• Journal of Ceramic Processing Research
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• v.13 no.spc2
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• pp.394-397
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• 2012

In this work, we studied the influence of the dopant elements concentration on the properties of SnO2 thin films deposited by pulsed laser deposition. X-ray diffraction (XRD), field emission scanning electron microscopy (FE-SEM), Hall effect measurement and UV-Vis studies were performed to characterize the deposited films. XRD results showed that the films had polycrystalline nature with tetragonal rutile structure. FE-SEM micrographs revealed that the as deposited films composed of dense microstructures with uniform grain size distribution. All the films show n-type conduction and the best transparent conductive oxide (TCO) performance was obtained on 6 wt% Sb2O5 doped SnO2 film prepared at pO2 of 60mtorr and Ts of 500 ℃. Its resitivity, optical transmittance, figure of merit are 7.8 × 10-4 Ω cm, 85% and 1.2 × 10-2 Ω-1, respectively.

• Transactions on Electrical and Electronic Materials
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• v.15 no.5
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• pp.262-264
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• 2014

Pristine ZnO, 3 wt.% Ga-doped (3GZO) and 3 wt.% Ag-doped (3SZO) ZnO nanowires (NWs) were grown using the hot-walled pulse laser deposition (HW-PLD) technique. The doping of Ga and Ag in ZnO NWs was observed by analyzing the optical and chemical properties. We optimized the synthesis conditions, including processing temperature, time, gas flow, and distance between target and substrate for the growth of pristine and doped ZnO NWs. The diameter and length of pristine and doped ZnO NWs were controlled under 200 nm and several ${\mu}m$, respectively. Low temperature photoluminescence (PL) was performed to observe the optical property of doped NWs. We clearly observed the shift of the near band edge (NBE) emission by using low temperature PL. In the case of 3GZO and 3SZO NWs, the center photon energy of the NBE emissions shifted to low energy direction using the Burstein Moss effect. A strong donor-bound exciton peak was found in 3 GZO NWs, while an acceptor-bound exciton peak was found in 3SZO NWs. X-ray photoelectron spectroscopy (XPS) also indicated that the shift of binding energy was mainly attributed to the interaction between the metal ion and ZnO NWs.

• Laser Solutions
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• v.4 no.1
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• pp.21-28
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• 2001

Simulation on the electron beam welding of Al 2219 alloy was carried out by using commercial FEM code MARC, which encounters moving heat sources. Due to axisymmetry of geometry, a half of the cylinder was simulated. A coupled thermo-mechanical analysis was carried out and subroutine for heat flux was substituted in the program. The material properties such as specific heat, heat transfer coefficient and thermal expansion coefficient were given as a function of temperature and the latent heat associated with a given temperature range is considered. As a result, the proper beam power is 60㎸${\times}$60㎃ and welding speed is 1∼1.5 m/min. The residual stress in the heat-affected zone as well as the fusion zone does not increase. It is necessary to use jigs for preventing distortion of cylinder and improving weld quality.

• Journal of Powder Materials
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• v.31 no.1
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• pp.1-7
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• 2024

This study explores the profound impact of varying oxygen content on microstructural and mechanical properties in specimens HO and LO. The higher oxygen concentration in specimen HO is found to significantly influence alpha lath sizes, resulting in a size of 0.5-1 ㎛, contrasting with the 1-1.5 ㎛ size observed in specimen LO. Pore fraction, governed by oxygen concentration, is high in specimen HO, registering a value of 0.11%, whereas specimen LO exhibits a lower pore fraction (0.02%). Varied pore types in each specimen further underscore the role of oxygen concentration in shaping microstructural morphology. Despite these microstructural variations, the average hardness remains consistent at ~370 HV. This study emphasizes the pivotal role of oxygen content in influencing microstructural features, contributing to a comprehensive understanding of the intricate interplay between elemental composition and material properties.

• Design & Manufacturing
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• v.11 no.2
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• pp.37-41
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• 2017

With light vehicle weight gradually becoming ever more importance due to tightened exhaust gas regulations, hot-stamping processing using boron alloyed steel is being applied more and more by major automobile OEMs since process assures both moldability and a high strength of 1.5 GPa. Although laser trimming is generally applied to the post-processing of the hot-stamped process with high strength, there have been many studies of in-die hot trimming using shear dies during the quenching of material in order to shorten processing times. As such, this study investigated the effects of the Shear rate and Shear mechanism on shear processes during the quenching process of hot-stamping material. In case of pad variable, padding force is very weak compared with shear force, so it does not affect the shear surface. In case of shear rate, the higher the shear at high temperatures and the higher the friction effect. As a result the rollover and the fracture distribution decreased, and the burnish distribution increased. Therefore, it is considered that the shear quality is guaranteed when high shear rate is applied in high temperature shear process.

• The Journal of Korean Academy of Prosthodontics
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• v.45 no.3
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• pp.303-309
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• 2007

Statement of problem. The effect of gold electroforming on gold alloy was not studied. Purpose. This in vitro study investigate the effect of gold electroforming on gold-silver-palladium alloy. Material and methods. Three pieces of gold strips had undergone the electroforming procedures on one side and then half of the side again electroformed. The set mode for this study was program 1 ($200{\mu}m$). And the processing time was 15min (1/20 time to form $200{\mu}m$ coping). The confocal laser scanning microscope (PASCAL 5, Carl Zeiss, Bernried, Germany) was used to measure the thickness of the pure gold layer electroformed on the gold strips. Half of the gold strip was coated two times with electroformed gold, and the other half one time. The data from the cone focal laser system was processed to get the vertical profile of the strips and the difference of the vertical height between the double coated and single coated layer was regarded as the thickness of the gold coating. The layer thickness value to built 3D image of the cone-focal laser was set $0.5{\mu}m$. Next to the measurement of the thickness of the coating, the Vicker's hardness test was done. It was performed on the double coated surface, single coated surface and non-coated surface (back side) three times each. Results. The mean thickness value gained from gold electroforming technique was measured to be $22{\mu}m$ for sample 1, $23{\mu}m$ for sample 2, $21{\mu}m$ for sample 3. In the same condition of time, power and the amount of electrolyte, the data showed no difference between samples. According to the results of variance analysis, the differences among the variations in number of coating were statistically insignificant (p>0.05), meaning that the two times of gold electroforming coating did not change the hardness of gold-silver-palladium alloy. Conclusion. The test of thickness of gold coating proved the coherency of the gold electroforming procedure, in other words, when the power, the exposed surface area, processing time and the amount of electrolytes were set same, the same thickness of gold would be coated on. The hardness test showed that the electroformed gold coating did not change the hardness of the gold-silver-palladium alloy when it is coated not more than $45{\mu}m$.

• KIEE International Transactions on Electrophysics and Applications
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• v.4C no.2
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• pp.55-59
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• 2004

Throughout manufacturing processes, pulse shaping is required for material processing and it is regarded as an important (actor according to the specific characteristics of materials. Therefore, this study suggests a highly appropriate pulse shaping technique using a multi-switching method. This is a pulse superposition method in which one flash lamp can consecutively turn on by the double switching of the discharging system. It is possible to construct a variety of pulse shapes and pulse widths by the consecutive trigger of the silicon-controlled rectifiers (SCR) of a PIC (program integrated circuit) one-chip microprocessor. The use of this technique can provide a number of advantages to people who require suitable pulse shaping for particular applications such as welding, cutting, and drilling.

• Journal of the KSME
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• v.34 no.7
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• pp.539-545
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• 1994

레이저 가공은 60년대 초기 레이저가 기술적으로 가능해진 후 기초 연구단계를 거쳐 산업에 활 용되면서 활기를 띄기 시작하였다. 레이저 가공의 대표적인 것으로 절단을 꼽을 수 있으며 박 판절단의 경우 레이저는 이미 산업현장에서 굳건히 그 자리를 차지하고 있다. 레이저 용접의 경우에는 절단과 달리 기술적 문제점 등으로 인해 활용도가 낮은 편이나 점차 그 중요성이 인 식되고 있고 따라서 용접이 안고 있는 기술적 문제점을 해결하려는 연구개발과 기술적 시도가 활발히 추진되고 있다. 레이저 용접은 무엇보다도 자동화를 통해서만 활용이 가능하고 또한 이 로써 타 용접방법보다 경제적 우위를 점하게 된다. 따라서 용접을 이용한 대량생산품의 대표격인 자동차 제조에 레이저 용접을 활용하고자 하는 노력은 레이저 개발 이후 끊임없이 계속되었다. 레이저 용접의 활용이유는 이미 언급된 경제성외에도 경량화를 꼽을 수 있다. 본고에서는 레 이저 가공중 용접을 중심으로 구조물의 경량화 실례를 들어 방법을 제시하고, 이를 바탕으로 향후 폭넓게 적용될 수 있다는 가능성을 제시하고자 한다.

• Transactions of Materials Processing
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• v.20 no.6
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• pp.427-431
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• 2011

In general, hot stamped component is trimmed by costly and time consuming laser cutting when the material strength is over 1,500MPa. The aim of this work was to demonstrate that the trimming die life is improved and the trimming load is decreased by lowering the strength of the region to be trimmed. The model employed in this study was a hat shape, similar to the cross section of many hot stamped products. FE-analysis of hot stamping process was performed to evaluate the effect of tool shape on cooling rate at the area to be trimmed. The best tool shape was thus identified, which created slower cooling and lower hardness at the region to be trimmed. The wear at the cutting tool edge was also reduced.

• Transactions of Materials Processing
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• v.13 no.3
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• pp.242-247
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• 2004

Literature review on reliability test method for developing high performance optical/thermofluidic components. Since the miniaturization by the conventional mechanical process is limited to milli-structure, i.e. $10^{-3}m$, new technology for fabricating of mechanical components is needed to match cost, reliability, and integrability criteria of micro-structure. Although numbers of various researches on MEMS/MOEMS devices and components, including material characterization, design and optimization, system validation, etc., the lack of standards and specifications make the researches and developments difficult. For that reason, this paper is intended to propose the methods of reliability test for measuring the mechanical property of optical/ thermofluidic components.