• Journal of Magnetics
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• 제14권2호
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• pp.75-79
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• 2009

Nickel (Ni) and ferrite ($Fe_3O_4$, $NiFe_2O_4$) nanoparticles were synthesized by LGC using both wire feeding (WF) and micron powder feeding (MPF) systems. Phase evolution and magnetic properties were then investigated. The Ni nanopowder included magnetic-ordered phases. The LGC synthesis yielded spherical particles with large coercivity while the abnormal initial magnetization curve for Ni indicated a non-collinear magnetic structure between the core and surface layer of the particles. Since the XRD pattern cannot actually distinguish between magnetite ($Fe_3O_4$) and maghemite (${\gamma}-Fe_2O_3$) as they have a spinel type structure, the phase of the iron oxide in the samples was unveiled by $M{\ddot{o}}ssbauer$ spectroscopy. The synthesized Ni-ferrite consisted of single domain particles, including an unusual ionic state. The synthesized nanopowder bore an active surface due to the defects that affected abnormal magnetic properties.

• 대한기계학회논문집B
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• 제21권10호
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• pp.1303-1313
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• 1997

A micro-macroscopic analysis on the conduction-controlled directional casting of Al-Cu alloys is performed, in which emphases are placed on the microstructural features. In order to facilitate the solution procedure, an iterative micro-macroscopic coupling algorithm is developed. The predicted results show that the effect of finite back diffusion on the transient solidification process in comparison with the lever rule depends essentially on the initial concentration of an alloy. In the final casting, the eutectic fraction is distributed in an increasing-decreasing-increasing pattern, each mode of which is named the chill, interior and end zones. This nonuniformity per se suffices to justify the necessity of this work because it originates from the combined effects of finite back diffusion and cooling path-dependent nature of the eutectic formation. As the cooling rate is enhanced, not only the influence depths of boundaries narrow, but also the eutectic fractions in the chill and interior zones increase. In addition, it is revealed for the first time that the micro segregation band is formed in response to a sudden change in cooling rate during the directional casting. An increasing change creates an overshooting band in the eutectic fraction distribution, and vice versa.

• 전자공학회논문지 IE
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• 제48권1호
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• pp.45-50
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• 2011

본 논문에서는 UHF RFID 시스템을 콘크리트 블록에 매립하기 위해 다양한 종류의 RFID tag를 선택하여 실험한다. 매립된 tag의 수신율을 측정하기 위해 매립 깊이를 달리하고, 재질을 바꿔가며 감쇄율을 측정한다. 실험결과에서 콘크리트의 혼합비율은 성능에 큰 영향을 주지 않는 것을 알 수 있다. 본 연구는 GPS 신호를 사용할 수 없는 유비쿼터스 환경의 실내에서 위치기반의 서비스를 위해서 필요한 위치정보를 얻어 내는 방법인 RFID 시스템의 기반시설 매립에 초점을 맞춰 진행한다.

• 대한치과보철학회지
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• 제44권2호
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• pp.157-164
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• 2006

Purpose: The purpose of this study was to compare the fracture strength of the zirconia monolithic all-ceramic crowns according to the thickness(0.5 mm, 0.8 mm, 1.1 mm) and IPS Empress II ceramic crown of 1.5 mm thickness. Material and method: Eight crowns for each of 3 zirconia crown groups were fabricated using CAD/CAM system(Kavo, Germany) and eight Empress II crowns were made from silicone mold and wax pattern. Each crown group was finished in accordance with the specific manufacturer s instruction. All crowns were luted to the metal dies using resin cement and mounted on the testing jig in a universal testing machine. The load was directed at the center of crown with perpendicular to the long axis of each specimen until catastrophic failure occurred. Analysis of variance and Tukey multiple comparison test(p<.05) were applied to the data. Results and Conclusion: 1. The fracture strength of the zirconia monolithic all-ceramic crown was higher thickness increased(p<.05). 2 The fracture strength of 1.1 mm thickness zirconia monolithic all-ceramic crown was higher than the fracture strength of 1.5 mm thickness IPS Empress II crown(p<.05). 3. The fracture strength of 0.5 mm thickness zirconia monolithic all-ceramic crown exceeded maximum occlusal forces.

• 자원환경지질
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• 제31권3호
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• pp.265-271
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• 1998

In the hydrologic and hydrochemical studies of natural waters, oxygen and hydrogen isotope compositions of waters are very important to elucidate the origin and circulation pattern of water in the hydrologic system. The hydrogen isotope analysis of waters usually has been undertaken through the reduction of water to form hydrogen gas using pure metals (in general, zinc and uranium). In 1996, a new apparatus (H/Device) was developed to prepare the water samples (by the reduction with Cr metal) without some intrinsic problems that may yield incorrect and/or inaccurate data, and was installed at 1997 in the Center for Mineral Resources Research (CMR) in Korea University. However, the optimistic conditions of preparation and analysis of samples has not been established. In this paper, we introduce the efficiency of H/Device to obtain accurate hydrogen isotope values of water, and discuss both the optimum conditions including the effective reduction time and the probable mixing (memory) effect between successive samples. We obtained large amounts of a laboratory working standard (KUW; Korea University Water) with the average ${\delta}D_{SMOW}$ value of $-42.1{\pm}1.0$‰ $(1{\sigma})$.

• 한국재료학회지
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• 제16권11호
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• pp.698-704
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• 2006

In this study, the effect of chill layers occurred in shot sleeve on the molten metal filling was analyzed through computer simulation. The behavior of chill layers with temperature variation of shot sleeve set from 200 to $280^{\circ}C$ was also investigated. The simulation results showed the chill layers set in the in-gates during the injection process change the main filling direction and cause turbulent flow pattern, resulting in porosities inside the castings. The amount of chill layers with the increasing temperature of shot sleeve was considerably reduced. Particularly, at the setting temperature of $280^{\circ}C$ by heat control unit, the biggest reduction in chill layers, excellent trimmed surface and the highest density were achieved, suggesting that as the optimal sleeve condition in aluminum high pressure diecasting, especially for highly complex parts like valve body.

• 한국재료학회지
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• 제16권11호
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• pp.668-675
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• 2006

In the partial squeeze casting process, the filling behavior of liquid metal and solidification pattern in thick area have significant influence on the quality of casting products and die life. For the optimal casting design of automobile transmission gear housing, various analyses were performed in this study by using computer simulation code, MAGMAsoft and the simulation results were compared and analyzed with experimental results. By air pressure criteria, internal porosities caused by air entrap during the mold filling were predicted and reduced remarkably by modification of gating system. Also, optimal squeeze-time lag to apply partial squeeze pin in thick area was calculated and the castings was free from shrinkage defects with the result of solidification analysis. Consequently, casting design for automobile transmission gear housing was optimized and approved by Computer Tomography.

• 한국정밀공학회지
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• 제18권12호
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• pp.192-199
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• 2001

Chemical mechanical planarization (CMP) has emerged as the planarization technique of choice in both front-end and back-end integrated circuit manufacturing. Conventional CMP process utilize a polyurethane polishing pad and liquid chemical slurry containing abrasive particles. There hale been serious problems in CMP in terms of repeatability and deflects in patterned wafers. Especial1y, dishing and erosion defects increase the resistance because they decrease the interconnection section area, and ultimately reduce the lifetime of the semiconductor. Methods to reduce dishing & erosion have recently been interface hardness of the pad, optimization of the pattern structure as dummy patterns. Dishing & erosion are initially generated an uneven pressure distribution in the materials. These defects are accelerated by free abrasives and chemical etching. Therefore, it is known that dishing & erosion can be reduced by minimizing the abrasive concentration. Minimizing the abrasive concentration by using CeO$_2$is the best solution for reducing dishing & erosion and for removal rate. This paper introduce dishing & erosion generating mechanism and a method fur developing a semi-rigid abrasive pad to minimize dishing & erosion during CMP.

• Journal of the korean society of oceanography
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• 제36권1호
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• pp.9-18
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• 2001

Chemical speciation of five heavy metals (Cr, Cu, Ni, Pb, Zn) has been analyzed from 37 surface and 2 core sediments of Kyeonggi Bay, using the modified sequential extraction method based on Tessier et at. (1979). The results show that heavy metals in the Kyeonggi Bay surface sediments are associated dominantly with the crystal lattice fraction. But in the polluted sediments of the Incheon North Harbor, the importance of the labile fractions increased while that of the lattice fraction decreased. In particular, the adsorbed and the easily reducible fractions showed a noticeable increase. In the core samples emerged a speciation pattern which differed significantly from that of the surface sediments. A sharp increase in the percentage of the reducible and organic/sulfide fractions and a decrease in the lattice fraction were observed. Throughout the vertical column, however, the metal contents in the lattice fraction showed stability while those of the labile fractions showed an upward increase. The strong association of heavy metals with the organic/sulfide fraction could be attributed in part to the sulfate reduction prevailing in the polluted harbor sediments.

• Smart Structures and Systems
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• 제28권6호
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• pp.727-735
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• 2021

Recently, non-destructive health monitoring methods such as magnetic flux leakage (MFL) method, have become popular due to their advantages over destructive methods. Currently, numerical study on this field has been limited to simplified studies by only obtaining MFL instead of induced voltage inside coil sensor. In this study, it was proposed to perform a novel numerical simulation of MFL's coil sensor by considering vital parameters including specimen's motion with constant velocity and saturation status of specimen in time domain. A steel-rod specimen with two stepwise cross-sectional changes (i.e., 21% and 16%) was fabricated using low carbon steel. In order to evaluate the results of numerical simulation, an experimental test was also conducted using a magnetic probe, with same size specimen and test parameters, exclusively. According to comparative results of numerical simulation and experimental test, similar signal amplitude and signal pattern were observed. Thus, proposed numerical simulation method can be used as a reliable source to check efficiency of sensor probe when different size specimens with different defects should be inspected.