• 제목/요약/키워드: KRISS

검색결과 591건 처리시간 0.027초

누설자속 측정에 의한 가스배관의 용접결함에 대한 비파괴 탐상 (Nondestructive Testing of Welding Flaw at Gas Pipeline by Measuring Magnetic Flux Leakage)

  • 유권상;박수영;김용일;이완규;임재균;남영현
    • 한국가스학회지
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    • 제12권2호
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    • pp.53-56
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    • 2008
  • 용접 부위의 결함을 비파괴적으로 탐지하기 위하여 홀센서에 의해 누설자속을 측정할 수 있는 시스템과 4 종류의 용접결함을 갖는 기준시편을 제작하였다. 제작한 시스템으로 시편에 생성시킨 4 종류의 결함에서 누설된 자속을 측정하였고, 신호의 피크-피크 크기와 피크-피크 간의 간격에서 결함의 종류를 구분할 수 있는 가능성을 확인하였다.

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Micro-TEM Cell을 사용한 표준 전자기장의 발생 및 측정불확도 평가 (Standard Field Generation Using a Micro-TEM Cell and Its Measurement Uncertainty Evaluation)

  • 강진섭;김정환;강웅택;강노원;강태원
    • 한국전자파학회논문지
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    • 제20권1호
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    • pp.91-99
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    • 2009
  • 본 논문에서는 micro-TEM cell을 사용한 표준 전자기장 발생법을 기술하고 측정불확도를 평가하였다. 표준 전자기장 발생 시스템은 auto-leveling 기능을 가진 신호발생부, 최대 1.2 GHz까지 동작하는 micro-TEM cell, 서미스터 마운트를 사용한 전력측정부로 구성된다. 표준 전자기장 발생법의 타당성을 보이기 위해 $10\;MHz{\sim}1\;GHz$ 대역에서 전자기장의 세기 20 V/m에 대해 실시된 전자기장의 세기 국제비교(CCEM.RF-K20)의 참여 결과를 제시하였다.

A Method for Absolute Determination of the Surface Areal Density of Functional Groups in Organic Thin Films

  • Min, Hyegeun;Son, Jin Gyeong;Kim, Jeong Won;Yu, Hyunung;Lee, Tae Geol;Moon, Dae Won
    • Bulletin of the Korean Chemical Society
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    • 제35권3호
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    • pp.793-797
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    • 2014
  • To develop a methodology for absolute determination of the surface areal density of functional groups on organic and bio thin films, medium energy ion scattering (MEIS) spectroscopy was utilized to provide references for calibration of X-ray photoelectron spectroscopy (XPS) or Fourier transformation-infrared (FT-IR) intensities. By using the MEIS, XPS, and FT-IR techniques, we were able to analyze the organic thin film of a Ru dye compound ($C_{58}H_{86}O_8N_8S_2Ru$), which consists of one Ru atom and various stoichiometric functional groups. From the MEIS analysis, the absolute surface areal density of Ru atoms (or Ru dye molecules) was determined. The surface areal densities of stoichiometric functional groups in the Ru dye compound were used as references for the calibration of XPS and FT-IR intensities for each functional group. The complementary use of MEIS, XPS, and FT-IR to determine the absolute surface areal density of functional groups on organic and bio thin films will be useful for more reliable development of applications based on organic thin films in areas such as flexible displays, solar cells, organic sensors, biomaterials, and biochips.

Development of Isotope Dilution LC-MS/MS Method for Accurate Determination of Arsenobetaine in Oyster Certified Reference Material

  • Lee, Woo Young;Yim, Yong-Hyeon;Hwang, Euijin;Lim, Youngran;Kim, Tae Kyu;Lee, Kyoung-Seok
    • Bulletin of the Korean Chemical Society
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    • 제35권3호
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    • pp.821-827
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    • 2014
  • An isotope dilution liquid chromatography tandem mass spectrometry (ID LC-MS/MS) method has been developed and applied to the determination of arsenobetaine (AsB, ${(CH_3)_3}^+AsCH_2COO^-$) from oyster candidate certified reference material (CRM). The exact matching isotope dilution approach was adopted for accurate determination of AsB using $^{13}C_2$-labeled AsB as an internal standard. Efficiencies of different AsB extraction methods were evaluated using a codfish reference material and a simple sonication method was selected as the method of choice for the certification of the oyster candidate CRM. The hydrophilic interaction liquid chromatography (HILIC) combined with electrospray ionization tandem mass spectrometry (ESI/MS/MS) in selected reaction monitoring (SRM) mode was optimized for adequate chromatographic retention and robust quantification of AsB from codfish and oyster samples. By analyzing 12 subsamples taken from each 12 bottles systematically selected from the whole oyster CRM batch, the certified value of AsB was determined as $6.60mg{\cdot}kg^{-1}{\pm}0.31mg{\cdot}kg^{-1}$ and it showed excellent between-bottle homogeneity of less than 0.42%, which is represented by relative standard deviation of 12 bottles from the CRM batch. The major source of uncertainty was the certified value of the AsB standard solution.

Measurement of the occipital alpha rhythm and temporal tau rhythm by using magnetoencephalography

  • Kim, J.E.;Gohel, Bakul;Kim, K.;Kwon, H.;An, Kyung-min
    • 한국초전도ㆍ저온공학회논문지
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    • 제17권4호
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    • pp.34-37
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    • 2015
  • Developing Magnetoencephalography (MEG) based on Superconducting Quantum Interference Device (SQUID) facilitates to observe the human brain functions in non-invasively and high temporal and high spatial resolution. By using this MEG, we studied alpha rhythm (8-13 Hz) that is one of the most predominant spontaneous rhythm in human brain. The 8-13 Hz rhythm is observed in several sensory region in the brain. In visual related region of occipital, we call to alpha rhythm, and auditory related region of temporal call to tau rhythm, sensorimotor related region of parietal call to mu rhythm. These rhythms are decreased in task related region and increased in task irrelevant regions. This means that these rhythms play a pivotal role of inhibition in task irrelevant region. It may be helpful to attention to the task. In several literature about the alpha-band inhibition in multi-sensory modality experiment, they observed this effect in the occipital and somatosensory region. In this study, we hypothesized that we can also observe the alpha-band inhibition in the auditory cortex, mediated by the tau rhythm. Before that, we first investigated the existence of the alpha and tau rhythm in occipital and temporal region, respectively. To see these rhythms, we applied the visual and auditory stimulation, in turns, suppressed in task relevant regions, respectively.

FPGA 모듈을 이용한 Long Range AFM용 다축 제어 프로그램 개발 (Development of Multi-Axis Control Program for Long Range AFM Using an FPGA Module)

  • 이재윤;엄태봉;김재완;강주식;김종안
    • 한국정밀공학회:학술대회논문집
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    • 한국정밀공학회 2006년도 춘계학술대회 논문집
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    • pp.289-290
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    • 2006
  • In general, atomic force microscope (AFM) used for metrological purpose has measuring range less than a few hundred micrometers. We design and fabricate an AFM with long measuring range of $200mm{\times}200mm$ in X and Y axes. The whole stage system is composed of surface plate, global stage, microstage. By combining global stage and microstage, the fine and long movement can be provided. We measure the position of the stage and angular motions of the stage by laser interferometer. A piezoresistive type cantilever is used for compact and long term stability and a flexure structure with PZT and capacitive sensor is used for Z axis feedback control. Since the system is composed of various actuators and sensors, a real time control program is required for the implementation of AFM. Therefore, in this work, we designed a multi-axis control program using a FPGA module, which has various functions such as interferometer signal converting, PID control and data acquisition with triggering. The control program achieves a loop rate more than 500 kHz and will be applied for the measurement of grating pitch and step height.

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폴리프로필렌(Polypropylene)박막의 트리현상 (The Tree Properties of Polypropylene Thin Film)

  • 강전홍;김한준;유광민;김종석;한상옥;박강식
    • 대한전기학회:학술대회논문집
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    • 대한전기학회 1999년도 하계학술대회 논문집 D
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    • pp.1584-1586
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    • 1999
  • The polypropylene has been known to have higher melting temperature than Polyethylene. and good mechanical properties. This paper introduces the experiment result for tree properties of polypropylene thin film with a crystal structure. According to the experiment. tree properties is appeared boundary section of thin film first of all. Also, Spherulites magnitude of slow cooling is larger than that of rapid cooling.

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van der Pauw와 four point probe 방법에 의한 반도체 웨이퍼의 면저항 비교 (Comparison of van der Pauw method with FPP method in Sheet Resistance Measurements of Semiconductor Wafer)

  • 강전홍;김한준;유광민;한상옥;김종석;박강식;구경완
    • 대한전기학회:학술대회논문집
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    • 대한전기학회 2004년도 하계학술대회 논문집 C
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    • pp.1634-1636
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    • 2004
  • 반도체 웨이퍼의 면저항을 정밀 측정하는 대표적인 두가지 방법인 4탐침(four point probe)방법과 van der Pauw방법으로 반도체 웨이퍼의 면저항을 비교평가 하였다. 4탐침방법에 의한 측정 시스템을 사용하여 웨이퍼의 전체 면에 대하여 면저항을 측정하고, 같은 웨이퍼의 가장자리 네 지점에 탐침 전극을 구성한 후 van der Pauw 방법으로 면저항을 측정한 결과 4탐침 방법에 의한 측정결과를 기준으로 1 %이하의 일치도를 나타냈다.

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박막 재료의 면저항 측정기 개발 (A Development of Sheet Resistance Meter for Thin Film Materials)

  • 강전홍;유광민;김한준;한상옥
    • 한국전기전자재료학회:학술대회논문집
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    • 한국전기전자재료학회 2009년도 하계학술대회 논문집
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    • pp.233-234
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    • 2009
  • 박막 재료의 면저항 측정은 일반적으로 FPP(Four-Point Probe)원리를 적용한 측정기률 사용하고 있다. 개발된 면저항 측정기의 특징은 dual configuration 기술을 적용하여 탐침 간격에 대한 시료의 크기 및 두께에 대한 보정계수를 고려하지 않아도 되므로 누구나 업고 정확하게 사용 할 수 있다. 측정범위는 $1\;m{\Omega}{/\square}\;{\sim}\;1\;G{\Omega}{/\square}$이며, 반복성과 재현성 및 직선성은 0.1 %이하로서 우수한 특성을 나타냈다. 또한 기존의 면저항 측정기에 적용된 single configuration 기술에서 나타나는 가장자리 효과의 단점을 dual configuration 기술을 적용하여 해결하였고 정밀 정확도를 향상시켰다. 개발된 면저항 측정기의 특성평가는 국가측정표준으로부터 소급성이 유지된 표준저항, 분할저항기, 면저항 인증표준물질 등을 사용하였다.

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The Design of Calculable Standard Dipole Antennas in the Frequency Range of 1~3 GHz

  • Kim, Ki-Chai;Kim, Sang-Myeong;Kwon, Jae-Yong;Kang, Tae-Weon;Kim, Jeong-Hwan
    • Journal of electromagnetic engineering and science
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    • 제12권1호
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    • pp.63-69
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    • 2012
  • This paper presents the design of a calculable standard dipole antenna with a hybrid balun in the frequency range of 1 GHz to 3 GHz. A new formula of the antenna factor for a dipole antenna with a hybrid balun is derived using the power mismatch-loss concept. The antenna factors derived in this paper are in good agreement with the results calculated from S-parameters. The design results show that the calculable dipole antenna with a hybrid balun can be characterized by power mismatch-loss component factors.