• Korean Journal of Metals and Materials
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• v.47 no.11
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• pp.687-693
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• 2009

Experiments have demonstrated that a moderate amount of Be added to $Zr_{57.5}Cu_{38.3}Al_{4.2}$ amorphous alloy enhances the plasticity of the alloy. In particular, $Zr_{54}Cu_{36}Al_{4}Be_{6}$ alloy exhibited 19% of strain to fracture along with a strength exceeding 2 GPa. Energy dispersive x-ray spectroscopy conducted on the $Zr_{54}Cu_{36}Al_{4}Be_{6}$ alloy exhibited the presence of compositional modulation, indicating that nm-scale phase separation had occurred at local regions. In this study, the role played by the nm-scale phase separation on the plasticity was investigated in terms of structural disordering, structural softening and shear localization in order to better understand the structural origin of the enhanced plasticity shown by the developed alloy.

• Proceedings of the KWS Conference
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• 2002.10a
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• pp.620-625
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• 2002

Considering the fuel consumption of car, a light structure of aluminum alloys is desired for car body nowadays. However, fusion welding of aluminum alloys has some problems of reduction of joint efficiency, porosity formation and hot cracking. ill the present work, investigation to improve the joint performance of laser welded joint has been carried out by addition of Cu, Ni, and Zr to A6N01 alloy welds. Aluminum alloy plate of 2.0mm in thickness with filler metal bar was welded by twin beam Nd:YAG laser facility (total power:5kW). The filler metals were prepared by changing the chemical compositions for adding the elements into the weld metal. Thirteen filler metal bars were prepared and pre-placed into the base metal before welding. Ar gas shielding with a flow rate of 10 l/min was used. The defocusing distance is kept at 0 mm. At travel speeds of 3 to 9 m/min and at laser power of 5kW (front beam 2kW rear beam 3kW), full penetration welds were obtained, whereas at travel speeds of 12 to 18 m/min and same power, partial penetration was observed. The joint efficiency of laser-welded joint was improved by the addition of Cu, Ni, and Zr due to the solid solution hardening, grain refining and precipitation hardening. The type of hardening has been further considered by metallurgical examination.

• International Journal of Korean Welding Society
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• v.2 no.2
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• pp.26-31
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• 2002

Considering the fuel consumption of car, a light structure of aluminum alloys is desired fer car body nowadays. However, fusion welding of aluminum alloys has some problems of reduction of joint efficiency, porosity formation and hot cracking. In the present work, investigation to improve the joint performance of laser welded joint has been carried out by addition of Cu, Ni, and Zr to A6NO 1 alloy welds. Aluminum alloy plate of 2.Omm in thickness with filler metal bar was welded by twin beam Nd: YAG laser facility (total power: 5kW). The filler metals were prepared by changing the chemical compositions for adding the elements into the weld metal. Thirteen filler metal bars were prepared and pre-placed into the base metal before welding. Ar gas shielding with a flow rate of 10 1/min was used. The defocusing distance is kept at 0 mm. At travel speeds off 3 to 9 and at laser power of 5kW (front beam 2kW rear beam 3kW), full penetration welds were obtained, whereas at travel speeds of 12 to 18 m/min and same power, partial penetration was observed. The joint efficiency of laser-welded joint was improved by the addition of Cu, Ni, and Zr due to the solid solution hardening, grain refining and precipitation hardening. The type of hardening has been further considered by metallurgical examination.

• Korean Journal of Materials Research
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• v.17 no.3
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• pp.142-146
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• 2007

Vacuum brazing method has been coming to an important process as one of the new fabricating techniques of metals and alloys. In this study, a vacuum brazing of SUS304 stainless steel with BNi-2 filler metal was carried out in $1{\times}10^{4}$ Torr of vacuum atmosphere. The formation of brittle intermetallic compounds in brazed joints between SUS304 stainless steel and BNi-2 filler metal is a major concern, since they considerably degrade the mechanical properties of joints. To obtain enough stable joining strength, it is necessary to understand the unique properties of brazing process with Ni-based filler metals containing boron. So, in this research we investigated the performance of SUS304/BNi-2 brazed system and the brazed joint properties were evaluated at room temperature by using tensile test. Metallurgical and fractographic analysis were used to characterize the microstructure, the mechanisms of brazing, and joint failure modes.

• Korean Journal of Metals and Materials
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• v.50 no.8
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• pp.583-589
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• 2012

This work is concerned with a statistical approach to the life prediction on irradiation-assisted stress corrosion cracking (IASCC) of stainless steel (SS) for core internals of a pressurized water reactor (PWR). The previous results of the time-to-failure of IASCC measured on neutron-irradiated stainless steel components were statistically analyzed in terms of stress and irradiation. The accelerating life testing model of IASCC of cold worked Type 316 SS was established based on an inverse power model with two stress-variables, the applied stress and irradiation dose. Considering the variation of the yield strength and applied stress with the irradiation dose in the model, the remaining life of the baffle former bolt was statistically predicted during operation under complex environments of stress and irradiation.

• Korean Journal of Metals and Materials
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• v.50 no.1
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• pp.86-91
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• 2012

Ti-6Al-4V extra low interstitial (ELI) alloy has been widely used as an orthopedic implant material because of its excellent biocompatibility, corrosion resistance and mechanical properties. However, V-free titanium alloys such as Ti-6%Al-7%Nb and Ti-5%Al-2.5%Fe have recently been developed because of the toxicity of V. Hydroxyapatite (HA) is used as a coating material on Ti or Ti biomaterials due to its good biocompatibility. However, HA coated on Ti alloy causes a problem for tissue by peeling off during usage. Therefore, such peeling off during long time usage can be suppressed by adding HA in Ti or Ti alloy composites. The aim of this study was to manufacture an ultra fine grained (UFG) Ti-Nb-HA bulk alloy, which is usually difficult to fabricate using melting and casting technology, by rapid sintering process using high energy mechanical milled (HEMM) powder.

• Korean Journal of Metals and Materials
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• v.49 no.7
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• pp.541-548
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• 2011

Thermomechanical fatigue (TMF) behavior of heat resistant austenitic stainless steel was evaluated in the temperature range from 100$^{\circ}C$ to peak temperatures of 600 to 800$^{\circ}C$; The fatigue lives under TMF conditions were plotted against the plastic strain range and the dissipated energy per cycle. In the expression of the inelastic strain range versus fatigue life, the TMF data obtained at different temperature ranges were located close to a single line with a small deviation; however, when the dissipated energy per cycle, calculated from the area of the stress-strain hysteresis loops at the half of the fatigue life, was plotted against the fatigue life, the data showed greater scattering than the TMF life against the inelastic strain range. A noticeable stress relaxation in the stress-strain hysteresis curve took place at the peak temperatures higher than 700$^{\circ}C$, but all specimens in this study exhibited cyclic hardening behavior with TMF cycles. Recrystallization occurred during the TMF cycle concurrent with the formation of fine subgrains in the recrystallized region, which is considered to cause the cyclic hardening of the steel.

• Korean Journal of Metals and Materials
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• v.47 no.12
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• pp.860-865
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• 2009

The effect of Co additive on the electrical properties of Fe-Si alloys prepared by a RF inductive furnace was investigated. The electrical conductivity and Seebeck coefficient were measured as a function of the temperature under an Ar atmosphere to evaluate their applicability to thermoelectric energy conversion. The electrical conductivity of the specimens increased as the temperature increased, showing typical semiconducting behavior. The electrical conductivity of Co-doped specimens was higher than that of undoped specimens and increased slightly as the amount of Co additive increased. This is most likely due to the difference in the carrier concentration and the amount of residual metallic phase ${\varepsilon}$-FeSi (The ${\varepsilon}$-FeSi was detected in spite of an annealing treatment of 100 h at $830^{\circ}C$). Additionally, metallic conduction increased slightly as the amount of Co additive increased. On the other hand, Co-doped specimens showed a lower Seebeck coefficient due to the metallic phase. The power factor of Co-doped specimens was higher than that of undoped specimens. This would be affected more by the electrical conductivity compared to the Seebeck coefficient.

• Journal of the Korean Society of Manufacturing Technology Engineers
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• v.19 no.4
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• pp.539-547
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• 2010

Laser shock peening is useful to improve fatigue characteristic of multiple number of metals and alloys. This process induces a compressive residual stress on the metal surface, and when tensile load is applied, growth of crack is delayed and which changes the characteristic of the metal surface. It is an innovative surface treatment technique for strengthening metals. Specimens of SM45C are used in this study. The effect of an inertial tamping layer on the residual stress field using laser shock peening setup and Nd:YAG laser power is evaluated. Residual stress distribution measured by X-ray diffraction. As a result of this study it can be presented that following condition of Nd:YAG laser power and inertial tamping layer parameters, compressive residual stress is generated on the surface of the SM45C. Results to experimental data indicate that laser shock peening has great potential as a means of improving the mechanical performance of the metal surface.

• Korean Journal of Metals and Materials
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• v.48 no.11
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• pp.965-973
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• 2010

The small punch creep (SPC) test has recently received much attention as a new alternative to the conventional uniaxial creep test because it needs only a miniature-sized specimen directly detached from an operating system or component without any serious sampling damages. However, it is difficult to obtain the equivalent uniaxial creep data directly from the SPC data. As a specimen is deformed by a punch in the SPC test, the test result is sensitive to the friction between them. Finite element analyses with various friction coefficients was performed and showed a tendency of increased SPC life with an increased friction coefficient. The necking position predicted by the SPC simulation with a proper friction coefficient showed good agreement with that observed from the real SPC test. Finally, a noble method to convert the SPC load and displacement rate into the equivalent uniaxial creep stress and strain rate, respectively, was established in this study.