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Evaluation of Marginal and Internal Integrity of Modified Resin-Bonded Fixed Partial Dentures: An In Vitro Study

  • Ahn, Sung-Hyeon;Choi, Jae-Won;Jeon, Yong-Chan;Jeong, Chang-Mo;Yoon, Mi-Jung;Lee, So-Hyoun;Huh, Jung-Bo
    • Journal of Korean Dental Science
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    • v.10 no.1
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    • pp.29-34
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    • 2017
  • Purpose: The purpose of this study was to evaluate the microleakage of various types of resin-bonded fixed partial dentures (RBFPDs) after artificial aging. Materials and Methods: Forty models with missing first molar were fabricated using artificial resin teeth and were divided into four groups: Group A, conventional RBFPDs design; Group B, modified RBFPDs design; Group C, assembled 3-piece RBFPDs design; and Group D, assembled 3-piece RBFPDs with different occlusal rest positions. Half of the specimens underwent chewing simulation process (240,000 cycles, 50 N load, 1.7 Hz) and thermocycling (temperatures $5^{\circ}C{\sim}55^{\circ}C$, dwelling time 30 seconds) and the remaining 20 specimens didn't receive any treatment. All the specimens were immersed in 2% methylene blue solution for 24 hours to evaluate microleakage, and were sectioned at the middle part of abutment teeth. To evaluate the microleaskage, a dye penetration was calculated. Result: With artificial aging, cyclic loading and thermocycling, a 3-piece RBPFD and a 2-piece RBPFD using original tooth undercuts have significantly lower microleakge (P<0.05) compared to the conventional design of RBPFD and modified RBPFD. Conclusion: Within the limit of this experiment, the assembled RBFPDs exhibited a smaller microleakage than the conventional RBFPDs, implying that the assembled RBFPDs can be more effective for reducing the dislodgement of the RBFPDs.

Development of a Multifunctional Design Concept to Improve Constructed Wetland Performance (인공습지의 성능향상을 위한 다기능 설계기법 개발)

  • Reyes, N.J.D.G.;Choi, H.S.;Kim, L.H.
    • Journal of Wetlands Research
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    • v.22 no.2
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    • pp.161-170
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    • 2020
  • Constructed wetlands (CWs) are widely used to solve water quality problems caused by diffuse pollution from agricultural areas; however, phytoplankton blooms in CW systems can occur due to long hydraulic retention time (HRT), high nutrient loading, and exposure to sunlight. This study was conducted to evaluate the efficiency of a CW designed to treat agricultural diffuse pollution and develop a design concept to improve the nature-based capabilities of the system. Monitoring was conducted to assess contribution of individual wetland components (i.e. water, sediments, and plants) in the treatment performance of the system. During dry days, the turbidity and particulates concentration in the CW increased by 80 to 197% and 10 to 87%, respectively, due to the excessive growth of phytoplankton. On storm events, the concentration of particulates, organics, and nutrients were reduced by 43% to 70%, 22% to 49%, and 15% to 69% due to adequate water circulation and constant flushing of pollutants in the system. Based on the results, adequate water circulation is necessary to improve the performance of the CW. Free water surface CWs are usually designed to have a constant water level; however, the climate in South Korea is characterized by distinct dry and rainy seasons, which may not be suitable for this conventional design. This study presented a concept of multifunctional design in order to solve current CW design problems and improve the flood control, water quality management, and environmental functions of the facility.

Pretreatment of Rice Straw by Using Ammonia Recycled Percolation Process (암모니아 재순환 침출공정을 이용한 볏짚의 전처리)

  • Kang, Choon-Hyoung
    • Korean Chemical Engineering Research
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    • v.47 no.1
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    • pp.89-95
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    • 2009
  • Because of high contents of cellulose (~37 wt%) and hemicellulose (~17%), rice straw seems to be a potential lignocellulosic biomass for production of bioethanol. In this study, Ammonia Recycled Percolation (ARP) pretreatment of rice straw was extensively investigated. In particular, the experimental study included the effects of temperature, reaction time and concentration of ammonia on compositions and enzymatic digestibility of the resulting solid residues; the ranges of pretreatment conditions were, in turn, $150{\sim}190^{\circ}C$, 10~90 min and 0~20 wt%. Through ARP pretreatment, the lignin content was reduced by as high as ~84% while 20~80% of the hemicellulose was also solubilized. The solid residue resulted from the pretreatment with 15 wt% aqueous ammonia solution at $170^{\circ}C$ for 90 mim showed as high as ~90% of digestibility with 15FPU/g of glucan enzyme loading. Supplement of xylanese to cellulase led to a notable enhancement of digestibility, indicating a discernable inhibitory role of hemicellulose. Simultaneous Saccharification and Fermentation (SSF) and Simultaneous Saccharification and Co-Fermentation (SSCF) were performed to obtain ethanol productions of 13.8 g/L (corresponding to 81% yield) and 15 g/L (corresponding to 89% yield), respectively.

THE EFFECT OF CONSISTENCY OF SEALER ON CANAL OBTURATION IN INJECTION-THERMOPLASTICIZED GUlTA-PERCHA METHOD (연화(軟化) Gutta-percha 충전법(充塡法)에서 Sealer의 조도(稠度)가 근관폐쇄(根管閉鎖)에 미치는 영향(影響))

  • Lee, Young-Ho
    • Restorative Dentistry and Endodontics
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    • v.14 no.2
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    • pp.38-48
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    • 1989
  • The purpose of this study was to investigate the proper consistency of root canal sealer needed in obtaining an efficient canal obturation in injection-thermoplasticized low-temperature ($70^{\circ}C$) gutta-percha method. The sealer was made by incorporating zinc oxide powder into $0.5m{\ell}$ of eugenol and then the $0.5m{\ell}$ of mixture slurry was placed between two flat glass plates. The consistency was determined by measuring the degree of spread of the slurry at loading the 120gm of weight from the top plate. The sealer was prepared according to P/L ratio corresponding to the acquired consistency of 65.45mm, 46.80mm, 28.95mm and 22.60mm. The distal roots were obtained by cutting off from 125 extracted human lower molars and the root canals were prepared by using step-back method. The prepared canals were coated with the sealers on their walls and obturated by using the injection-thermoplasticized low-temperature ($70^{\circ}C$) gutta-percha method. All specimens were immersed in 2% methylene blue dye solution for 48 hours at $37^{\circ}C$. Calipers was used to measured the dye penetration into the root canals from apical constrictions. The results were as follows : The canals obturated without sealer showed significantly more leakage than the canals obturated with sealer. Within the consistency from 65.45mm to 22.60mm, the sealer of 65.45mm appeared significantly better than that of 28.95mm and 22.60mm in the canals obturated by injection-thermoplasticized gutta-percha method, and better than that of 46.80mm without statistical significance.

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Reliability and Validity of the Korean Version of the Fear of Daily Activities Questionnaire for Patients with Low Back Pain (허리통증 환자의 한국판 일상동작 공포설문지의 신뢰도와 타당도)

  • Cha, Yong-Jun;Kim, Kyoung
    • The Journal of the Korea Contents Association
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    • v.11 no.5
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    • pp.224-232
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    • 2011
  • The purpose of this study was to test the reliability and validity of the Korean version of the fear of daily activities questionnaire (FDAQ) for low back pain patients. Seventy-three subjects with low back pain were participated in this study. The subjects completed ten standardized self-administered questionnaires that measure fear of specific daily activities. The reliability of the acquired data was determined by the intra-class correlation coefficient (ICC) and the Cronbach's ${\alpha}$ for internal consistency. Constructive validity was analyzed by factor analysis, and concurrent validity was acquired from comparison FDAQ scores to the visual analogue scale (VAS) and Oswestry disability index (ODI) scores. The test-retest reliability of the Korean version of the FDAQ showed good ICC (2,1)= 0.96 (95%CI 0.94.0.98) and Cronbach's alpha value was 0.93. Factor analysis suggested two factors solution consisting of spinal loading and spinal movement/posture, it explained 76.1% of the total variance. The concurrent validity was moderately related with pain and disability. Therefore, the Korean version of the FDAQ is a useful method for measuring the fear of daily activities of patients with low back pain.

Solar Photochemical Degradation and Toxicity Reduction of Trichloroethlylene (TCE) (Trichloroethlylene (TCE)의 광화학적 분해 및 독성 저감)

  • Park, Jae-Hong;Kwon, Soo Youl
    • Clean Technology
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    • v.12 no.4
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    • pp.244-249
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    • 2006
  • The photocatalytic degradation of trichloroethlylene (TCE), has been investigated over $TiO_2$ photocatalysts irradiated with solar light. The effect of operational parameters, i.e., initial TCE concentration, $TiO_2$ concentration, pH and additives ($H_2O_2$, persulphate($S_2O{_8}^-$)) on the degradation rate of aqueous solution of TCE has been examined. The results presented in this work demonstrated that degradation of the TCE with $TiO_2/solar$ light was enhanced by augumentation in $TiO_2$ loading, pH, and adding additives but was inhibited by increase in initial TCE concentration. Also individual use of $H_2O_2$ was far more effective than using persulphate in TCE removal efficiency. Furthermore, the relative toxicity with a $solar/TiO_2/H_2O_2$ system was about 15% lower than with a $solar/TiO_2/persulphate$ system and about 35% lower than with a $solar/TiO_2$ system within a reaction time of 150 min, respectively.

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Exact Solutions for Vibration and Buckling of Rectangular Plates Loaded at Two Simply-Supported Opposite Edges by In-Plane Moments, Free along the Other Two Edges (면내(面內) 모멘트를 받는 단순지지된 두 모서리와 자유경계인 나머지 두 모서리를 갖는 직사각형 판의 진동과 좌굴의 엄밀해)

  • Shim, Hyun-Ju;Woo, Ha-Young;Kang, Jae-Hoon
    • Journal of Korean Association for Spatial Structures
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    • v.6 no.4 s.22
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    • pp.81-92
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    • 2006
  • This paper presents exact solutions for the free vibrations and buckling of rectangular plates having two opposite, simply supported edges subjected to linearly varying normal stresses causing pure in-plane moments, the other two edges being free. Assuming displacement functions which are sinusoidal in the direction of loading (x), the simply supported edge conditions are satisfied exactly. With this the differential equation of motion for the plate is reduced to an ordinary one having variable coefficients (in y). This equation is solved exactly by assuming power series in y and obtaining its proper coefficients (the method of Frobenius). Applying the free edge boundary conditions at y=0, b yields a fourth order characteristic determinant for the critical buckling moments and vibration frequencies. Convergence of the series is studied carefully. Numerical results are obtained for the critical buckling moments and some of their associated mode shapes. Comparisons are made with known results from less accurate one-dimensional beam theory. Free vibration frequency and mode shape results are also presented. Because the buckling and frequency parameters depend upon Poisson's ratio ( V ), results are shown for $0{\leq}v{\leq}0.5$, valid for isotropic materials.

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Surface Chemistry in Biocompatible Nanocolloidal Particles (생체 적합한 나노입자와 계면화학)

  • Kim Jong-Duk;Jung Jae Hyun
    • Journal of the Society of Cosmetic Scientists of Korea
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    • v.30 no.3 s.47
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    • pp.295-305
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    • 2004
  • Colloid and surface chemistry have been focused on surface area and surface energy. Local surface properties such as surface density, interaction, molecular orientation and reactivity have been one of interesting subjects. Systems of such surface energy being important would be listed as association colloid, emulsion, particle dispersion, foam, and 2-D surface and film. Such nanoparticle systems would be applied to drug delivery systems and functional cosmetics with biocompatible and degradable materials, while nanoparticles having its size of several nm to micron, and wide surface area, have been accepted as a possible drug carrier because their preparation, characteristics and drug loading have been inves-tigated. The biocompatible carriers were also used for the solubilization of insoluble drugs, the enhancement of skin absorption, the block out of UV radiation, the chemical stabilization and controlled release. Nano/micro emulstion system is classified into nano/microsphere, nano/microcapsule, nano/microemulsion, polymeric micelle, liposome according to its prep-aration method and size. Specially, the preparation method and industrial applications have been introduced for polymeric micelles self-assembled in aqueous solution, nano/microapsules controlling the concentration and activity of high concen-tration and activity materials, and monolayer or multilayer liposomes carrying bioactive ingredients.

Transparent Polyimide Nanocomposite Films with Various Equi-biaxial Stretching Ratios (다양한 이축연신 비율에 따른 투명 폴리이미드 나노복합체 필름)

  • Kim, Young-Min;Chang, Jin-Hae
    • Polymer(Korea)
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    • v.36 no.4
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    • pp.478-485
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    • 2012
  • A series of transparent polyimide (PI) nanocomposite films was synthesized from bicyclo(2,2,2)oct-7-ene-2,3,5,6-tetracarboxylic dianhydride (BTDA) and 1,3-bis(3-aminophenoxy)benzene (BAPB) with various organoclay contents via solution intercalation polymerization to poly(amic acid)s, followed by thermal imidization. Varying organoclay loading in a range of 0 to 1.5 wt% produced variations in the optical transparency, morphology, and oxygen barrier property of the hybrids. An optimum oxygen barrier property was observed for the hybrids containing 1.0 wt% Cloisite 30B; these properties were degraded gradually by further increases in the clay content. The PI hybrid films were found to exhibit excellent optical transparency and almost no color. However, the transparency of the hybrid films decreased slightly with increasing organoclay content. Transparent PI hybrid films containing 1.0 wt% Cloisite 30B were stretched equi-biaxially with various stretching ratios in a range of 100-140% to investigate their optical transparency and oxygen permeability in detail; the variations of clay dispersion and morphology were also determined as a function of equi-biaxial stretching ratio. PI hybrid films with ${\geq}120%$ stretching were found to contain homogeneously dispersed clay in the polymer matrix and exfoliated nanocomposites. The highest barrier to oxygen permeation was found at an equi-biaxial stretching ratio of 130%.

Bio-Derived Poly(${\gamma}$-Glutamic Acid) Nanogels as Controlled Anticancer Drug Delivery Carriers

  • Bae, Hee Ho;Cho, Mi Young;Hong, Ji Hyeon;Poo, Haryoung;Sung, Moon-Hee;Lim, Yong Taik
    • Journal of Microbiology and Biotechnology
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    • v.22 no.12
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    • pp.1782-1789
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    • 2012
  • We have developed a novel type of polymer nanogel loaded with anticancer drug based on bio-derived poly(${\gamma}$-glutamic acid) (${\gamma}$-PGA). ${\gamma}$-PGA is a highly anionic polymer that is synthesized naturally by microbial species, most prominently in various bacilli, and has been shown to have excellent biocompatibility. Thiolated ${\gamma}$-PGA was synthesized by covalent coupling between the carboxyl groups of ${\gamma}$-PGA and the primary amine group of cysteamine. Doxorubicin (Dox)-loaded ${\gamma}$-PGA nanogels were fabricated using the following steps: (1) an ionic nanocomplex was formed between thiolated ${\gamma}$-PGA as the negative charge component, and Dox as the positive charge component; (2) addition of poly(ethylene glycol) (PEG) induced hydrogen-bond interactions between thiol groups of thiolated ${\gamma}$-PGA and hydroxyl groups of PEG, resulting in the nanocomplex; and (3) disulfide crosslinked ${\gamma}$-PGA nanogels were fabricated by ultrasonication. The average size and surface charge of Dox-loaded disulfide cross-linked ${\gamma}$-PGA nanogels in aqueous solution were $136.3{\pm}37.6$ nm and $-32.5{\pm}5.3$ mV, respectively. The loading amount of Dox was approximately 38.7 ${\mu}g$ per mg of ${\gamma}$-PGA nanogel. The Dox-loaded disulfide cross-linked ${\gamma}$-PGA nanogels showed controlled drug release behavior in the presence of reducing agents, glutathione (GSH) (1-10 mM). Through fluorescence microscopy and FACS, the cellular uptake of ${\gamma}$-PGA nanogels into breast cancer cells (MCF-7) was analyzed. The cytotoxic effect was evaluated using the MTT assay and was determined to be dependent on both the concentration and treatment time of ${\gamma}$-PGA nanogels. The bio-derived ${\gamma}$-PGA nanogels are expected to be a well-designed delivery carrier for controlled drug delivery applications.