• 한국주조공학회지
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• 제21권4호
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• pp.239-245
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• 2001

Microstructure and mechanical properties of Sn-3.1 wt.%Ag-6.9 wt.%Bi system solders on Cu-substrate were studied. The Sn3.1 wt.%Ag-6.9 wt.%Bi alloy was designed by phase diagram and chemical properties and was prepared by melting in argon atmosphere. The mechanical properties of solder/Cu joints were examined by shear strength test, and also creep test. The microstructure of Sn-3.1 wt.%Ag-6.9 wt.%Bi alloy consists of Bi-rich phase and $Ag_3Sn$ precipitate in {\beta}-Sn$ matrix phase. The shear strength of the joint was decreased with aging treatment. Crack path under shear test was through the solder. Similar crack path change mode was observed at the creep test of solder/Cu joint. The creep behavior of Sn-3.1 wt.%Ag-6.9 wt.%Bi alloy represented the inverse primary creep behavior at all test condition. It is suggested that the inverse primary creep behavior is induced from Bi solute atoms in Sn-matrix. The creep resistance of Sn-3.1Ag-6.9Bi alloy is better than that of Sn-3.5 wt.%Ag alloy at all test conditions.

• 폴리머
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• 제39권2호
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• pp.200-209
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• 2015

In this study, the influence of dilauroyl peroxide on mechanical and thermal properties of different polypropylene (PP) matrices was investigated. Polypropylene matrices, different molecular weight isotactic PP containing 0.01, 0.02, 0.04, 0.06, 0.08, and 0.1 wt% of dilauroyl peroxide (DLP) were prepared by using a single-screw extruder. The effect of the visbreaking agent (DLP) on mechanical, physical, thermal and morphological properties of different molecular weight PP had been studied. Mechanical properties (tensile strength at break point, at yield and elongation at break point), melt flow index (MFI), scanning electron microscope (SEM) and differential scanning calorimetric (DSC) analyses of these matrices were examined. Melting ($T_m$) and crystallization ($T_c$) temperatures, crystallinity ratio (%) and enthalpies were determined. The microstructure of isotactic polypropylene matrix was investigated by scanning electron microscopy (SEM). From SEM analysis, it was observed that the surface disorder increased by the increasing amount of DLP. As a result of DSC analyses, the crystallinity ratio of the PP matrices has varied between 1.64-7.27%. Mechanical properties of the matrices have been improved. Particularly, the mechanical tests of PP have given interesting results when compounded with 0.06-0.08 wt% dilauroyl peroxide (DLP). Mechanical properties and thermal decomposition processes were all changed by increasing the amount of DLP in the matrix structure.

• 한국정밀공학회:학술대회논문집
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• 한국정밀공학회 2005년도 춘계학술대회 논문집
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• pp.1358-1362
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• 2005

The Ni-base superalloy GTD-111DS was designed in the 1970s and is widely used as the material of the first stage blade under a severe combination of temperature and pressure in gas turbines. But because GTD-111DS is distributed in the shape of blade and blade has a unique figure and many cooling channels, it is hard to manufacture the test specimen. In this reason, there are little data on the microstructure and mechanical properties of the alloy. Therefore through the microstructure analysis, present paper observed that the shape of $\gamma{'}$ did not change even if aging time was increased but the amount and volume of the deposition of secondary $\gamma{'}\;rose\;and\;secondary\;\gamma{'}\;grew\;among\;primary\;\gamma{'}$. Also, by tensile test for different temperature, there was difference between yield strength and tensile strength in room temperature on heat treatment and extracting region but the more increasing temperature, the more decreasing difference between yield strength and tensile strength.

• 한국건축시공학회:학술대회논문집
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• 한국건축시공학회 2009년도 추계 학술논문 발표대회
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• pp.161-164
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• 2009

This research is to show the mechanical properties of structural steels by welding at high temperature. Welding parts are divided with weld metal and HAZ(Heat Affected Zone). HAZ is formed by interval from welding heat source and heating and cooling rates. Then, the change of both microstructure and mechanical properties occurs. Discontinuity of mechanical and chemical property at HAZ is the cause of safety decrease of structure. At this point, in this research, tensile tests at high temperature with test pieces of base metal and weld metal of SS400 and SM490 are accomplished. From the results, the mechanical properties of both SS400 and SM490 are standardized without welding or non-welding.

• 한국주조공학회지
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• 제38권1호
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• pp.9-15
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• 2018

Electromagnetic continuous casting (EMCC) was used to fabricate Ti-6Al-4V alloys with properties suitable for medical applications. Ti-6Al-4V alloy ingots fabricated by EMCC were subjected to heat treatment, such as residual stress removing (RRS), furnace cooling after solution treatment (ST-FC) and water-cooling after solution treatment (ST-WC), in order to obtain characteristics suitable for the standard. After component analysis, the microstructure and mechanical properties (tensile strength and elongation) were evaluated by ICP, gas analysis, OM, SEM, a Rockwell hardness tester and universal testing machine. The Ti-6Al-4V alloy ingot fabricated by EMCC was fabricated without segregation, and the lamellar structure was observed in the RRS and ST-FC specimens. The ST-WC specimen showed only martensite structure. As a result of evaluating the mechanical properties based on the microstructure results, we found that the water-cooled heat treatment condition after the solution treatment was most suitable for the Ti-6Al-4V ELI standard.

• 한국건축시공학회:학술대회논문집
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• 한국건축시공학회 2023년도 가을학술발표대회논문집
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• pp.161-162
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• 2023

Limestone slag cement is a green and sustainable building material with huge market potential. However, its shortcoming of low early compressive strength needs to be improved. A method of using aluminum sulfate to improve the early strength of ternary mixed mortar was proposed, and its effect and optimal dosage were tested. Macroscopic properties such as mechanical properties and surface electrical resistivity were measured at different dosages (0%, 1%, 2%, 3%). The microstructure and products of the mixtures were tested in detail, including by scanning electron microscopy, thermogravimetric analysis, and X-ray diffraction. The results show aluminum sulfate enhances mechanical properties and significantly increases surface electrical resistivity. The 1% and 2% doses had no adverse effects on the 28-day mechanical properties, while the 3% dose reduced the 28-day strength. Considering the changes in mechanical properties and surface electrical resistivity, 1% aluminum sulfate is the optimal dosage.

• Computers and Concrete
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• 제12권1호
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• pp.1-18
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• 2013

This paper presents an actual microstructure-based numerical method to investigate the mechanical properties of concrete at mesoscopic level. Digital image processing technique is used to capture the concrete surface image and generate the actual 3-phase microstructure of the concrete, which consists of aggregate, matrix and interfacial transition zones. The microstructure so generated is then transformed into a mesh or grid for numerical analysis. A finite difference code FLAC2D is used for the numerical analysis to simulate the mechanical responses and failure patterns of the concrete. Several cases of concrete with different degrees of material heterogeneity and under different compression loading conditions have been analysed. From the numerical results, the effects of the internal material heterogeneities as well as the external confining stresses are studied. It is shown that the material heterogeneities arising from the presence of different phases and the existence of interfacial transition zones have great influence on the overall mechanical behaviour of concrete and that the numerically simulated behaviour of concrete with or without confining stresses applied agrees quite well with the general observations reported in the literature.

• 열처리공학회지
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• 제27권3호
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• pp.115-120
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• 2014

Microstructural features were comparatively investigated in AZ91 (Mg-9%Al-1%Zn) and AZ91-0.5%Sn alloys, in order to clarify the reason for the enhancement in room temperature tensile properties by the addition of small amount of Sn in Mg-Al-based alloy. In as-cast state, the Sn-containing alloy showed increased YS, UTS and elongation than the Sn-free alloy. The microstructural examination revealed that various factors including finer cell size, reduction of lamellar (${\alpha}+{\beta}$) phase and morphological change of bulky ${\beta}$ phase from partially divorced shape to fully divorced shape, are likely to be responsible for the improvement in tensile properties for the Sn-containing alloy. It is noted that two alloys showed similar tensile properties after solution treatment. This implies that microstructural evolution related to the ${\beta}$ phase plays a key role in better tensile properties in the Sn-containing alloy.

• 한국재료학회지
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• 제32권11호
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• pp.489-495
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• 2022

This research investigated how adding Sb (0.75, 1.0, 2.0 and 5.0 wt%) to as-extruded aluminum alloys affected their microstructure, mechanical properties, electric and thermal conductivity. The addition of Sb resulted in the formation of AlSb intermetallic compounds. It was observed that intermetallic compounds in the alloys were distributed homogenously in the Al matrix. As the content of Sb increased, the area fraction of intermetallic compounds increased. It can be clearly seen that the intermetallic compounds were crushed into fine particles and homogenously arrayed during the extrusion process. As the Sb content increased, the average grain size decreased remarkably from 282.6 ㎛ (0.75 wt%) to 109.2 ㎛ (5.0 wt%) due to dynamic recrystallization by the dispersed intermetallic compounds in the aluminum matrix during the hot extrusion. As the Sb content increased from 0.75 to 2.0 wt%, the electrical conductivity decreased from 61.0 to 59.8 % of the International Annealed Copper Standard. Also, as the Sb content increased from 0.75 to 2.0 wt%, the ultimate tensile strength did not significantly change, from 67.3 to 67.8 MPa.

• Advances in Computational Design
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• 제7권2호
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• pp.129-137
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• 2022

Compo-casting method is one of the popular technique to produce metal based matrix composites. But, one of the main challenges in this process is un-uniform spreading of reinforced subdivisions (particles) inside the metallic matrix and the lack of desirable mechanical properties of the final produced composites due to the low bonding strength among the metal matrix and reinforcement particles. To remove these difficulties and to promote the mechanical properties of these kind of composites, the WARM ARB technique was utilized as supplementary technique to heighten the mechanical and microstructural evolution of the casted Al/Al₂O₃ composite strips. The microstructure evolution and mechanical properties of these composites have been considered versus different WARM ARB cycles by tensile test, average Vickers micro hardness test, wear test and scanning electron microscopy (SEM). The SEM results revealed that during the higher warm- ARB cycles, big alumina clusters are broken and make a uniform distribution of alumina particles. It was shown that cumulating the forming cycles improved the mechanical properties of composites. In general, combined compo-casting and ARB process would consent making Al/Al₂O₃ composites with high consistency, good microstructural and mechanical properties.