• Title/Summary/Keyword: Micro forming

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Effects of Property Transformation and Marginal Gap Depending on Heat-Treatment of Metal-Porcelain by Gold Electro-Forming System (전기성형법을 이용한 치과용 금속-도재관의 소성에 따른 물성 변화가 변연 간격에 미치는 영향)

  • Kim, Chi-Young;Chung, In-Sung;Choi, Sung-Min
    • The Journal of the Korea Contents Association
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    • v.10 no.6
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    • pp.352-359
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    • 2010
  • The objective of this paper is to study on the property transformation for materials and to evaluate the precision through marginal gap depending on heat-treatment of metal-porcelain by the gold electro-forming system. Specimens for evaluating property of hardness treat non-treat(HC), once(H1), twice(H2), and three times(H3) by heating, respectively. Specimens for marginal gap classified as each groups of special bonder(FS), special bonder, opaque(FO), special bonder, opaque, body(FB) and non-treatment(FC). As a result for micro-hardness test, the level of hardness on each groups of H1, H2, H3 decreased rather than HC group(p<0.05). In addition, marginal gap was not affected by the number of times being treated by heating. Therefore, the marginal fitness and the precision for mterials were not affected by the heat-treatment on the process to make GES metal-porcelain.

Development of Spray Thin Film Coating Method using an Air Pressure and Electrostatic Force (공압과 정전기력을 이용한 스프레이 박막 코팅 기술 개발)

  • Kim, Jung Su;Kim, Dong Soo
    • Journal of the Korean Society for Precision Engineering
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    • v.30 no.6
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    • pp.567-572
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    • 2013
  • In many electro-devices, the vacuum process is used as the manufacturing process. However, the vacuum process has a problem, it is difficult to apply to a continuous process such as a R2R(roll to roll) printing process. In this paper, we propose an ESD (electro static deposition) printing process has been used to apply an organic solar cell of thin film forming. ESD is a method of liquid atomization by electrical forces, an electrostatic atomizer sprays micro-drops from the solution injected into the capillary with electrostatic force generated by electric potential of about several tens kV. The organic solar cell based on a P3HT/PCBM active layer and a PEDOT:PSS electron blocking layer prepared from ESD method shows solar-to-electrical conversion efficiency of 1.42% at AM 1.5G 1sun light illumination, while 1.86% efficiency is observed when the ESD deposition of P3HT/PCBM is performed on a spin-coated PEDOT:PSS layer.

Improvement of Light-Harvesting Efficiency of TiO2 Granules Through Chemical Interconnection of Nanoparticles by Adding TEOT to Spray Solution

  • Lim, Mi Ja;Song, Shin Ae;Kang, Yun Chan;So, Won-Wook;Jung, Kyeong Youl
    • Korean Chemical Engineering Research
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    • v.53 no.5
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    • pp.632-637
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    • 2015
  • Mesoporous $TiO_2$ granules were prepared by spray pyrolysis using nano-sized titania particles which were synthesized by a hydrothermal method, and they were evaluated as the photoanode of dye-sensitized solar cells. To enhance the cell efficiency, nanoparticles within granules were chemically interconnected by adding titanium ethoxide (TEOT) to colloidal spray solution. The resulting titania particles had anatase phase without forming rutile. $TiO_2$ granules obtained showed about 400 nm in size, the specific surface area of $74-77m^2/g$, and average pore size of 13-17 nm. The chemical modification of $TiO_2$ granules by adding TEOT initially to the colloidal spray solution was proved to be an effective way in terms of increasing both the light scattering within photoanode and the lifetimes of photo-excited electrons. Consequently, the light-harvesting efficiency of TEOT-modified granules (${\eta}=6.72%$) was enhanced about 14% higher than primitive nanoparticles.

Effect of Al Doping Concentration on Resistance Switching Behavior of Sputtered Al-doped MgOx Films

  • Lee, Gyu-Min;Kim, Jong-Gi;Park, Seong-Hun;Son, Hyeon-Cheol
    • Proceedings of the Korean Vacuum Society Conference
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    • 2012.08a
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    • pp.307-307
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    • 2012
  • In this study, we investigated that the resistance switching characteristics of Al-doped MgOx films with increasing Al doping concentration and increasing film thickness. The Al-doped MgOx based ReRAM devices with a TiN/Al-doped MgOx/Pt/Ti/SiO2 were fabricated on Si substrates. The 5 nm, 10 nm, and 15 nm thick Al-doped MgOx films were deposited by reactive dc magnetron co-sputtering at $300^{\circ}C$ and oxygen partial ratio of 60% (Ar: 16 sccm, O2: 24 sccm). Micro-structure of Al-doped MgOx films and atomic concentration were investigated by XRD and XPS, respectively. The Al-doped MgOx films showed set/reset resistance switching behavior at various Al doping concentrations. The process voltage of forming/set is decreased and whereas the initial current level is increased with decreasing thickness of Al-doped MgOx films. Besides, the initial current of Al-doped MgOx films is increased with increasing Al doping concentration in MgOx films. The change of resistance switching behavior depending on doping concentration was discussed in terms of concentration of non-lattice oxygen of Al-doped MgOx.

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Radical Mist Generator Using a Water Plasma Jet and Its Sterilization Effect

  • Huh, Jin Young;Ma, Suk Hwal;Kim, Kangil;Choi, Eun Ha;Hong, Yong Cheol
    • Proceedings of the Korean Vacuum Society Conference
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    • 2016.02a
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    • pp.175.1-175.1
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    • 2016
  • In recent, tract infections such as atopic dermatitis, allergic rhinitis and a respiratory disease are increasing, giving rise to the atmospheric pollution, inflow of micro-size dust and side effect of humidifier disinfectant. In this context, the environment-friendly technology is required to eliminate airborne pathogens. We propose solution of the previous problems, making use of Radical Mist Generator (RMG). Existing technologies of air purification using a gas discharge produce harmful substances such as ozone, NOx, etc. However, the RMG uses a pure water as a plasma forming material. The RMG sprays the water mist, which contains reactive radicals to sterilize microorganisms. RMG is comprised of a power supply, plasma electrodes and a nozzle. In order to analyze the electrical characteristic and concentrations of reactive radicals, we employ an oscilloscope and a titration method. To test the sterilization effect of RMG, we used E.coli. We confirmed that E.coli was killed over 90%. Eventually, we expect that RMG can be promising tool for a purified system.

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Study on the gate cutting of light guiding plate for mobile using quenching element (박형 도광판의 음각, 양각 마이크로 패턴 성형성에 관한 연구)

  • Hwang, Chul-Jin;Kim, Jong-Sun;Min, In-Gi;Kim, Jong-Dug;Yoon, Kyung-Hwan
    • Design & Manufacturing
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    • v.2 no.5
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    • pp.1-4
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    • 2008
  • LCD-BLU (Liquid Crystal Display - Back Light Unit) is one of kernel parts of LCD unit and it consists of several optical sheets(such as prism, diffuser and protector sheets), LCP (Light Guide Plate), light source (CCFL or LED) and mold frame. The LGP of LCD-BLU is usually manufactured by forming numerous dots with $50-200{\mu}m$ in diameter on it by erosion method. But the surface of the erosion dots of LGP is very rough due to the characteristics of the erosion process during the mold fabrication, so that its light loss is high along with the dispersion of light into the surface. Accordingly, there is a limit in raising the luminance of LCD-BLU. Especially, the negative and positive micro-lens pattern fabricated by modified LiGA with thermal reflow process was applied to the optical design of LGP.

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H2S Gas Sensing Properties of SnO2:CuO Thin Film Sensors Prepared by E-beam Evaporation

  • Sohn, Jae-Cheon;Kim, Sung-Eun;Kim, Zee-Won;Yu, Yun-Sik
    • Transactions on Electrical and Electronic Materials
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    • v.10 no.4
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    • pp.135-139
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    • 2009
  • $H_2S$ micro-gas sensors have been developed employing $SnO_2$:CuO composite thin films. The films were prepared by e-beam evaporation of Sn and Cu metals on silicon substrates, followed by oxidation at high temperatures. Results of various studies, such as scanning electron microscopy (SEM), X-ray diffraction (XRD) and X-ray photoelectron spectroscopy (XPS) reveal that $SnO_2$ and CuO are mutually non-reactive. The CuO grains, which in turn reside in the inter-granular regions of $SnO_2$, inhibit grain growth of $SnO_2$ as well as forming a network of p-n junctions. The film showed more than a 90% relative resistance change when exposed to $H_2S$ gas at 1 ppm in air at an operating temperature of $350^{\circ}C$ and had a short response time of 8 sec.

Synthesis of Polymer-Carbon Nanotubes Composite Nanoparticles and Their Applications into Forming Hybrid Composite Thin Films (폴리머-탄소나노튜브 복합체 에어로졸 입자의 생성 및 이를 이용한 하이브리드 복합체 박막 제조)

  • Kim, Whi-Dong;Ahn, Ji-Young;Kim, Soo Hyung
    • Particle and aerosol research
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    • v.6 no.2
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    • pp.61-67
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    • 2010
  • In this paper, we describe a new method to form polymer thin films, in which carbon nanotubes (CNTs) are homogeneously distributed so that they can strengthen the mechanical property of resulting polymer film. To do so, we first homogeneously mixed CNTs with polymer in a DMF solvent. With the assistance of ultrasonic nebulizer, the polymer/CNT solution was then aerosolized into micro-sized droplets and finally turned into solidified polymer/CNT composite particles by gas-phase drying process. As the results of SEM and TEM analysis, CNTs were found to be homogeneously immobilized in the polymer matrix particles due to rapid drying process in the gas phase. For comparison purpose, (i) the polymer/CNTs composite particles prepared by aerosol processing method and (ii) polymer/CNTs sheets prepared by simple solution-evaporation method were employed to form polymer/CNTs composite thin films using a hot press. As the result, the aerosol processing of composite particles was found to be a much more effective method to form homogeneously distributed-CNTs in the polymer matrix thin film.

Effects of Viscosity Control by Induction Heating on Micro Cell in Forming Process of Foamed Aluminum (알루미늄 발포재의 성형공정에서 유도가열 법에 의한 점도 제어가 미세 기공에 미치는 영향)

  • Jeon, Yong-Pil;Kang, Chung-Gil
    • Journal of the Korean Society for Precision Engineering
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    • v.19 no.6
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    • pp.136-144
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    • 2002
  • Melting method has long been considered difficult to realize because of problems such as the low foamability of molten metal, the varying size of cellular structures and solidification shrinkage. The parameters to solve the problem in electric furnace were stirring temperature, stirring velocity, heating velocity and foaming temperature It is important to consider the effects of induction heating, because it brings about the inner flow by the temperature gradient. Aspect ratio also depends on the induction heating. Mechanical properties are dependent on cell sizes and aspect rations. Therefore, this paper presents the effects of these parameters on the cell sizes. For the sake of this, combined stirring process was used to fabricate aluminum foam materials by the above mentioned parameters. Image analysis was performed to calculate the cell sizes, distributions, and aspect ratioes at the cross section of feared aluminum in the direction of height.

Characterization of Si/Mo Multilayer Anode for Microbattery (박막전지용 Si/Mo 다층박막 음극의 전기화학적 특성)

  • 이기령;정주영;문희수;이승원;이유기;박종완
    • Proceedings of the Materials Research Society of Korea Conference
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    • 2003.11a
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    • pp.209-209
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    • 2003
  • The adventages of Li alloys have attracted the attention of many research groups, many of which have investigated tin-based alloys [1-2], Despite interesting performances of these, the irreversible capacity loss systematically observed on the first cycle for these compounds is a main drawback for their use as anode materials in lithium ion cells. Not only Sn is efficient in forming alloys with Li, Si can also react with Li to form alloys with a high Li/Si ratio, like Li$\_$22/Si$\_$5/ at 400$^{\circ}C$. It corresponds to a capacity of 4200mAh/g. Electrochemical Li-Si reaction occurs between 0 and 0.3 V against Li/Li$\^$+/, so that high-energy density battery can be realized. Despite the high theoretical capacity of elements like Si, however, particles of the alloys crack and fragment due to the repeated alloying and do-alloying which occurs as cell are charged and discharged. The research groups of Muggins [3] and Besenhard [4] have proposed that the volume expansion due to the insertion of Li can be reduced in micro- and submicro-structured matrix alloys. For this reason, the research group of J.R. Dahn investigated Sn/Mo sequential sputter deposition to prepare nanocomposites [5]. In this study, we investigated the characterization and the electrochemical characteristics of sequentially sputtered Si/Mo multilayer for microbattery anode.

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