• 한국주조공학회지
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• 제21권4호
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• pp.246-252
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• 2001

Variation in the microstructure of Mg-5%Al semi-solid slurry during isothermal heating was investigated in relation to initial microstructure, holding time, and holding temperature. Specimens with three different initial microstructures were isothermally heated. Dendritic structure in as-cast ingot was decomposed into solid globules in the semi-solid slurry during isothermal holding, while in the recrystallized specimens prepared by extrusion or rolling the size of solid particles was continuously increased during the heating. Effects of mold temperature and liquid fraction of slurry on the mold filling ability were also studied. Very thin section (0.4 mm) could be successfully filled up to 50 mm by 60% liquid slurry when the mold was heated to $600^{\circ}C$.

• Food Science and Biotechnology
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• 제16권2호
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• pp.255-259
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• 2007

The effects of temperature heating-up rate and pressure building-up phase on the inactivation of Listeria innocua ATCC 33090 were evaluated in buffered peptone water. The number of L. innocua was reduced by 5.57 and 6.52 log CFU/mL during the nonisothermal treatment (the come-up time followed by isothermal process) and the isothermal treatment, respectively, at $60^{\circ}C$. When compared to the isothermal treatment (0.76$33.2^{\circ}C/min$ of temperature heating-rate. The effect of the combined high pressure and thermal processing on the inactivation of L. innocua increased with increasing pressure and temperature. At all temperature levels from 40 to $60^{\circ}C$ under 700 MPa, L. innocua was not detected by enrichment culture (>7 log reduction).

• Journal of Welding and Joining
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• 제23권2호
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• pp.52-58
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• 2005

This study was carried out to investigate the effect of bonding temperature and heating rate on transient liquid phase diffusion bonding of Ni-base superalloy. The heating rate was varied by $0.1^{\circ}C$/sec, $1^{\circ}C$/sec, $10^{\circ}C$/sec to the bonding temperatures $1100^{\circ}C,\;1150^{\circ}C,\;1200^{\circ}C$ under vacuum. As bonding temperature increased, maximum dissolution width of base metal increased, but a dissolution finishing time decreased. The eutectic width of insert metal in the bonded interlayer decreased linearly in proportion to the square root of holding time during isothermal solidification stage. The bonding temperature was raised, isothermal solidification rate slightly increased. As the heating rate decreased and the bonding temperature increased, the completion time of dissolution after reaching bonding temperature decreased. When the heating rate was very slow, the solidification proceeded before reaching bonding temperature and the time required for the completion of isothermal solidification became reduced.

• 한국안전학회지
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• 제22권1호
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• pp.19-23
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• 2007

The aim of this study was to determine residual stresses in thermal barrier coatings(TBCs) by isothermal heating. Specimens were heated at the range of $1000{\sim}1600^{\circ}C$. A finite element method was used to determine the residual stresses. Finite element coupled heat transfer and elastic-plastic thermal stress analysis using a general purpose commercial FEM software ABAQUS. I obtained the stresses were not affected below the temperature of $1400^{\circ}C$ but affected over that of temperature.

• 한국분말재료학회지
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• 제16권3호
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• pp.167-172
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• 2009

This study has been carried out to investigate the non-isothermal behaviors and kinetic parameter of calcium carbonate by different thermal analysis methods. At the heating rate of $10^{\circ}C$/min, the onset calcination temperature, the peak and final temperatures of calcium carbonate were $612^{\circ}C$, $748^{\circ}C$, and $890^{\circ}C$ respectively. As the heating rate of the calcium carbonate increased from $5^{\circ}C$/min to $20^{\circ}C$/min, the peak temperature increased from $719^{\circ}C$ to $782^{\circ}C$. The activation energies of the calcium carbonate calculated by the methods of Kissinger and Freeman-Carroll were 40.15 kcal/mol and 43.47 kcal/mol, respectively.

• Korea-Australia Rheology Journal
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• 제19권4호
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• pp.201-209
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• 2007

The present paper is concerned with non-isothermal spherical Couette flow of Oldroyd-B fluid in the annular region between two concentric spheres. The inner sphere rotates with a uniform angular velocity while the outer sphere is kept at rest. Moreover, the two spherical boundaries are maintained at fixed temperature values. Hence, the fluid is effect by two heat sources; namely, the viscous heating and the temperature gradient between the two spheres. The viscoelasticity of the fluid is assumed to dominate the inertia such that the latter can be neglected. An approximate analytical solution of the energy and momentum equations is obtained through the expansion of the dynamical fields in power series of Nahme number. The analysis show that, the temperature variation due to the external source appears in the zero order solution and its effect extends to the fluid velocity distribution up to present second order. Viscous heating contributes in the first and second order solutions. In contrast to isothermal case, a first order axial velocity and a second order stream function fields has been appeared. Moreover, at higher orders the temperature distribution depends on the gap width between the two spheres. Finally, there exist a thermal distribution of positive and negative values depend on their positions in the domain region between the two spheres.

• Geomechanics and Engineering
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• 제12권4호
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• pp.707-721
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• 2017

The objective of this paper is to experimentally study the consolidation of saturated silty clay subjected to repeated heating-cooling cycles using a modified temperature-controlled triaxial apparatus. Focus is placed on the influence of the water content, confining pressure, and magnitudes and number of thermal loading cycles. The experimental results show that the thermally induced pore pressure increases with increasing water content and magnitude of thermal loading in undrained conditions. After isothermal consolidation at an elevated temperature, the pore pressure continues to decrease and gradually falls below zero during undrained cooling, and the maximum negative pore pressure increases as the water content decreases or the magnitude of thermal loading increases. During isothermal consolidation at ambient temperature after one heating-cooling cycle, the pore pressure begins to rise due to water absorption and finally stabilizes at approximately zero. As the number of thermal loading cycles increases, the thermally induced pore pressure shows a degrading trend, which seems to be more apparent under a higher confining pressure. Overall, the specimens tested show an obvious volume reduction at the completion of a series of heating-cooling cycles, indicating a notable irreversible thermal consolidation deformation.

• 설비공학논문집
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• 제13권8호
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• pp.739-745
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• 2001

The objective of this research is to analyze the ventilation effectiveness in the non-isothermal air supply using mixing and displacement ventilation systems for indoor air quality control and management. In this study, a ventilation effectiveness is evaluated in a simplified model chamber using a tracer gas technique of $CO^2$ gas injected into a supply duct as a function of ventilation rates, supply/extract sites and cooling/heating air supply. The ventilation effectiveness decreased with increasing ventilation rate on the cooling and heating conditions. And the ventilation effectiveness of case 3 (down supply and upper extract) was better thant that of case 1(upper supply and upper extract) and case 2(upper supply and down extract) with the cooling supply conditions. but for the heating supply air conditions, the ventilation effectiveness of case 2 was better than that of case 3 and case 1.

• Elastomers and Composites
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• 제53권2호
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• pp.52-56
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• 2018

The present study examines the transformation of dynamic DSC data into the equivalent isothermal data for the formation kinetics of a polyurethane elastomer. The reaction of 2'-dichloro-4,4'-methylenedianiline (MOCA) with a PTMG/TDI-based isocyanate prepolymer was evaluated. DSC measurement was performed in the dynamic scanning mode with several different heating rates to obtain the reaction thermograms. Then, the data was transformed into the isothermal data through a procedure based on Ozawa analysis. The main feature of this procedure was the transformation of $({\alpha}-T)_{\beta}$ curves from dynamic DSC into $({\alpha}-t)_T$ curves using the isoconversional $(t-T)_{\alpha}$ diagram. Validity was discussed for the relationship between the dynamic DSC data and the transformed isothermal results.

• 폴리머
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• 제24권1호
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• pp.105-112
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• 2000

본 연구에서는 항공기 구조용 재료로 쓰이는 탄소섬유/에폭시 복합재료 프리프레그(DMS 2224)를 모델시스템으로 하여 등온환경과 등속도 가열환경에서 경화반응 속도를 연구하였다. 이 복합재료의 공정온도에서의 가공공정을 묘사할 수 있는 현상학적인 반응속도 모델을 differential scanning calorimetry (DSC)와 이론을 통하여 제안하였다. 등온환경에서의 실험으로부터 반응특성곡선을 관찰한 결과 경화반응이 1차 반응함수임을 확인하였고, 활성화 에너지는 78.43 kJ/mo1을 얻었다. 이 프리프레그는 경화온도에 따라 한계경화도를 보여주어 유리화가 존재함을 확인하였고 이를 1차 반응속도 모델에 적용시킨 결과, 유리화 이후의 확산우세현상을 포함한 반응속도 모델을 제안하였다. 제안된 모델식을 이용하여 등온/등속도 가열환경을 포함한 실제 경화공정을 성공적으로 표현할 수 있었다.