• Title/Summary/Keyword: Microstructure and mechanical properties

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C-Ring Stress Corrosion Test for Inconel 600 Tube and Inconel 690 welded by Nd:YAG Laser (Nd:YAG 레이저로 용접한 인코넬 600관과 인코넬 690의 C링 응력 부식시험)

  • 김재도;문주홍;정진만;김철중
    • Proceedings of the KWS Conference
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    • 1998.10a
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    • pp.288-291
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    • 1998
  • Inconel 600 alloy is used as the material of nuclear steam generator tubing because of its mechanical properties, formability, and corrosion properties. According to reports, the life time of nuclear power plants decreases because of the pitting, intergranular attack, primary water stress corrosion cracking(PWSCC), and intergranular stress corrosion cracking(IGSCC), and denting in the steam generator. The SCC test is very important because of SCC appears in various environment such as solutions, materials, and stress. The C-Rig specimen was made of the steam generator welded sleeve repairing by the pulsed Nd:YAG laser. In the corrosion invironment, corrosion solutions are Primary Water, Caustic, and Sulfate solution and corrosion time is 1624-4877hr. The permitted stress is 30-60ksi.In this C-Ring SCC test is the relationship between corrosion depth, crack and corrosion environment is evaluated. SCC was happens in Sulfate and Corrosion solution but doesn't happen in Primary Water. The corrosion time and stress is very affected by the severely environment of Sulfate or Caustic solution. The microstructure observation indicates that SCC causes interganular failure in the grain boundary of vertical direction.

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Fatigue Assessment of Reactor Vessel Outlet Nozzle Weld Considering the LBZ and Welding Residual Stress Effect (국부 취화부와 용접 잔류응력 효과를 고려한 원자로 출구노즐 용접부의 피로강도 평가)

  • Lee, Se-Hwan
    • Journal of Welding and Joining
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    • v.24 no.2
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    • pp.48-56
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    • 2006
  • The fatigue strength of the welds is affected by such factors as the weld geometry, microstructures, tensile properties and residual stresses caused by fabrication. It is very important to evaluate the structural integrity of the welds in nuclear power plant because the weldment undergoes the most of damage and failure mechanisms. In this study, the fatigue assessments for a reactor vessel outlet nozzle with the weldment to the piping system are performed considering the welding residual stresses as well as the effect of local brittle zone in the vicinity of the weld fusion line. The analytical approaches employed are the microstructure and mechanical properties prediction by semi-analytical method, the thermal and stress analysis including the welding residual stress analysis by finite element method, the fatigue life assessment by following the ASME Code rules. The calculated results of cumulative usage factors(CUF) are compared for cases of the elastic and elasto-plastic analysis, and with or without residual stress and local brittle zone effects, respectively. Finally, the fatigue life of reactor vessel outlet nozzle weld is slightly affected by the local brittle zone and welding residual stresses.

Effect Boron and Silicon on Various Properties of Dental Cobalt-Chromium Alloys (치과용 Co-Cr 합금의 제성질에 미치는 Boron과 Silicon의 영향)

  • Jung, Jong-Hyun
    • Journal of Technologic Dentistry
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    • v.14 no.1
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    • pp.119-132
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    • 1992
  • This paper aims to investigate the effect of B and Si upon the mechanical properties, microstructure and corrosion resistance of Co-Cr base alloy. Ten groups of alloy ingot ingot with various contents of B and Si were remelted by high frequency electrical induction furnace and cast into tensile specimen of ADA Specification No. 14 Tensile and hardness test were carried out by Amsler and Rockwell hardness tester(R-30N), respectively. The microstructures of specimen were observed by SEM. The results obtained are summarized as follows : 1. As B content is increased, tensile strength, yield strength and Rockwell hardness number(R-30N) are also increased significantly, while the elongation is decreased significantly. 2. As Si contect os increased, no significant chang in tensile strength is noticed, yield strength is slightly decreased, but Rockwell hardness number(R-30N) is moderately in creased, Elongation marks maxium value with 1% Si content while with more than 1% Si it is decreased. 3. As B content is increased corrosion resistance is decreased and is at best with 1.5% B content. Corrosion resistance is increased with the increase of Si content and the alloys with Si over 3.0% showed corrosion resistance. 4. As B content increased, precipitates are increased in number at grain boundaries. The grain size tends to become coarse with the increase of Si content. 5. Co rich-Cr alloy is present through matrix whereas at the grain boundaries Cr base precipitates are primarily formed.

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Development of an Mg-Based Alloy with a Hydrogen-Storage Capacity over 6 wt% by Adding Graphene

  • Choi, Eunho;Kwak, Young Jun;Song, Myoung Youp
    • Metals and materials international
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    • v.24 no.6
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    • pp.1403-1411
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    • 2018
  • Graphene (multilayer graphene) was chosen as an additive to improve the hydrogen uptake and release properties of magnesium (Mg). Five weight percent of graphene was added to pre-milled Mg by milling in hydrogen (reaction-involving milling). The hydrogen uptake and release properties of the graphene-added Mg were investigated. The activation of Mg-5graphene, which was prepared by adding 5 wt% graphene to Mg pre-milled for 24 h, was completed after the second cycle (cycle number, CN=2). Mg-5graphene had a high effective hydrogen-storage capacity (the quantity of hydrogen absorbed for 60 min) of 6.21 wt% at CN=3 at 593 K in 12 bar $H_2$. At CN=1, Mg-5graphene released 0.46 wt% hydrogen for 10 min and 4.99 wt% hydrogen for 60 min. Milling in hydrogen is believed to create defects (leading to facilitation of nucleation), produce cracks and clean surfaces (leading to increase in reactivity), and decrease particle size (leading to diminution of diffusion distances or increasing the flux of diffusing hydrogen atoms). The added graphene is believed to have helped the sample have higher hydrogen uptake and release rates, weakly but partly, by dispersing heat rapidly.

Changes in Flexural Strength and Electrical Resistivity of Bulk Graphite According to the Viscosity of Impregnant (함침재의 점도에 따른 벌크흑연의 굽힘강도 및 전기비저항 변화)

  • Lee, Sang-Min;Lee, Sang-Hye;Roh, Jae-Seung
    • Korean Journal of Materials Research
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    • v.31 no.2
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    • pp.108-114
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    • 2021
  • In the manufacturing of bulk graphite, pores produced by vaporization and discharge of volatile materials in binders during carbonization reduce the density of bulk graphite, which adversely affects the electrical conductivity, strength and mechanical properties. Therefore, an impregnation process is introduced to fill the pores and increase the density of bulk graphite. In this study, bulk graphite is prepared by varying the viscosity of the impregnant. The microstructure of bulk graphite is observed. The flexural strength and electrical resistivity are measured. As the viscosity of the impregnants decreases and the number of impregnations increases, it is shown that the number of pores decreases. The density before impregnation is 1.62 g/㎤. The density increases to 1.67 g/㎤ and porosity decreases by 18.6 % after three impregnations using 5.1 cP impregnant, resulting in the best pore-filling effect. After three times of impregnation with a viscosity of 5.1 cP, the flexural strength increases by 55.2 % and the electrical resistivity decreases by 86.76 %. This shows that a slight increase in density due to the pore-filling effect improves the properties of bulk graphite.

Exploration of Aluminum Alloy using Multi-feeder 3D Additive Manufacturing-based Combinatorial Experiment (Multi-feeder 3차원 적층제조 기반 조합실험을 활용한 알루미늄 합금탐색)

  • Suwon Park;Yongwook Song;Jiyoon Yeo;Songyun Han;Hyunjoo Choi
    • Journal of Powder Materials
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    • v.30 no.3
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    • pp.255-261
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    • 2023
  • Aluminum alloys are widely utilized in diverse industries, such as automobiles, aerospace, and architecture, owing to their high specific strength and resistance to oxidation. However, to meet the increasing demands of the industry, it is necessary to design new aluminum alloys with excellent properties. Thus, a new method is required to efficiently test additively manufactured aluminum alloys with various compositions within a short period during the alloy design process. In this study, a combinatory approach using a direct energy deposition system for metal 3D printing process with a dual feeder was employed. Two types of aluminum alloy powders, namely Al6061 and Al-12Cu, were utilized for the combinatory test conducted through 3D printing. Twelve types of Al-Si-Cu-Mg alloys were manufactured during this combinatory test, and the relationship between their microstructures and properties was investigated.

A Study on the Microstructure and Physical Properties of Cold Sprayed Cu/CNT Composite Coating (저온 분사 코팅법으로 제조된 Cu/CNT 복합 코팅층의 미세조직 및 물성 연구)

  • Kwon, Seong-Hee;Park, Dong-Yong;Lee, Dae-Yeol;Euh, Kwang-Jun;Lee, Kee-Ahn
    • Korean Journal of Metals and Materials
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    • v.46 no.3
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    • pp.182-188
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    • 2008
  • Carbon nanotubes(CNTs) have outstanding mechanical, thermal, and electrical properties. Thus, by placing nanotubes into appropriate matrix, it is postulated that the resulting composites will have enhanced properties. Cold spray can produce thick metal-based composite coatings with very high density, low oxygen content, and phase purity, which leads to excellent physical properties. In this study, we applied cold spray coating process for the consolidation of Cu/CNT composite powder. The precursor powder mixture, in which CNTs were filled into copper particles, was prepared to improve the distribution of the CNT in copper matrix. Pure copper coating was also conducted by cold spraying as a reference. Annealing heat treatment was applied to the coating to examine its effect on the properties of the composite coating. The hardness of Cu/CNT composite coating represented similar value to that of pure copper coating. It was importantly found that the electrical conductivity of the Cu/CNT composite coating significantly increased from 53% for the standard condition to almost 55% in the optimized condition, taking annealed ($500^{\circ}C/1hr$.) copper coating as a reference (100%). The thermal conductivity of Cu/CNT composite coating layer was higher than that of pure Cu coating. It was also found that the electrical and thermal conductivities of Cu/CNT composite could be improved through annealing heat treatment. The microstructural evolution of Cu/CNT coating was also investigated and related to the macroscopic properties.

Formation of ultrafine Grains in the Al 5083 Alloy by Cryogenic Rolling Process (극저온 압연에 의한 초세립 Al 5083 Alloy 제조)

  • 이영범;심혜정;남원종
    • Proceedings of the Korean Society for Technology of Plasticity Conference
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    • 2003.10a
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    • pp.163-167
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    • 2003
  • The large deformation at cryogenic temperature would be one of the effective methods to produce large bulk UFG materials. The effects of annealing temperature 150∼300$^{\circ}C$, on microstructure and mechanical properties of the sheets received 85% reduction at cryogenic temperature were investigated. In comparison with those at room temperature. Annealing of 5083 Al alloy deformed 85%, at 200$^{\circ}C$ for an hour, results in the considerable increase of tensile elongation without the great loss of strength and the occurrence of equiaxed grains less than 300nm in diameter.

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Fabrication of Electrically Conductive $TiB_2$-BN-AlN Composites (전기 전도성 $TiB_2$-BN-AlN 복합체의 제조)

  • 배동식;한경섭;최상홀
    • Journal of the Korean Ceramic Society
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    • v.33 no.5
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    • pp.524-530
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    • 1996
  • TiB2-BN-AlN composite was fabricated with the addition of 0~12 wt% WC by HP-sintering. Their sinterability. microstructure mechanical and electrical properties were studied as a function of the WC content. The addition of WC up to 12 wt% increased the flexural strength and decreased electrical resistivity as compared with those of the TiB2-BN-AlN composites. The electrical resistivity of TiB2-BN-AlN composite with 4.3 wt% WC was 640$\mu$$\Omega$-cm. It was found that the TiB2-BN-AlN composites with WC addition more than 4wt% was suitable for the application to the Al evaporation boat.

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Microstructure and Mechanical Interfacial Properties of Diamond in Ag-based Filler Metal for mini Wire by Vacuum Brazing (Ag계 금속필러를 이용한 다이아몬드와 극세선의 브레이징 접합부의 거동연구)

  • Chae, Na-Hyeon;Lee, Jang-Hun;Im, Cheol-Ho;Park, Seong-Won;Lee, Ji-Hwan;Song, Min-Seok
    • Proceedings of the KWS Conference
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    • 2007.11a
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    • pp.251-253
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    • 2007
  • 현재 다이아몬드 공구에서 극세선에 브레이징 공정을 이용하여 다이아몬드를 접합하는 기술은 국내외 적으로 전무한 상태이다. 이 연구는 금속 와이어에 다이아몬드를 브레이징을 실시하여 최적의 와이어 브레이징 공정법을 개발 하는데 있다. 다이아몬드와 금속필러메탈 접합 계면에서의 금속성분과 탄화물의 거동을 분석하며, 브레이징에 따른 와이어의 물성 변화를 관찰하였다. 금속필러로는 Ag-Cu-5Ti(wt.%)을 사용하였으며, 와이어는 스테인리스를 이용하였다. 브레이징 공정은 진공 접합 장치를 이용하여 $800{\sim}1000^{\circ}C$에서 유지시간 $5{\sim}30$분로 실시하였다. 브레이징된 다이아몬드는 $900{\sim}950$도, 유지시간 10분 사이에서 각각 건전한 계면과 표면을 얻을 수 있었으며, 계면에서 Ti-rich상과 화합물이 확인되었다. 또한 열처리 따른 와이어의 최적의 건전한 상태를 고찰 하였다. 다이아몬드와 Ag계 브레이징 필러의 계면에서의 미세조직 및 화학반응의 메커니즘은 SEM, EPMA, XRD를 이용하여 분석하였다.

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