixture in HMVF and LMVF deposition. The excellent optical performance showed above 98% of absorptance in visible wavelength region.

Flux Loss and Neutron Diffraction Measurement Ag-sheathed Bi-2223 Tapes in terms of Flux Creep

  • Jang Mi-Hye
    • KIEE International Transactions on Electrophysics and Applications
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    • v.5C no.5
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    • pp.204-210
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    • 2005
  • Alternating current (AC) losses of two Bi-2223 ([Bi, Pb]: Sr: Ca: Cu: O = 2:2:2:3) tapes [(Tape I, un-twist-pitch) and the other with a twist-pitch of 10 mm (Tape II)] were measured and compared. These samples, produced by the powder-in-(Ag) tube (PIT) method, are multi-filamentary. Also, it's produced by non-twist and different twist pitch (8, 10, 13, 30, 50 and 70 mm). The critical current measurement was carried out under the environment in liquid Nitrogen and in zero-field by 4-probe method. Susceptibility measurements were conducted while cooling in a magnetic field. Flux loss measurements were conducted as a function of ramping rate, frequency and field direction. The AC flux loss increases as the twist-pitch of the tapes decreased, in agreement with the Norris Equation. Neutron-diffraction measurements have been carried out investigate the crystal structure, magnetic structures, and magnetic phase transitions in Bi-2223([Bi, Pb]:Sr:Ca:Cu:O)

A study on correlation between frictional coefficients and subjective evaluation while rubbing cosmetic product on skin (화장품을 바를 때 피부 마찰계수의 변화와 주관적인 평가와의 상관관계 연구)

  • Kwon Young-Ha;Kwon Hyun-Joon;Rang Moon-Jeong;Lee Su-Min
    • Science of Emotion and Sensibility
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    • v.8 no.4
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    • pp.385-391
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    • 2005
  • A frictional coefficients of in-vivo skin characteristic is the most important factor of the cutaneous mechanical properties ant the method of evaluating skin care in the fields of cosmetics products. In-vivo skin characteristic varies in many different ways depends on what is applied to the skin, loading condition, shape, surface roughness, and material of the probe. In this research, we designed a system which can be measured frictional coefficients of a human skin on real time. It consists of multi-components load-cell, actuator, linear motor and arm fixator. This measurement system was automatically controlled by computer. We measured frictional coefficients between probe an4 skin using this system ant inquired adjectives for subjective evaluation while rubbing cosmetic product on skin. Lastly, we analyzed correlation between two factors by calculating Pearson Correlation Coefficient. As a result, we could know that frictional coefficients varied from 0.17-1.2 according to cosmetic products, normal forte, materials and surface conditions of probe. We also confirmed sensual feelings of cosmetic products have close correlation with frictional coefficients.

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Characterization of various crystal planes of beta-phase gallium oxide single crystal grown by the EFG method using multi-slit structure (다중 슬릿 구조를 이용한 EFG 법으로 성장시킨 β-Ga2O3 단결정의 다양한 결정면에 따른 특성 분석)

  • Hui-Yeon Jang;Su-Min Choi;Mi-Seon Park;Gwang-Hee Jung;Jin-Ki Kang;Tae-Kyung Lee;Hyoung-Jae Kim;Won-Jae Lee
    • Journal of the Korean Crystal Growth and Crystal Technology
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    • v.34 no.1
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    • pp.1-7
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    • 2024
  • β-Ga2O3 is a material with a wide band gap of ~4.8 eV and a high breakdown-voltage of 8 MV/cm, and is attracting much attention in the field of power device applications. In addition, compared to representative WBG semiconductor materials such as SiC, GaN and Diamond, it has the advantage of enabling single crystal growth with high growth rate and low manufacturing cost [1-4]. In this study, we succeeded in growing a 10 mm thick β-Ga2O3 single crystal doped with 0.3 mol% SnO2 through the EFG (Edge-defined Film-fed Growth) method using multi-slit structure. The growth direction and growth plane were set to [010]/(010), respectively, and the growth speed was about 12 mm/h. The grown β-Ga2O3 single crystal was cut into various crystal planes (010, 001, 100, ${\bar{2}}01$) and surface processed. The processed samples were compared for characteristics according to crystal plane through analysis such as XRD, UV/VIS/NIR/Spec., Mercury Probe, AFM and Etching. This research is expected to contribute to the development of power semiconductor technology in high-voltage and high-temperature applications, and selecting a substrate with better characteristics will play an important role in improving device performance and reliability.

Characteristic Analysis and Preparation of Multi-layer TiNOx Thin Films for Solar-thermal Absorber (태양열 흡수판용 복층 TiNOx 박막의 제조와 특성 분석)

  • Oh, Dong-Hyun;Han, Sang-Uk;Kim, Hyun-Hoo;Jang, Gun-Eik;Lee, Yong-Jun
    • Journal of the Korean Institute of Electrical and Electronic Material Engineers
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    • v.27 no.12
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    • pp.820-824
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    • 2014
  • TiNOx multi-layer thin films on aluminum substrates were prepared by DC reactive magnetron sputtering method. 4 multi-layers of $TiO_2$/TiNOx(LMVF)/TiNOx(HMVF)/Ti/substrate have been prepared with ratio of Ar and ($N_2+O_2$) gas mixture. $TiO_2$ of top layer is anti-reflection layer on double TiNOx(LMVF)/TiNOx(HMVF) layers and Ti metal of infrared reflection layer. In this study, the crystallinity and surface properties of TiNOx thin films were estimated by X-ray diffraction(XRD) and field emission scanning electron microscopy(FE-SEM), respectively. The grain size of TiNOx thin films shows to increase with increasing sputtering power. The composition of thin films has been investigated using electron probe microanalysis(EPMA). The optical properties with wavelength spectrum were recorded by UV-Vis-NIR spectrophotometry at a range of 200~1,500 nm. The TiNOx multi-layer films show the excellent optical performance beyond 9% of reflectance in those ranges wavelength.

High throughput automated 96-well solid-phase extraction and liquid chromatography-tandem mass spectrometric analysis of beraprost in human plasma

  • Chang, Kyu-Young;Kim, Ho-Hyun;Lee, Hee-Joo;Lee, Kyung-Ryul
    • Proceedings of the PSK Conference
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    • 2003.10b
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    • pp.224.1-224.1
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    • 2003
  • A sensitive and selective liquid chromatographic method coupled with tandem mass spectrometry (LC-MS/MS) was developed for the determination of beraprost in human plasma. Plasma samples were transferred into 96-well OASIS HLB extraction plate using an automated sample handling system and the drugs were eluted with methanol. The eluents were then evaporated and reconstituted with water. All sample transfer and solid-phase extraction (SPE) was automated through the application of both the PerkinElmer MultiPROBE II HT and TOMTEC Quadra 96 workstation. (omitted)

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Exonic copy number variations in rare genetic disorders

  • Man Jin Kim
    • Journal of Genetic Medicine
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    • v.20 no.2
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    • pp.46-51
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    • 2023
  • Exonic copy number variation (CNV), involving deletions and duplications at the gene's exon level, presents challenges in detection due to their variable impact on gene function. The study delves into the complexities of identifying large CNVs and investigates less familiar but recurrent exonic CNVs, notably enriched in East Asian populations. Examining specific cases like DRC1, STX16, LAMA2, and CFTR highlights the clinical implications and prevalence of exonic CNVs in diverse populations. The review addresses diagnostic challenges, particularly for single exon alterations, advocating for a strategic, multi-method approach. Diagnostic methods, including multiplex ligation-dependent probe amplification, droplet digital PCR, and CNV screening using next-generation sequencing data, are discussed, with whole genome sequencing emerging as a powerful tool. The study underscores the crucial role of ethnic considerations in understanding specific CNV prevalence and ongoing efforts to unravel subtle variations. The ultimate goal is to advance rare disease diagnosis and treatment through ethnically-specific therapeutic interventions.

Evaluation of Thermal Response Test of Energy Pile (에너지 파일의 현장 열응답 시험에 관한 연구)

  • Yoon, Seok;Lee, Seung-Rae;Kim, Min-Jun;Go, Gyu-Hyun
    • Journal of the Korean Geotechnical Society
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    • v.30 no.4
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    • pp.93-99
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    • 2014
  • Use of geothermal energy has been increased for its economical application and environmentally friendly utilization. Particularly, for energy piles, a spiral coil type ground heat exchanger (GHE) is more preferred than line type GHEs such as U and W shaped GHEs. A PHC energy pile with spiral coil type GHE was installed in an area of partially saturated dredged soil deposit, and a thermal response test (TRT) was conducted for 240 hours under a continuous operation condition. Besides, remolded soil samples from different layers were collected in the field, and soil specimens were reconstructed according to the field ground condition. Non-steady state probe methods were conducted in the lab, and ground thermal conductivity and thermal diffusivity were measured for the different soil layers. An equivalent ground thermal conductivity was calculated from the lab test results and it was compared with the field TRT result. The difference was less than 5%, which advocates the use of an equivalent ground thermal conductivity for the multi-layered ground. Furthermore, this paper also represents an equivalent ground thermal diffusivity evaluation method which is another very important design parameter.

Electrocardiogram-Gated Multi-Angle Doppler Optical Coherence Tomography (심전도 게이트를 사용한 다관점 도플러 광 단층촬영법)

  • Ahn, Yeh-Chan
    • Transactions of the Korean Society of Mechanical Engineers B
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    • v.35 no.7
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    • pp.685-691
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    • 2011
  • The aim of this study is to point out the uniqueness of Doppler optical coherence tomography (DOCT) for use in a probe station for (in vivo) visualization of microscale flow and structure and to maximize the effectiveness of DOCT by overcoming its limitations. Conventional DOCT produces images of only one of the velocity components that is parallel to the incident light. In this study, a multi-angle DOCT to quantify a velocity vector field is proposed; this is an extension from a velocity scalar field to a vector field. Quantifying an instantaneous three-dimensional velocity field in a pulsating flow is another challenge because of its limited frame rate. The in-vivo pulsating blood flow is measured by using an electrocardiogram-gated multi-angle DOCT in a hamster cheek pouch model. It is shown that the aliasing problem caused by a relatively low frame rate is resolved by using this method of measurement.