• Title/Summary/Keyword: Materials testing

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Dedicated preparation for in situ transmission electron microscope tensile testing of exfoliated graphene

  • Kim, Kangsik;Yoon, Jong Chan;Kim, Jaemin;Kim, Jung Hwa;Lee, Suk Woo;Yoon, Aram;Lee, Zonghoon
    • Applied Microscopy
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    • v.49
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    • pp.3.1-3.7
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    • 2019
  • Graphene, which is one of the most promising materials for its state-of-the-art applications, has received extensive attention because of its superior mechanical properties. However, there is little experimental evidence related to the mechanical properties of graphene at the atomic level because of the challenges associated with transferring atomically-thin two-dimensional (2D) materials onto microelectromechanical systems (MEMS) devices. In this study, we show successful dry transfer with a gel material of a stable, clean, and free-standing exfoliated graphene film onto a push-to-pull (PTP) device, which is a MEMS device used for uniaxial tensile testing in in situ transmission electron microscopy (TEM). Through the results of optical microscopy, Raman spectroscopy, and TEM, we demonstrate high quality exfoliated graphene on the PTP device. Finally, the stress-strain results corresponding to propagating cracks in folded graphene were simultaneously obtained during the tensile tests in TEM. The zigzag and armchair edges of graphene confirmed that the fracture occurred in association with the hexagonal lattice structure of graphene while the tensile testing. In the wake of the results, we envision the dedicated preparation and in situ TEM tensile experiments advance the understanding of the relationship between the mechanical properties and structural characteristics of 2D materials.

Distribution of Korean Syllables by Characters

  • Lee, Soon-Hyang
    • Speech Sciences
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    • v.9 no.1
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    • pp.185-192
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    • 2002
  • This study classifies Korean syllables into various types and investigates the distribution of syllables by each type. Korean syllables are classified into four or eight types. In this study, they are classified into thirty-two types based on character combination in order to evaluate the intelligibility of Korean synthetic syllables. Among those Korean syllables derived from the possible combinations of Korean characters, only currently used syllables were selected. Based on this classification and distribution, representative and diagnosable testing materials can be made. These testing materials can be applicable to intelligibility tests of Korean synthetic syllables.

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A Study on the Microdefect Detection of Semiconductor Package by Digital Ultrasonic Image Processing (디지탈 초음파 화상처리에 의한 반도체 패키지의 미소결함 검출에 관한 연구)

  • Kim, J.Y.;Han, E.K.
    • Journal of the Korean Society for Nondestructive Testing
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    • v.10 no.2
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    • pp.43-49
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    • 1990
  • Ultrasonic testing is one of the most useful NDT method for detection of microdefect in the opaque materials. Recently, many applications of the ultrasonic techniques have been extended widely in the new field like electron is and advanced materials. From the result of the experiment, we have hardly found out a crack in the internal parts of the resin and a delamination between chip and resin because of poor performance of the system.

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Effect of pH and Concentration on Electrochemical Corrosion Behavior of Aluminum Al-7075 T6 Alloy in NaCl Aqueous Environment

  • Raza, Syed Abbas;Karim, Muhammad Ramzan Abdul;Shehbaz, Tauheed;Taimoor, Aqeel Ahmad;Ali, Rashid;Khan, Muhammad Imran
    • Journal of Electrochemical Science and Technology
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    • v.13 no.2
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    • pp.213-226
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    • 2022
  • In the present study, the corrosion behavior of aluminum Al-7075 tempered (T-6 condition) alloy was evaluated by immersion testing and electrochemical testing in 1.75% and 3.5% NaCl environment at acidic, neutral and basic pH. The data obtained by both immersion tests and electrochemical corrosion tests (potentiodynamic polarization and electrochemical impedance spectroscopy tests) present that the corrosion rate of the alloy specimens is minimum for the pH=7 condition of the solution due to the formation of dense and well adherent thin protective oxide layer. Whereas the solutions with acidic and alkaline pH cause shift in the corrosion behavior of aluminum alloy to more active domains aggravated by the constant flux of acidic and alkaline ions (Cl- and OH-) in the media which anodically dissolve the Al matrix in comparison to precipitated intermetallic phases (cathodic in nature) formed due to T6 treatment. Consequently, the pitting behavior of the alloy, as observed by cyclic polarization tests, shifts to more active regions when pH of the solutions changes from neutral to alkaline environment due to localized dissolution of the matrix in alkaline environment that ingress by diffusion through the pores in the oxide film. Microscopic analysis also strengthens the results obtained by immersion corrosion testing and electrochemical corrosion testing as the study examines the corrosion behavior of this alloy under a systematic evaluation in marine environment.

Detection of Subsurface Defects in Metal Materials Using Infrared Thermography; Image Processing and Finite Element Modeling

  • Ranjit, Shrestha;Kim, Won Tae
    • Journal of the Korean Society for Nondestructive Testing
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    • v.34 no.2
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    • pp.128-134
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    • 2014
  • Infrared thermography is an emerging approach to non-contact, non-intrusive, and non-destructive inspection of various solid materials such as metals, composites, and semiconductors for industrial and research interests. In this study, data processing was applied to infrared thermography measurements to detect defects in metals that were widely used in industrial fields. When analyzing experimental data from infrared thermographic testing, raw images were often not appropriate. Thus, various data analysis methods were used at the pre-processing and processing levels in data processing programs for quantitative analysis of defect detection and characterization; these increased the infrared non-destructive testing capabilities since subtle defects signature became apparent. A 3D finite element simulation was performed to verify and analyze the data obtained from both the experiment and the image processing techniques.

Dog bone shaped specimen testing method to evaluate tensile strength of rock materials

  • Komurlu, Eren;Kesimal, Ayhan;Demir, Aysegul Durmus
    • Geomechanics and Engineering
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    • v.12 no.6
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    • pp.883-898
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    • 2017
  • To eliminate the holding and gluing problems making the direct tensile strength test hard to be applied, a new method of testing specimens prepared using lathe machine to make the dog bone shape is assessed whether it could be applied to determine accurate direct tensile strength values of rock materials. A series of numerical modelling analyses was performed using finite element method to investigate the effect of different specimen and steel holder geometries. In addition to numerical modelling study, a series of direct tensile strength tests was performed on three different groups of rock materials and a rock-like cemented material to compare the results with those obtained from the finite element analyses. A proper physical property of the lathed specimens was suggested and ideal failure of the dog bone shaped specimens was determined according to the results obtained from this study.

Experimental Study on Wear Characteristics of Metallic Materials used in Oil Sands Plants (오일샌드 플랜트용 금속소재의 마모 특성에 대한 실험적 연구)

  • Won, Sung-Jae;Cho, Seung-Hyun;Kang, Dae-Kyung;Heo, Joong-Sik
    • Tribology and Lubricants
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    • v.33 no.1
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    • pp.31-35
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    • 2017
  • Recently, international attention has been focused on the development of non-traditional energy resources such as shale gas and oil sands, due to the steep increase in the demand for natural resources. The materials incorporated in an oil gas plant module experience extreme environments, and are prone to various problem such as fracture, corrosion and abrasion due to low-temperature brittleness. In order to improve the plant life, it is necessary to perform characteristics study and performance evaluation of the materials. In particular, this paper explains the main set of materials which are most frequently used in oil sands plant project. In order to investigate wear characteristics, the authors carried out abrasive wear tests of TP 316, stainless steel and SS 400, structural rolled steel. For the analysis of the abrasive wear resistance of an oil sands plant, the authors carried out the test according to ASTM G 105 "Standard Test Method for Conducting Wet Sand/Rubber Wheel Abrasion Test" standard guidelines. The authors have derived the results from the data associated with the loss of mass with respect to wear rate. During the test, for a given wear length for 10,000 revolutions, the rotational speed and applied force of the rubber wheel were varied.

Polycrystalline Ceramic Fibers by Extrusion

  • Sagesser, Peter;Wegmann, Markus;Gut, Beat;Berroth, Karl;,
    • The Korean Journal of Ceramics
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    • v.4 no.4
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    • pp.382-386
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    • 1998
  • titanate and a silicon carbide/zirconium diboride particulate composite have each been blended with thermoplastic of aqueous binders and extruded. The green extrudates have diameters ranging between 50 and 150 ㎛ and polyethylene-base 150 ${\mu}m$ diameter fibers can be drawn down at elevated temperature to approximately 40 ${\mu}m$ diameter. Hollow fibers with 150${\mu}m$ outer and 90 ${\mu}m$ inner diameter can also be fabricated. Green fibers have been processed into chopped fiber felts for use as gas distributors/current collectors in an experimental solid oxide fuel cell (SOFC) and the first attempts at producing simple textile structures have been successful. The fibers, tubes and felts have been successfully debound and sintered and characterization of the sintered PSZ fibers, for example, has revealed a density in excess of 99% and tensile failure stresses up to 1.0 GPa for 78 ${\mu}m$ diameter fibers.

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Wireless sensor networks for long-term structural health monitoring

  • Meyer, Jonas;Bischoff, Reinhard;Feltrin, Glauco;Motavalli, Masoud
    • Smart Structures and Systems
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    • v.6 no.3
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    • pp.263-275
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    • 2010
  • In the last decade, wireless sensor networks have emerged as a promising technology that could accelerate progress in the field of structural monitoring. The main advantages of wireless sensor networks compared to conventional monitoring technologies are fast deployment, small interference with the surroundings, self-organization, flexibility and scalability. These features could enable mass application of monitoring systems, even on smaller structures. However, since wireless sensor network nodes are battery powered and data communication is the most energy consuming task, transferring all the acquired raw data through the network would dramatically limit system lifetime. Hence, data reduction has to be achieved at the node level in order to meet the system lifetime requirements of real life applications. The objective of this paper is to discuss some general aspects of data processing and management in monitoring systems based on wireless sensor networks, to present a prototype monitoring system for civil engineering structures, and to illustrate long-term field test results.