• Title/Summary/Keyword: Limit of Detection

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Determination of 105 pesticide residues by GC/MS/MS (GC/MS/MS를 이용한 105종의 잔류농약 분석에 관한 연구)

  • Kim, W.S.;Do, J.A.;Lee, H.J.;Lee, J.Y.;Yang, S.J.;Lee, S.H.
    • Analytical Science and Technology
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    • v.23 no.4
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    • pp.395-404
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    • 2010
  • A multi-residual method using gas chromatography coupled with mass spectrometry (GC/MS/ MS) was developed for the analysis of 105 pesticides. This method was tested on lemons, beans and other vegetables. The pretreatment of these pesticides was performed by liquid-liquid partition followed by cleanup with solid phase extraction cartridge (SPE Florisil), after acetonitrile extraction from matrices and sodium chloride (15 g) addition. The recovery ranged from 71.1% to 126.0% except for azinphosmethyl, famoxadone, fenamidone, flufenoxuron and triadimefon in lemons and from 72.5% to 124.5% in bean. In lemon, the limit of detection (LOD) and limit of quantification (LOQ) were 0.001~150 ng/ mL and 0.004~500 ng/mL, respectively.

A Study on Non-propagating Crack in Fatigue Behavior of Pure Titanium (공업용 순 티타늄의 피로거동에서 정류균열에 관한 연구)

  • Kim, Dong-Yeol;Kim, Jin-Hak;Kim, Min-Geon
    • Transactions of the Korean Society of Mechanical Engineers A
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    • v.24 no.4 s.175
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    • pp.1001-1006
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    • 2000
  • To verify the existing theory, non-propagating crack(NPC) does not exist in Ti which fulfills the good conditions for being of NPC, NPC detection in Ti was tried out. Also, the conception of fatigue limit in Ti and a main cause for NPC being were inquired. NPC was detected in both sharp notch root ( $\rho$=0.02mm) and micro pit (diameter = 0.25mm) which held fast to the end under stressing of fatigue limit. Therefore, the existing theory was identified as mistake. But, NPC can not be detected in smooth specimen. This fact would be due to the presumption that NPC is very small or crack does not initiate in smooth specimen. Anyway, the fatigue limit of Ti does not correspond to critical stress of crack initiation but correspond to critical stress of NPC growth. Measurement on the COD of NPC in Ti showed that the crack tip was closed even under the peak stress level at fatigue limit. But, after stress relieving annealing crack tip was opened. Consequently, compressive residual stress which is induced around the crack tip is considered to be the factor causing the NPC being.

Multiple-Background Model-Based Object Detection for Fixed-Embedded Surveillance System (고정형 임베디드 감시 카메라 시스템을 위한 다중 배경모델기반 객체검출)

  • Park, Su-In;Kim, Min Young
    • Journal of Institute of Control, Robotics and Systems
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    • v.21 no.11
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    • pp.989-995
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    • 2015
  • Due to the recent increase of the importance and demand of security services, the importance of a surveillance monitor system that makes an automatic security system possible is increasing. As the market for surveillance monitor systems is growing, price competitiveness is becoming important. As a result of this trend, surveillance monitor systems based on an embedded system are widely used. In this paper, an object detection algorithm based on an embedded system for a surveillance monitor system is introduced. To apply the object detection algorithm to the embedded system, the most important issue is the efficient use of resources, such as memory and processors. Therefore, designing an appropriate algorithm considering the limit of resources is required. The proposed algorithm uses two background models; therefore, the embedded system is designed to have two independent processors. One processor checks the sub-background models for if there are any changes with high update frequency, and another processor makes the main background model, which is used for object detection. In this way, a background model will be made with images that have no objects to detect and improve the object detection performance. The object detection algorithm utilizes one-dimensional histogram distribution, which makes the detection faster. The proposed object detection algorithm works fast and accurately even in a low-priced embedded system.

Fundamental Study on the Limit of Thermographic Survey Applied to Detection of Void in Concrete (적외선법을 이용한 콘크리트 공동의 적용한계에 관한 기초적 연구)

  • ;Tanigawa Yasuo
    • Proceedings of the Korea Concrete Institute Conference
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    • 1999.04a
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    • pp.799-806
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    • 1999
  • This study describes the results of experiment and numerical analysis for heating image by thermographic method when the size of void in concrete are changed. By comparing analytical solution by finite element method with measured image by thermography, the relationships between the surface temperature which can be confirmed by this method, the size of void and optimum time for detection of void and the difference of temperature are cleared.

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Real-Time Voltammetric Assay of Lead Ion in Biological Cell Systems

  • Ly, Suw-Young
    • Toxicological Research
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    • v.25 no.4
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    • pp.231-235
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    • 2009
  • Trace lead detection for cyclic voltammetry (CV) and square-wave (SW) stripping voltammetry was performed using mercury immobilized onto a carbon nanotube electrode (HNPE). Using the characteristics of mercury and the catalytic carbon nanotube structure, a modified technique, the $0.45{\mu}g/l$ detection limit of lead ion was attained. The developed method can be applied to pond water, fish tissue, plant tissue, and in vivo direct assay.

Supervised classification for greenhouse detection by using sharpened SWIR bands of Sentinel-2A satellite imagery

  • Lim, Heechang;Park, Honglyun
    • Journal of the Korean Society of Surveying, Geodesy, Photogrammetry and Cartography
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    • v.38 no.5
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    • pp.435-441
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    • 2020
  • Sentinel-2A satellite imagery provides VNIR (Visible Near InfraRed) and SWIR (ShortWave InfraRed) wavelength bands, and it is known to be effective for land cover classification, cloud detection, and environmental monitoring. Greenhouse is one of the middle classification classes for land cover map provided by the Ministry of Environment of the Republic of Korea. Since greenhouse is a class that has a lot of changes due to natural disasters such as storm and flood damage, there is a limit to updating the greenhouse at a rapid cycle in the land cover map. In the present study, we utilized Sentinel-2A satellite images that provide both VNIR and SWIR bands for the detection of greenhouse. To utilize Sentinel-2A satellite images for the detection of greenhouse, we produced high-resolution SWIR bands applying to the fusion technique performed in two stages and carried out the detection of greenhouse using SVM (Support Vector Machine) supervised classification technique. In order to analyze the applicability of SWIR bands to greenhouse detection, comparative evaluation was performed using the detection results applying only VNIR bands. As a results of quantitative and qualitative evaluation, the result of detection by additionally applying SWIR bands was found to be superior to the result of applying only VNIR bands.

Nanosecond Gated Raman Spectroscopy for Standoff Detection of Hazardous Materials

  • Chung, Jin Hyuk;Cho, Soo Gyeong
    • Bulletin of the Korean Chemical Society
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    • v.35 no.12
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    • pp.3547-3552
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    • 2014
  • Laser Raman spectroscopy is one of the most powerful technologies for standoff detection of hazardous materials including explosives. Supported by recent development of laser and sensitive ICCD camera, the technology can identify trace amount of unknown substances in a distance. Using this concept, we built a standoff detection system, in which nanosecond pulse laser and nanosecond gating ICCD technique were delicately devised to avoid the large background noise which suppressed weak Raman signals from the target sample. In standoff detection of explosives which have large kill radius, one of the most important technical issues is the detection distance from the target. Hence, we focused to increase the detection distance up to 54 m by careful optimization of optics and laser settings. The Raman spectra of hazardous materials observed at the distance of 54 m were fully identifiable. We succeeded to detect and identify eleven hazardous materials of liquid or solid particles, which were either explosives or chemical substances used frequently in chemical plants. We also performed experiments to establish the limit of detection (LOD) of HMX at 10 m, which was estimated to be 6 mg.

Rapid and Sensitive Detection of Hepatitis C Virus in Clinical Blood Samples Using Reverse Transcriptase Polymerase Spiral Reaction

  • Sun, Wenying;Du, Ying;Li, Xingku;Du, Bo
    • Journal of Microbiology and Biotechnology
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    • v.30 no.3
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    • pp.459-468
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    • 2020
  • This study established a new polymerase spiral reaction (PSR) that combines with reverse transcription reactions for HCV detection targeting 5'UTR gene. To avoid cross-contamination of aerosols, an isothermal amplification tube (IAT), as a separate containment control, was used to judge the result. After optimizing the RT-PSR reaction system, its effectiveness and specificity were tested against 15 different virus strains which included 8 that were HCV positive and 7 as non-HCV controls. The results showed that the RT-PSR assay effectively detected all 8 HCV strains, and no false positives were found among the 7 non-HCV strains. The detection limit of our RT-PSR assay is comparable to the real-time RT-PCR, but is more sensitive than the RT-LAMP. The established RT-PSR assay was further evaluated for detection of HCV in clinical blood samples, and the resulting 80.25% detection rate demonstrated better or similar effectiveness compared to the RT-LAMP (79.63%) and real-time RT-PCR (80.25%). Overall, the results showed that the RT-PSR assay offers high specificity and sensitivity for HCV detection with great potential for screening HCV in clinical blood samples.

System Capacity Analysis with the Retransmission Limit on ARQ in a Voice/Data DS-CDMA System

  • Lee, Chiho;Gwangzeen Ko;Kim, Kiseon
    • Proceedings of the IEEK Conference
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    • 2000.07a
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    • pp.513-516
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    • 2000
  • In this paper, we investigate the effect of the retransmission limit both the system capacity and the average number of retransmissions in a voice/data DS-CDMA system. Basically, we consider the IS-95 type reverse link of the CDMA system, which supports two kinds of services: a general voice and a packetized data service. ARQ is used for the reliable data transmission. Convolutional code is used for FEC and CRC-CCITT code is used for the error detection in ARQ. The result shows that the number of concurrent data users decreases as we reduce the number of the retransmissions. However, at the same time, we can also reduce the average number of retransmissions. Concluding1y, we can select the retransmission limit so as to reduce large amount of' retransmissions with small sacrifice in the system capacity.

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Detection Performance Improvement by Limit&STC Assembly Betterment of Surveillance Radar (천마 탐지레이더 Limit&STC 조립체 개선을 통한 탐지성능 향상)

  • Yoon, Jaebok;Kim, Siok;Keum, Jongju
    • Journal of the Korea Institute of Military Science and Technology
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    • v.19 no.1
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    • pp.1-8
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    • 2016
  • In this paper, we have described the performance improvement of surveillance radar to prevent damage or malfunction of surveillance radar RF head unit due to the strong reflections caused by artificial obstacles at close range. We have proposed a technique to improve the performance of the RF head unit as a solution to overcome the limitations of the operating system and improve radar performance. We have verified the effectiveness of the improvement by comparing the before and after results applied to actual system.