• The Korean Journal of Ceramics
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• 제1권4호
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• pp.191-196
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• 1995

Using sol-gel processing method, thin films of lathanum modified lead titanate(PLT) on Corning 7059 glass were prepared. A differential thermal analysis (DTA/TG) curve of gel powder and infrared spectra (FT-IR) of the films were measured to estimate residual organices in them. The heat-treated films were characterized by X-ray diffraction(XRD). Microstructures of the films were observed by a scanning electron microscope (SEM). Optical properties of the films were determined by a UV-VIS spectrophotometer. The waveguiding properties and optical attenuation were measured with the end coupling method and the cut back method. Effects of the drying conditions on the transmittance and the propagation loss of the films were investigated. Experimemtal results showed that the content of residual organics in the film decreased as the drying temperature of the film increased. As the La content of the film increased, the grain size decreased and the transmittance increased. The transmittances of the films increased with the increasing of the drying temperature. The propagation losses in the film decreased as the drying temperature increased.

• 한국약용작물학회:학술대회논문집
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• 한국약용작물학회 2011년도 추계학술발표회
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• pp.336-337
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• 2011

• 한국약용작물학회:학술대회논문집
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• 한국약용작물학회 2011년도 추계학술발표회
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• pp.338-339
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• 2011

• Journal of Pharmaceutical Investigation
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• 제18권4호
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• pp.181-186
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• 1988

Inclusion complex of sulfamethoxazole with ${\beta}-cyclodextrin$ was prepared by freeze-drying method in molar ratios of 1:1, 1:1.25, 1:1.5 and 1:1.75, and the complex formation was identified by ultraviolet and infrared spectroscopies, powder X-ray diffractometry and differential scanning calorimetry. Dissolution rate and solid state stability of the complex were investigated in comparison with those of sulfamethoxazole powder and the physical mixture of sulfamethoxazole with ${\beta}-cyclodextrin$. As a result, the dissolution rate and the stability of solid complexes in various relative humidity conditions increased more remarkably than those of sulfamethoxazole powder and physical mixture. But the difference according to molar ratio of the complex was not recognized.

• 한국의류산업학회지
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• 제24권2호
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• pp.260-266
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• 2022

Cellulose fiber is a material used in various fields. It is the most used type of fiber because of its excellent hygroscopicity and dyeability. Recently, as natural fiber materials have been highlighted due to the influence of eco-friendliness and well-being, bamboo fiber has become a commonly used eco-friendly fiber. Cellulose fibers are part of the -OH hydroxyl group, which means they are more chemically reactive than synthetic fibers. In this study, the cationization properties of bamboo-cotton blended fabrics cationized using CHPTAC (3-chloro-2-hydroxypropyl trimethyl ammonium chloride) in the PDC (padding-drying-curing) method were investigated. Various characteristics according to cationization were studied through elemental analysis, FT-IR (fourier-transform infrared spectroscopy) analysis, X-ray diffraction analysis, TGA (thermogravimetric) analysis, and SEM (scanning electron microscope) analysis. The nitrogen content of the cationized bamboo-cotton blended fabric increased with an increase in the concentration of the cationizing agent CHPTAC, and it was seen to be highly bound to cellulose molecules. As a result of the FT-IR analysis, both 100% pure cotton fabrics and CHPTAC-0 and CHPTAC-150 fabrics were seen to be typical cellulose. As a result of the X-ray diffraction analysis, both 100% pure cotton fabrics and CHPTAC-0 and CHPTAC-150 fabrics showed typical cellulose I structures. As a result of the X-ray diffraction analysis, both 100% pure cotton fabrics and CHPTAC-0 and CHPTAC-150 fabrics showed typical cellulose I structures. As the cationization progressed, micropores appeared on the surface of the blended fabric.

• 대한약침학회지
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• 제20권1호
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• pp.36-44
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• 2017

Objectives: The goal of this study was to characterize Suvarna Bhasma Parada Marit by using the Ayurvedic test parameters, physico-chemical tests, and various instrumentation techniques. Methods: Suvarna Bhasma, an Ayurvedic formulation manufactured as per Bharat Bhaishajya Ratnakar 5/8357 (BBR), has been studied using various instrumentation techniques: X-ray diffraction (XRD), scanning electron microscopy (SEM), energy dispersive X-ray analysis (EDAX), laser particle size distribution (PSD) analysis, fourier transform infrared spectroscopy (FT-IR), and atomic absorption spectroscopy (AAS), and physico-chemical parameters, such as the loss on drying (LOD), loss on ignition (LOI), and acid insoluble Ash (AIA) were determined. In addition, Ayurvedic tests, such as Rekhapurnatva (enterable in the furrows of the fingers), Varitaratwa (floatable over water), Nirdhoomta (smokeless), Dantagre Kach-Kach (gritty particle feeling between the teeth), were performed. Results: The XRD study showed Suvarna Bhasma to be crystalline in nature and to contain more than 98% gold. The mean size of the gold crystallites was less than 10 microns, and the morphology was globular and irregular. Suvarna Bhasma contains gold as its single and major element, with EDAX and FT-IR spectra showing that it is more than 98% pure gold. The moisture content (LOD) is less than 0.5%, the LOI is less than 2%, and the AIA is not less than 95%. The Ayurvedic tests, as specified above, helped to confirm the quality of Suvarna bhasma prepared as per the text reference (BBR). Conclusion: This chemical characterization of Suvarna Bhasma performed in this study by using modern instrumentation techniques will be helpful in understanding its pharmacological actions and will help in establishing quality protocols and specifications to substantiate the safety, efficacy & quality of Suvarna Bhasma.

• 유기물자원화
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• 제24권4호
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• pp.105-112
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• 2016

우분을 원료로 하여 구 모양의 펠릿(Spherical pellet) 형태로 가공한 우분 고체연료에 대한 건조실험을 수행하였다. 제조한 구 형태의 우분 고체 연료를 선별기에 투입하여 각 크기별로 분리하였다. 건조방식으로는 대류형 열풍건조 방법과 적외선 조사 건조 방법. 그리고 과열증기 적용에 의한 건조방법을 적용하였다. 제조된 펠릿의 직경에 따라 5 mm, 10 mm, 20 mm 로 구분하여 각 입경별 우분 고체연료 가공품의 수분 감소효과를 분석하였다. 가공된 우분 펠릿의 건조에 소요된 시간은 대류형 열풍기 건조 > 적외선 건조 > 과열증기 건조 방법의 순이었다. 과열 증기 적용에 의한 건조방법의 경우 건조에 소요된 시간은 열풍과 적외선 방법에 비해 상대적으로 짧았다. 건조된 상태인 우분 펠릿의 겉보기 비중은 $250{\sim}350kg/m^3$ 수준이었으며, 건조된 우분 펠릿의 저위발열량은 가축분뇨의 관리 및 이용에 관한 법률 시행규칙 별표 2에서 정한 가축분뇨 고체연료의 성분 등에 관한 기준에 규정된 3,000 kcal/kg 보다 높은 수준이었다. 우분 펠릿의 입자크기가 작을수록 모든 건조방법에서 건조에 필요한 시간이 짧게 소요되었다. 5 mm 크기의 우분 펠릿을 건조하였을 때 시료의 무게 변화가 1% 내외가 될 때까지 소요된 시간은 과열증기 적용 시 약 30분, 적외선 조사 시 약 108분, 대류형 열풍 적용 시 약 120분이 소요되었다. 동일한 건조조건일 경우에는 펠릿 입자의 크기를 작게 하는 것이 가축 분 고체연료의 건조시간을 단축하는 중요한 요소인 것으로 판단된다.

• 한국세라믹학회지
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• 제34권9호
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• pp.986-992
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• 1997

Cordierite ceramic was prepared by sol-gel method. It was analyzed by Infrared spectroscopy and X-ray diffraction patterns that the ceramic was chemically mixed in molecular level and transformed to $\alpha$-cordierite at 125$0^{\circ}C$. Water vapour treatments for aging and drying process were conducted to get porous cordierite with thermally stable pore structure. It resulted in 220-410 $m^2$/g BET surface area and mesoporous structure with mean pore diameter, 40$\AA$. Compared to naturally dried ceramic, the ceramic showed superior thermal stability of surface area up to $700^{\circ}C$. Surfaces of porous cordierite ceramics were observed by SEM.

• 한국가구학회지
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• 제19권6호
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• pp.452-459
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• 2008

The compressed injection yellow ocher soil is the process-technology by drying the product through sunshine, not by firing like pottery and ceramic ware. It is the technology of development being able to achieve the far infrared ray and humidity adjustment by adding recycling paper, Korean paper and bamboo salt, and it corresponds with the construction enforcement ordinance 2007 as an interior-finishing product which is fire-resistant. In case that the yellow ocher soil would be used as lighting device and interior-finishing material and decoration, it could contribute to an improvement of National Health by avoiding the sick house syndrome and adding humidity adjustment, and it has more efficient economic effect due to using recycle-available additives. Through such developments of the yellow ocher soil products the domestic market of lighting device and construction material can be advanced and the replacement effect of imported goods & also export effect can be expected accordingly.

• 한국농업기계학회:학술대회논문집
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• 한국농업기계학회 2002년도 하계 학술대회 논문집
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• pp.157-162
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• 2002

지금까지 우리나라 벼농사는 고품질 쌀의 생산보다는 다수확재배기술로 생산량을 늘리는 것이 농가소득에 유리하였다. 그러나 소비수준이 높아지고 쌀의 제고가 충분한 현시점에서는 풀질의 경쟁력 향상이 더욱 중요하다 이를 위해서는 고품질 쌀 생산을 위한 건조, 저장, 가공 등 기반시설의 현대화하여 브랜드화에 의한 차별화를 통하여 소비자의 신뢰를 얻기 위한 연구가 수행되어야 할 것이다. 쌀의 밥맛을 결정하는 요인은 품종, 재배, 관리, 수확에 이르기까지 관계가 있겠지만, 수확후처리 공정과정에서도 품질의 우열이 좌우된다 특히 건조 중 열풍온도 관리 소홀로 인하여 과건이 되는 경우에는 밥맛에 치명적이라고 할 수 있다. (중략)