• Applied Microscopy
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• v.43 no.4
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• pp.164-172
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• 2013

In this work, microstructural and hardness evolution of the X20 steel upon short-term creep test ($550^{\circ}C$ to $650^{\circ}C$, $180^{\circ}C$ to 60 MPa) was studied by using scanning electron microscope, electron backscattered diffraction, and transmission electron microscope, microhardness tester. After creep rupture, gauge and grip part of the specimens were microstructurally analyzed. Creep at the $650^{\circ}C$/60 MPa resulted in a rupture at 1,460 hours with growth of lath width from 1.31 to $2.87{\mu}m$ and a grain growth with a more equiaxed feature. There is a close relationship between Microhardness and lath width. The formation and coarsening of Laves phase, which was observed up to $600^{\circ}C$ of creep temperature, was accelerated by the applied stress. Slight coarsening of the $M_{23}C_6$ was observed in the $550^{\circ}C$ and $600^{\circ}C$ crept or aged specimens. The coarsening of $M_{23}C_6$ depended on the temperature, where specimens crept at $650^{\circ}C$ showed higher growth rate. The microstructural evolution of X20 after short-term creep test was extensively discussed in relation to the long-term creep/aging test reported in literatures.

• Journal of the Korean Ceramic Society
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• v.37 no.5
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• pp.479-490
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• 2000

The microstructure of Ni-YSZ composite as an anode of SOFC was investigated as a function of Ni content(10-70 vol%) in order to examine the correlation between microstructural-and electrical property. Image analysis based on quantitative microscopy theory was performed to quantify the microstructural property. We could get the informations about the size and distribution, contiguity and interfacial area of each phase or between the phases from the image analysis. According to the image analysis, contiguity between the same phae was mainly dependent on the amount of the phase while the contiguity between different phases was additionally influenced by the microstructural changes, especailly by the coarsening of the Ni phase. The whole length of pores perimeter was increased as Ni content increased, which indicated the overall microstructural evolution was mostly related with the coarsening of Ni phase. Ni-Ni interfacial area was also gradually increased as Ni content increased but controlled by pore phase at low Ni content region and by YSZ phase at intermediate Ni content region. These quantified microstructural properties were used to characterize the electrical properties of Ni-YSZ composite.

• Journal of Powder Materials
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• v.31 no.1
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• pp.1-7
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• 2024

This study explores the profound impact of varying oxygen content on microstructural and mechanical properties in specimens HO and LO. The higher oxygen concentration in specimen HO is found to significantly influence alpha lath sizes, resulting in a size of 0.5-1 ㎛, contrasting with the 1-1.5 ㎛ size observed in specimen LO. Pore fraction, governed by oxygen concentration, is high in specimen HO, registering a value of 0.11%, whereas specimen LO exhibits a lower pore fraction (0.02%). Varied pore types in each specimen further underscore the role of oxygen concentration in shaping microstructural morphology. Despite these microstructural variations, the average hardness remains consistent at ~370 HV. This study emphasizes the pivotal role of oxygen content in influencing microstructural features, contributing to a comprehensive understanding of the intricate interplay between elemental composition and material properties.

• Journal of Korea Foundry Society
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• v.33 no.5
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• pp.193-203
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• 2013

The Ni-base superalloy CM247LC was directionally solidified (DS) using the Bridgman-type furnace to understand the effect of the chill plate on the microstructural evolution, such as dendrite arm spacing, microporosity, and MC-type carbide. The DS process was also modeled by the PROCAST to predict the solidification rate, thermal gradient, and resultant cooling rate in the entire length of the DS specimen. Due to the quenching effects of chill plate, four distinct areas were found to form in the specimen, in which the solidification rate was changed, during DS at a given withdrawal rate of 0.083 mm/s. Among the microstructural features investigated, the dendrite arm spacings and average size of the MC-type carbide near the chill plate were found to be influenced by the quenching effect of the chill plate. However, no significant influence was found on the size and volume fraction of microporosity, and the volume fraction of the MC-type carbide. The relationship between the microstructural features and the solidification variables was also analyzed and discussed on the basis of a combination of experimental and modeling results.

• Journal of Korea Foundry Society
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• v.21 no.3
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• pp.192-197
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• 2001

본 연구에서는 여러 다른 냉각속도로 냉각되는 강의 조직과 경도를 예측하는 수치 해석을 수행하였다. 해석 프로그램은 확산과 비확산 변태에 대한 변태 이행 방정식과 유한차분법을 이용하여 제품에 대해서 온도분포 및 조직변태에 대한 예측을 수행하고 또한 경도를 예측하도록 하였다. 해석 결과와의 비교를 위해 여러 다른 냉각속도로 냉각되는 AISI 410시편들에 대한 일련의 시험을 행하여 각각의 조직과 경도를 구하였으며 특히 온도해석에 사용하는 열전달계수는 실험을 통하여 구한 값을 사용하였다. 실험에 의해 구해진 결과는 해석 프로그램을 이용한 값과 잘 일치 하였다.

• Proceedings of the Korean Society for Technology of Plasticity Conference
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• 2009.10a
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• pp.263-266
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• 2009

Transformation induced plasticity (TRIP) steel consisting of ferrite, austenite, and bainite phases was regarded as an excellent candidate for automotive applications due to the good combination of ductility and strength. The aim of the present study was to understand the microstructural characteristics of ultrafine grained (UFG) TRIP low-carbon steel fabricated via equal channel angular pressing accompanied with intercritical- and isothermal-annealing treatments. When compared to coarse grained counterpart, only the volume fraction of austenite phase in UFG TRIP steel remained unchanged, but all other microstructural variables such as size and morphology were different. It was found that UFG TRIP steel showed the homogeneous distribution of each constituent phase, which was discussed in terms of annealing treatments done in this study.

• Journal of the Korean Society for Heat Treatment
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• v.27 no.3
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• pp.115-120
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• 2014

Microstructural features were comparatively investigated in AZ91 (Mg-9%Al-1%Zn) and AZ91-0.5%Sn alloys, in order to clarify the reason for the enhancement in room temperature tensile properties by the addition of small amount of Sn in Mg-Al-based alloy. In as-cast state, the Sn-containing alloy showed increased YS, UTS and elongation than the Sn-free alloy. The microstructural examination revealed that various factors including finer cell size, reduction of lamellar (${\alpha}+{\beta}$) phase and morphological change of bulky ${\beta}$ phase from partially divorced shape to fully divorced shape, are likely to be responsible for the improvement in tensile properties for the Sn-containing alloy. It is noted that two alloys showed similar tensile properties after solution treatment. This implies that microstructural evolution related to the ${\beta}$ phase plays a key role in better tensile properties in the Sn-containing alloy.

• Proceedings of the KWS Conference
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• 2002.10a
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• pp.205-210
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• 2002

This article presents an integrated modeling approach for coupled analysis of heat transfer and microstructure evolution in welding carbon steel. The modeling procedure utilizes commercial [mite element code ABAQUS/Standard as the platform for solving the equation of heat conduction. User subroutines that implement computational thermodynamics and kinetics models are integrated with the FEA code to compute the transient microstructure evolution. In this study, the integrated models are applied to simulate the hot-tap repair welding of carbon steel pipeline. Microstructural components are treated as user output variables. Based on the predicted microstructure and cooling rates, hardness distributions in the welds were also predicted. The predicted microstructure and hardness distribution were found in good agreement with metallographic examinations and hardness measurements. This study demonstrates the applicability of computational models for the development of welding procedure for in-service pipeline repair.

• International Journal of Korean Welding Society
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• v.2 no.2
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• pp.1-6
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• 2002

This article presents an integrated modeling approach for coupled analysis of heat transfer and microstructure evolution in welding carbon steel. The modeling procedure utilizes commercial finite element code ABAQUS/Standard as the platform for solving the equation of heat conduction. User subroutines that Implement computational thermodynamics and kinetics models are integrated with the FEA code to compute the transient microstructure evolution. In this study, the integrated models are applied to simulate the hot-tap repair welding of carbon steel pipeline. Microstructural components are treated as user output variables. Based on the predicted microstructure and cooling rates, hardness distributions in the welds were also predicted. The predicted microstructure and hardness distribution were found in good agreement with metallographic examinations and hardness measurements. This study demonstrates the applicability of computational models for the development of welding procedure for in-service pipeline repair.

• Proceedings of the Materials Research Society of Korea Conference
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• 1992.05b
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• pp.94-95
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• 1992