• Title/Summary/Keyword: Mixed-size particles

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Determination of the Synthetic Time and the Transport Pattern of Vicilin and Legumin in Ginseng Endosperm Cell Using Double Immunogold Labeling (이중 면역금입자 표지법을 이용한 인삼 배유세포내 Vicilin과 Legumin의 합성시기 및 수송방식)

  • Lee, Chang-Seob;Yu, Seong-Cheol;Kim, Woo-Kap
    • Journal of Ginseng Research
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    • v.19 no.3
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    • pp.267-274
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    • 1995
  • Vicilin and legumin, the storage Proteins of seed, were Purified from ginseng (Panax ginseng C.A. Meyer) endosperm cells. They were immunized in rabbits, and antibodies were raised respectively. Using these two antibodies, double immunogold labeling of vicilin and legumin was carried out to determine the gap of synthetic time and the transport pattern of vicilin and legumin in the ginseng endosperm cells. Vicilin and legumin were synthesized at the same time at early embryo developmental stage. They were secreted from the Golgi bodies and accumulated into the small vacuoles. As the endosperm cells developed, vicilin and legumin localized in the small vacuoles were gradually transported toward the large central vacuole where they were stored. Protein bodies were derived from the vacuoles filled with proteins and distributed in the endosperm cells of mature red seed. Protein bodies were various in size from 1 to 8 ${\mu}{\textrm}{m}$ in which vicilin and legumin were mixed each other. The number of small particles labeled on the vicilin was greater than that of large particles labeled on the legumin in the protein bodies indicating that the amount of vicilin is higher than that of legumin in the protein bodies.

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Formation of Solid Solution and Microstructure in Processureless sintered SiC-AlN Composite (상압소결에 의하여 제조된 SiC-AlN 복합체에서의 고용체 형성과 미세구조)

  • Lee, Jong-Kook;Kim, Duk-Jun;Kim, Hwan
    • Journal of the Korean Ceramic Society
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    • v.33 no.7
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    • pp.785-792
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    • 1996
  • Formation of Solid Solution and Microstructure in Processureless sintered SiC-AlN compo-site using oxides as a sintering aid at 185$0^{\circ}C$ and 195$0^{\circ}C$ Regardless of SiC/AlN ratio in composition most of sintered specimens showed he complex structure mixed with 2H solid solution and SiC particles. High sintering temperature and large AlN content in starting composition enhanced the formation of 2H solid solution in sintered specimen 2H solid solution showed the spherical shape and core-rim structure. AlN content in the core is higher than that in the rim but SiC content . The size of 2H solid solution on fracture showed the transgranular fracture mode compared with the dispersed SiC particles which showed the intergranular fracture mode.

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Experimental study on the sediment sorting processes of the bed surface by geomorphic changes in the vegetated channels (실내실험에 의한 혼합사 식생하도의 지형변화와 하상토 분급 특성 연구)

  • Jang, Chang-Lae
    • Journal of Korea Water Resources Association
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    • v.49 no.1
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    • pp.73-81
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    • 2016
  • This study investigates the development of lower channels and sediment sorting processes in the vegetated channels with the mixed sediment. The sediment discharges fluctuate with time and decrease with vegetation density. The bed changes with irregular patterns, and the sediment particles in the vegetated zone at the surface of bed are fine. The dimensionless geometric mean decreases with vegetation density. The fine sediment particles are trapped by vegetation, and the bed between main steam and vegetated zone increases. Moreover, the particle sizes are distributed irregularly near the zone. The hiding functions decrease with dimensionless particle size. However, the functions increase with vegetation density, which is confirmed by decreasing sediment discharge with vegetation. The lower channel is stable and the migration decreases in the condition of $0.5tems/cm^2$. However, the migration of the lower channel in the condition of $0.7stems/cm^2$ increases due to the increased sinuosity and new generated channels in the sedimentated vegetation zone.

Studies on Factors to Increase Mold Inhibitor Effectiveness in Livestock Rations II. Effects of the Usage of a Mold Inhibitor in the Ration on the Nutritional Status and Performance of Chicks (배합사료에 대한 항곰팡이제의 효과적인 처리 방법과 사료내 영양소 보전 방법 II. 항곰팡이제의 이용이 사료 영양소 보전 및 병아리 성장에 미치는 요인)

  • Nahm, Kee H.;Nahm, Kee S.
    • Korean Journal of Poultry Science
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    • v.15 no.4
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    • pp.269-275
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    • 1988
  • The effect of mold inhibitor was determined in the commercial rations which had two different protein levels(18% and 12% ) and two different particle sizes(80% of the particles in the ration less than 1.19mm and 40% of the particles in the ration less than 1.1mm). After 40 days storage of the rations treated and not treated with the mold inhibitor the nutritional change of the experimental diets with 18% and 12% protein levels, the growth performance of chicks, and the weight of internal organs fed the 18% protein diet were observed as the criteria of this research The fat level and carotene content in the two diets with 18% and 12% protein level each were significantly (P<0.05) decreased when the diets were not treated by the mold inhibitor. Even if mold inhibitor was mixed in the diet, the fat content in the diet which had 40% of the particles in the ration less than 1.19mm tended to be decreased, especially, in the diet with a 12% protein level. The carotene content in the diet treated with mold inhibitor which had 40% of the particles in the ration less than 1.19mm also tended to be decreased in both diets (18% protein and 12% protein). Feed types$\times$particle size interaction was significant for the fat content (P<0.05) and for the carotene content (P<0.05). The amount of crude protein and ADF was not significantly (P>0.05) changed after 40 days storage. There was a significant decrease (P<0.05) in total body weight gain and total feed intake observed in chicks fed the untreated diet with 40% of the particles in the ration less than 1.19mm. Feed conversion was significantly (P<0.05) depressed in the chicks fed the untreated diet of both particle sizes. Particle size$\times$types of feed interaction in feed conversion was significant (P<0.05). Relative sizes of the liver, pancreas and spleen were not affected significantly (P>0.05) by the treatments.

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The Effect of Uni-nanoadditive Manufactured Using RF Plasma Processing on Core-shell Structure in MLCC

  • Song, Soon-Mo;Kim, Hyo-Sub;Park, Kum-Jin;Sohn, Sung-Bum;Kim, Young-Tae;Hur, Kang-Heon
    • Journal of the Korean Ceramic Society
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    • v.46 no.2
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    • pp.131-136
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    • 2009
  • Radio frequency (RF) plasma treatment is studied for the size reduction and the spheroidization of coarse particles to change them into nano-sized powders of spherical shape in MLCC fields. The uni-nanoadditives manufactured by RF plasma processing for high dispersion have been investigated for the effect on core-shell structure in dielectrics of MLCC. Microstructures have been characterized using scanning electron microscope (SEM), transmission electron microscope (TEM) and Electron Probe Micro Analyzer (EPMA). We compared the distribution of core-shell grains between specimens manufactured using uni-nanoadditive and using mixed additive. In addition, the uniformity of rare earth elements in the core-shell structured grains was analyzed. It was shown, from TEM observations, that the sintered specimen manufactured using uni-nanoadditives had more dense small grains with well-developed core-shell structure than the specimen using mixed additives, which had a homogeneous microstructure without abnormal grain growth and shows broad temperature coefficient of capacitance (TCC) curves in all temperature ranges because of well dispersed additives.

Mechanical Properties of Denture Base Resin through Controlling of Particle Size and Molecular Weight of PMMA (폴리(메틸 메타아크릴레이트) 입자 크기 및 분자량 제어에 따른 의치상 재료로서의 기계적 물성 변화)

  • 양경모;정동준
    • Polymer(Korea)
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    • v.27 no.5
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    • pp.493-501
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    • 2003
  • Poly(methyl methacrylate) (PMMA) particles, denture base resin, were synthesized by suspension polymerization through control of polymerization conditions (stabilizer concentration, co-monomer concentration, and the agitation speed) and evaluated changes in molecular weight and particle size. We also investigated their mechanical properties of compression-molded samples which were from synthesized polymer powder mixed with methyl methacrylate (MMA) solution. under the condition of volumetric ratio as 2:1(PMMA powder and MMA solution). The results shows that the mechanical properties were mainly affected by particle size over 100 ${\mu}$m (in particle size) and by molecular weight under 100 ${\mu}$m (in particle size). From these results, we concluded that the most appropriate particle size of PMMA powder for heat-cured denture base resins is around 100 ${\mu}$m. and its molecular weight is around 300000 (M$\sub$n/).

Low temperature synthesis of $ZnWO_4$ nanopowders using polymeric complex precursor (착체중합법에 의한 $ZnWO_4$ 나노분말의 저온합성)

  • 류정호;임창성;오근호
    • Journal of the Korean Crystal Growth and Crystal Technology
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    • v.12 no.3
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    • pp.133-137
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    • 2002
  • $ZnWO_4$ nano-powders were successfully synthesized at low temperature by polymerized complex method using zinc acetate and tungstic acid as starting materials. The polymeric precursors were heat-treated at temperatures from 300 to $600^{\circ}C$ for 3 h. The precursors and heat-treated powders were evaluated for crystallization process, thermal decomposition, surface morphology and crystallite size. Crystallization of the $ZnWO_4$ powders were detected at $400^{\circ}C$ and entirely completed at a temperature of $600^{\circ}C$. The particles heat-treated at $400^{\circ}C$ showed primarily co-mixed morphology with spherical and silk-worm-like forms, while the particles heat-treated at $500^{\circ}C$ showed more homogeneous morphology. The average crystalline sizes were 17.62~24.71 nm showing an ordinary tendency to increase with the temperatures from 400 to $600^{\circ}C$.

A Study on the Wear Behavior of Tetrahedral Amorphous Carbon Coatings Based on Bending Angles of the Filtered Cathodic Vacuum Arc with Different Arc Discharge Currents (자장여과아크소스의 자장필터 꺾임 각도와 아크방전전류에 따라 증착된 ta-C 코팅의 마모 거동 연구)

  • Kim, Won-Seok;Kim, Songkil;Jang, Young-Jun;Kim, Jongkuk
    • Tribology and Lubricants
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    • v.38 no.3
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    • pp.101-108
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    • 2022
  • The structure and properties of tetrahedral amorphous carbon (ta-C) coatings depend on the main process parameters and bending angles of the magnetic field filter used in the filtered cathodic vacuum arc (FCVA). During the process, it is possible to effectively control the plasma flux of carbon ions incident on the substrate by controlling the arc discharge current, thereby influencing the mechanical properties of the coating film. Furthermore, we can control the size and amount of large particles mixed during carbon film formation while conforming with the bending angle of the mechanical filter mounted on the FCVA; therefore, it also influences the mechanical properties. In this study, we consider tribological characteristics for filtered bending angles of 45° and 90° as a function of arc discharge currents of 60 and 100 A, respectively. Experiment results indicate that the frictional behavior of the ta-C coating film is independent of the bending angle of the filter. However, its sliding wear behavior significantly changes according to the bending angle of the FCVA filter, unlike the effect of the discharge current. Further, upon changing the bending angle from 45° to 90°, abrasive wear gets accelerated, thereby changing the size and mixing amount of macro particles inside the coating film.

On Properties and Synthesis of Nanostructured W-Cu Alloys by Mechanical Alloying(I) (기계적합금화 방법에 의한 Nanostructured W-Cu 합금의 제조 및 물성연구(I))

  • 김진천
    • Journal of Powder Materials
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    • v.4 no.2
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    • pp.122-132
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    • 1997
  • Nanostructured(NS) W-Cu composite powders of about 20~30 nm grain size were synthesized by mechanical alloying. The properties of NS W-Cu powder and its sintering behavior were investigated. It was shown from X-ray diffraction and TEM analysis that the supersaturated solid solution of Cu in W was not formed by the mechanical alloying of mixed elemental powders, but the mixture of W and Cu particles with nanosize grains, i.e., the nanocomposite powder was attained. Nanocomposite W-20wt%Cu and W-30wt%Cu powders milled for 100 h were sintered to the relative density more than 96% and 98%, respectively, by sintering at 110$0^{\circ}C$ for 1 h in $H_2$. Such a high sinterability was attributed to the high homogeneous mixing and ultra-fine structure of W and Cu phases as well as activated sintering effect by impurity metal introduced during milling.

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A Study on the Preparation of $Al_2O_3-TiO_2$ Nanocomposite Powders ($Al_2O_3-TiO_2$계 Nanocomposite 분체의 합성에 관한 연구)

  • 이홍림;이호순
    • Journal of the Korean Ceramic Society
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    • v.30 no.2
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    • pp.115-122
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    • 1993
  • Transparent Al2O3 and TiO2 clear sols prepared by hydrolysis and subsequent peptization were mixed into wet gel. EDS analysis for this gel showed that wet gel was extremely homogeneous in chemical composition. Calcination of the wet gel at 120$0^{\circ}C$ for 50 minutes resulted in Al2O3-TiO2 nanocomposite powders where TiO2 particles of 101~102 nanometer were dispersed in the Al2O3 matrix. Both powders were sintered for 4 hours in the temperature range over 1500~1$650^{\circ}C$ with and without 5wt% MgO sintering aid. Among these sintered bodies, nanocomposite powder compacts sintered at 1$650^{\circ}C$ for 4 hours with 5wt% MgO showed the most dense structure with the grain size under 5${\mu}{\textrm}{m}$ and highest relative density of 98.2%.

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