• Title/Summary/Keyword: Micro-content

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A Study on the Recrystallization Behavior of Zr-xSn Binary Alloys (Zr-xSn 이원계 합금의 재결정에 관한 연구)

  • Lee, Myeong-Ho;Gu, Jae-Song;Jeong, Yong-Hwan;Jeong, Yeon-Ho
    • Korean Journal of Materials Research
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    • v.9 no.11
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    • pp.1123-1128
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    • 1999
  • To investigate the effect of Sn on the recrystallization of Zr-based alloys. Zr-xSn (x=0.5, 0.8, 1.5, 2.0wt.%) alloys were manufactured to be the sheets through the defined manufacturing procedure. The specimens were annealed at $300^{\circ}C$ to $800^{\circ}C$ for 1 hour. The hardness, microstructure and precipitate of the alloys with the annealing temperature were investigated by using micro- knoop hardness tester, optical microscope(O/M) and transmission electron microscope(TEM), respectively. The cold-worked Zr-xSn alloys showed the typical behavior of the recovery. recrystallization, and grain growth. The recrystallization of Zr-xSn alloys occurred between $500^{\circ}C$ and $700^{\circ}C$. As the Sn content increased. the recrystallization temperature of the cold-worked alloys increased but their grain sizes after recrystallization decreased. It is suggested that the recrystallization of the cold- worked Zr alloys be occurred by the subgrain coalescence and growth mechanism.

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Laser Cladding with Al-36%Si Powder Paste on A319 Al Alloy Surface to Improve Wear Resistance (A319 알루미늄 합금 표면에 Al-36%Si 합금분말의 레이저 클래딩에 의한 내마모성 향상)

  • Lee, Hyoung-Keun
    • Journal of Welding and Joining
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    • v.35 no.2
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    • pp.58-62
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    • 2017
  • A319 aluminum alloy containing 6.5% Si and 3.5% Cu as major alloying elements has been widely used in machinery parts because of its excellent castability and crack resistance. However it needs more wear resistance to extend its usage to the severe wear environments. It has been known that hyper-eutectic Al-Si alloy having more than 12.6% Si contains pro-eutectic Si particles, which give better wear resistance and lubrication characteristics than hypo-eutectic Al-Si alloy like A319 alloy. In this study, it was tried to clad hyper-eutectic Al-Si alloy on the surface of A319 alloy. In the experiments, Al-36%Si alloy powder was mixed with organic binder to make a fluidic paste. The paste was screen-printed on the A319 alloy surface, melted by pulsed Nd:YAG laser and alloyed with the A319 base alloy. As experimental parameters, the average laser power was changed to 111 W, 202 W and 280 W. With increasing the average laser power, the melting depth was changed to $142{\mu}m$, $205{\mu}m$ and $245{\mu}m$, and the dilution rate to 67.2 %, 72.4 % and 75.7 %, and the Si content in the cladding layer to 16.2 %, 14.6 % and 13.7 %, respectively. The cross-section of the cladding layer showed very fine eutectic microstructure even though it was hyper-eutectic Al-Si alloy. This seems to be due to the rapid solidification of the melted spot by single laser pulse. The average hardness for the three cladding layers was HV175, which was much higher than HV96 of A319 base alloy. From the block-on-roll wear tests, A319 alloy had a wear loss of 5.8 mg, but the three cladding layers had an average wear loss of 3.5 mg, which meant that an increase of 40 % in wear resistance was obtained by laser cladding.

Electrophoretic analysis of the major proteins of race horse erythrocyte membrane: Their relation to fast erythrocyte sedimentation rate (경주 적혈구막 단백의 전기영동법에 의한 분석 -빠른 적혈구 침강 속도와의 관계-)

  • Bahk, Yeong-woo;Lee, Si-yeong
    • Korean Journal of Veterinary Research
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    • v.31 no.3
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    • pp.259-264
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    • 1991
  • The proteins of the race horse erythrocyte membrane were analysed by polyacrylamide gel electrophoresis in sodium dodecyl sulfate(SDS-PAGE), and their relations to the fast erythrocyte sedimentation rate(ESR) of the race horse were investigated. The erythrocyte sedimentation rate of race horse were very fast compared with the human one(33 times <$90^{\circ}-plastic-ESR/30m$> and 25 times <$90^{\circ}-micro-ESR/30m$> as fast as the human one) are reported previously. Although the general protein profiles of the race horse erythrocyte membranes were almost similar to that of human, band 3 content was showing higher in race horse (34.7%) than in human (25.3%). The glycoprotein profiles of the race horse erythrocyte membranes revealed by periodic acid Schiff's(PAS) stain showed a marked difference from that of human. The PAS-1(glycophorin) and PAS-2(sialoglycoprotein) present in human erythrocyte memo brane were almost absent from the Holstein and race horse erythrocyte membranes, but PAS-2 was more in only race horse from that of human. Instead, the bovine erythrocyte membranes showed a strong PAS-B near the origin of the electrophorograms and the race horse erythrocyte membranes showed a strong PAS-negative band near the end of the electrophorograms, which is named as PAS-E in this study. These results suggest that the fast sedimentation rate of race horse erythrocyte is due in part to the presence of more band 3 protein fraction and PAS-E glycoproteins in the race horse erythrocytes.

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Production of Protein Hydrolyzate, that can be used as Food Additives, from Okara (산업폐기물인 비지로부터 식품첨가물로 이용할 수 있는 단백질 가수분해물의 생산)

  • Woo, Eun-Yeol;Kim, Min-Jung;Shin, Weon-Sun;Lee, Kyung-Ae;Kim, Kang-Sung
    • Korean Journal of Food Science and Technology
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    • v.33 no.6
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    • pp.769-773
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    • 2001
  • Protein content of okara and soybean were found to be 37.3% and 42.5%, respectively by micro-Kjeldahl analysis. Solubility of okara protein in phosphate buffer (pH 8) was 10% versus soy protein of 68.4%. Insolubilization of okara protein was mostly due to disulfide bonding between cysteine residues caused by excessive heat treatment during soymilk processing: hydrophobic interactions and hydrogen bondings were involved to lesser extent. Optimum extraction temperature and time were $60^{\circ}C$ and 40 min. Typical solubility profile of soy protein disappeared for okara protein though minimum solubility of the protein was around pH 3.0. Treating okara with protease was effective in solubilizing okara protein and solubility increased to 19.2%. Optimum reaction temperature and time were $80^{\circ}C$ and 50 min, respectively. Cell wall degrading enzyme did not increase solubility of the protein, however. Through enzymatic reaction okara protein could be effectively solubilized for uses as food ingredient.

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Effect of Cyclic Freezing-Thawing on Compressive Strength of Decomposed Granite Soils (동결-융해 반복작용으로 인한 화강풍화토의 압축강도 특성 변화에 관한 연구)

  • Yoo, Chung-Sik;Shin, Boo-Nam
    • Journal of the Korean Geosynthetics Society
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    • v.10 no.1
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    • pp.19-28
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    • 2011
  • This paper presents the results of an investigation into the effect of cyclic freezing-thawing on the compressive strength characteristics of decomposed granite soils. A plane strain compression (PSC) tests were performed on a series of test specimens with different freezing-thawing cycles and fine contents to investigate the change in compressive strength under the process of freezing-thawing cycles. Also performed were scanning electron microscope (SEM) tests to investigate the change in structural rearrangement from a micro-scale point of view. The test results showed that the soil particles tend to conglomerate when subject to cycles of freezing and thawing, and that the soil with less fines exhibited decreased shear strength due to the cyclic freezing-thawing while the soils with a larger fine content showed the opposite trend.

Microsatellite Analysis of the Silkworm Strains (Bombyx mori) Originated from China

  • Kim, Kee-Young;Kang, Pil-Don;Ryu, Kang-Sun;Kim, Ki-Hwan;Sung, Gyoo-Byung;Ji, Sang-Deok;Kim, Mi-Ja;Kim, Ik-Soo
    • International Journal of Industrial Entomology and Biomaterials
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    • v.25 no.1
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    • pp.81-92
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    • 2012
  • A total of 85 Chinese-origin silkworm strains preserved in Korea were genotyped for eight polymorphic micro-satellite loci. We obtained per-locus number of alleles, ranging from 5 to 14 with an average value of 9.5, perlocus observed heterozygosity, ranging from 0.07 to 0.99, and per-locus polymorphic information content (PIC), ranging from 0.34 to 0.82, indicating that some loci are highly variable. Phylogenetic analysis with the eight concatenated microsatellite loci showed no clustering on the basis of known strain characteristics. A total of 22 strain-specific apomorphic alleles, which discriminate 19 among 85 silkworm strains were obtained from eight loci. These strain-specific alleles, thus, can casually be utilized for the discrimination of applicable strains without any further typing of other loci. Furthermore, a substantial number of homozygote strains, represented by 27 among 76 alleles in eight loci were found. These results collectively suggest that the silkworm microsatellite DNA is actually and potentially important molecular markers for the eventual discrimination of silkworm strains that are preserved as hundreds in Korea.

Investigation of Ag Migration from Ag Paste Bump in Printed Circuit Board (Ag Paste bump 구조를 갖는 인쇄회로기판의 Ag migration 발생 안전성 평가)

  • Song, Chul-Ho;Kim, Young-Hun;Lee, Sang-Min;Mok, Jee-Soo;Yang, Yong-Suk
    • Korean Journal of Materials Research
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    • v.20 no.1
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    • pp.19-24
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    • 2010
  • The current study examined Ag migration from the Ag paste bump in the SABiT technology-applied PCB. A series of experiments were performed to measure the existence/non-existence of Ag in the insulating prepreg region. The average grain size of Ag paste was 30 nm according to X-ray diffraction (XRD) measurement. Conventional XRD showed limitations in finding a small amount of Ag in the prepreg region. The surface morphology and cross section view in the Cu line-Ag paste bump-Cu line structure were observed using a field emission scanning electron microscope (FE-SEM). The amount of Ag as a function of distance from the edge of Ag paste bump was obtained by FE-SEM with energy dispersive spectroscopy (EDS). We used an electron probe micro analyzer (EPMA) to improve the detecting resolution of Ag content and achieved the Ag distribution function as a function of the distance from the edge of the Ag paste bump. The same method with EPMA was applied for Cu filled via instead of Ag paste bump. We compared the distribution function of Ag and Cu, obtained from EPMA, and concluded that there was no considerable Ag migration effect for the SABiT technology-applied printed circuit board (PCB).

EFFECT OF CYCLIC STRAIN RATE AND SULFIDES ON ENVIRONMENTALLY ASSISTED CRACKING BEHAVIORS OF SA508 GR. 1A LOW ALLOY STEEL IN DEOXYGENATED WATER AT 310℃

  • Jang, Hun;Cho, Hyun-Chul;Jang, Chang-Heui;Kim, Tae-Soon;Moon, Chan-Kook
    • Nuclear Engineering and Technology
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    • v.40 no.3
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    • pp.225-232
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    • 2008
  • To understand the effect of the cyclic strain rate on the environmentally assisted cracking behaviors of SA508 Gr.1a low alloy steel in deoxygenated water at $310^{\circ}C$, the fatigue surface and a sectioned area of specimens were observed after low cycle fatigue tests. On the fatigue surface of the specimen tested at a strain rate of 0.008 %/s, unclear ductile striations and a blunt crack tip were observed. Therefore, metal dissolution could be the main cracking mechanism of the material at this strain rate. On the other hand, on the fatigue surfaces of the specimens tested at strain rates of 0.04 and 0.4 %/s, brittle cracks and flat facets, which are evidences of the hydrogen induced cracking, were observed. In addition, a tendency of linkage between the main crack and the micro-cracks was observed on the sectioned area. Therefore, at higher strain rates, the main cracking mechanism could be hydrogen induced cracking. Additionally, evidence of the dissolved MnS inclusions was observed on the fatigue surface from energy dispersive x-ray spectrometer analyses. Thus, despite the low sulfur content of the test material, the sulfides seem to contribute to environmentally assisted cracking of SA508 Gr.1a low alloy steel in deoxygenated water at $310^{\circ}C$.

An Fundamental Study on the Earth Wall Material Development by using of Lime Composition and Earth (석회복합체와 흙을 이용한 흙벽체 재료 개발에 관한 기초적 연구)

  • Hwang, Hey zoo;Kang, Nam Yi
    • KIEAE Journal
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    • v.10 no.5
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    • pp.115-121
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    • 2010
  • Lime was the solidifier mostly used at the fields of construction and civil works in the past. however, the development of Portland cement remarkably reduced the use of it. Recently as the concernment on circumstances gets higher, lime wined attention again as an eco-friendly material and was used at earth-using construction. This study examined the physical and chemical capacity of lime complexes with lime capacity improved, and performed fundamental study on the way to concretize by mixing it with earth. As a result, lime complex pressure strength was lower than cement pressure strength but it showed the possibility that its strength was improved by W/B control. The measurement of XRD after paste formation confirmed a compound generated by the reaction of Ca2+ion and Si, Al, and Fe from pozzolan reaction. A earth wall experiment by using lime complexes and earth showed that the higher, WB or the lower the quantity of unit combined materials, the lower the pressure strength was. The maximum pressure strength was maximum 11MPa when the quantity of unit combined materials was 450. It is because the composed earth particles had a high content of micro powder less than silt, so a lot of combination are demanded to secure fluidity. As a result of peptization experiment, after hardening, the material was not dissolved, which informed of the possibility of use as an outer subsidiary material. If the material is hardened by mold formation method, natural hardening crack appears. Cast expresses smart surface quality and enables to design for multiple purpose. The result shows the possibility of construction of low-story structures by using earth wall made of lime complexes and earth.

Absorption and Partition of $^{15}N-labeled$ Fertilizer in Rice under Different Nitrogen Application Time and Rate Conditions

  • Chun, Areum;Lee, Ho-Jin
    • KOREAN JOURNAL OF CROP SCIENCE
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    • v.51 no.1
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    • pp.32-40
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    • 2006
  • The nitrogen (N) absorption and partition of the rice plants are important indicators that can be used to improve the N use efficiency (NUE) of the plants. Improving the plant NUE can help to avoid nutrient waste that may cause environmental pollution. To investigate the N absorption and partition of the rice plants, Hwaseongbyeo (Japonica) and Dasanbyeo (indica/japonica) were applied with N fertilizers at the rates of 60, 120, and 180 kg N per ha in paddy field. Also micro plots of $0.81m^2$ were established inside each plot for application of $^{15}N-labeled$ fertilizer. The differences in N utilization of the rice plants were associated with the total N absorption and partitioning after the heading stage. In the grain filling period, the increase of nitrogen content in the total and leaf blades of Dasanbyeo was higher than that of Hwaseongbyeo. Soil N was the main contributor for the increase of total N of Dasanbyeo during the grain filling period. The N fertilizer uptake rate of Hwaseongbyeo rapidly increased with the increment of N fertilization rate. In Dasanbyeo, N fertilizer uptakes were similar under all rates and times of N application. From heading stage to harvest, Dasanbyeo continued accumulating nitrogen, whereas Hwaseongbyeo had small changes. In conclusion, the difference in nitrogen absorption and partition after heading of the two cultivars was caused by the ability of Dasanbyeo to accumulate and remobilize soil nitrogen to the grains during the grain filling period.