• The Korean Journal of Ceramics
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• v.6 no.3
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• pp.201-205
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• 2000

Fiber reinforced plastic (FRP) composites and ceramic matrix composites (CMC) which contain electrically conductive phases have been designed and fabricated to introduce the detection capability of damage/fracture detection into these materials. The composites were made electrically conductive by adding carbon and TiN particles into FRP and CMC, respectively. The resistance of the conductive FRP containing carbon particles showed almost linear response to strain and high sensitivity over a wide range of strains. After each load-unload cycle the FRP retained a residual resistance, which increased with applied maximum stress or strain. The FRP with carbon particles embedded in cement (mortar) specimens enabled micro-crack formation and propagation in the mortar to be detected in situ. The CMC materials exhibited not only sensitive response to the applied strain but also an increase in resistance with increasing number of load-unload cycles during cyclic load testing. These results show that it is possible to use these composites to detect and/or fracture in structural materials, which are required to monitor the healthiness or safety in industrial applications and public constructions.

• Transactions of the Korean Society of Mechanical Engineers A
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• v.30 no.6 s.249
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• pp.637-642
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• 2006

A plastic zone size is regarded as a measure of material resistance, and also it determines the fracture behavior. The importance of estimating or measuring the plastic zone size cannot be too emphasized. In this article, SDSP(Stereo Digital Speckle Photography) is examined as a new techniques to measure the plastic zone developed in a ductile metal. This technique is simple, vibration free and non-contact, and measures simultaneously in-plane displacements as well as out-of plane displacements like the side necking. Experimental results for a CT specimen are presented to demonstrate the accuracy in comparison with those obtained by recrystallization technique and finite element analysis.

• Journal of the Korean Ceramic Society
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• v.31 no.12
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• pp.1449-1458
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• 1994

A new analytical model which can discribe the relationship between the bridging stress and the crack opening displacement was proposed to investigate the microstructural effect on the R-curve behavior in a polycrystalline alumina. The crack opening displacement according to the distance behind the stationary crack tip was measured using in-situ fracture technique in an SEM, and then used for a fitting procedure to obtain the distribution of bridging stress. The current model and an empirical power law relation were introduced into the fitting procedure. The results indicated that the bridging stress function and R-curve computed by the current model were consistent with those computed by the power law relation. The microstructural factor, e.g., the distribution of grain size, was also found to be closely related to the bridging stress. Thus, this model explained well the interaction effect between the distribution of bridging stress and the local-fracture-controlling microstructure, providing important information for the systematic interpretation of microfracture mechanism including R-curve behavior of a monolithic alumina.

• Tunnel and Underground Space
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• v.6 no.3
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• pp.209-222
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• 1996

Shut-in pressure, reopenting pressure and fracture orientation are very important parameters to be evaluated precisely in in-situ stress measurement by hydraulic fracturing. Graphical methods on pressure-time curves have been conventionally used, even though these are seriously dependent on subjectivity of interpreters. So there have been many demands on new method to objectivity in determining parameters. We have developed integrated hydrofracturing data processing program (HYDFRAC), based on nonlinear regression analysis and can be invoked under the Window graphical user interface. HYDFRAC consiste of three routines, that is shut-in pressure routine, reopening pressure routine, and fracture delineation routine. Each of routines include independent modules according to parameter determination methods. Its application to field tests ensured both objectivity and facility in determining of hydraulic fracturing parameters. Determining shut-in pressures at each pressurization cycles, we adopted the exponential pressure-decay method(EPD method), the bilinear pressure-decay-rate method (PDR method), and the tangent intersection method in order to find the pressurization-cyclic tendency of shut-in pressures. The estimated pressure by PDR method exists in the range of the upper and lower values by EPD method, and lies near to the upper value more than the lower. Being the pressurization cycle increased, the range of upper and lower limits come to be stabilized gradually. By graphical superposition method and bilinear pressure-accumulated volume method, reopening pressures were determined. Vertical and inclined fracture attitudes were determined by applying the directional statistics and sinusoidal curve fitting, respectively. The results of evaluation of hydrofracturing parameters showed that statistical methods could enhance the objectivity better than graphical methods.

• Korean Journal of Metals and Materials
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• v.46 no.8
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• pp.524-537
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• 2008

Zr-based amorphous alloy matrix composites reinforced with metallic continuous fibers were fabricated by liquid pressing process, and their fracture properties were investigated by directly observing microfracture process using an in situ loading stage installed inside a scanning electron microscope chamber. About 60 vol.% of metallic fibers were homogeneously distributed inside the amorphous matrix. Apparent fracture toughness of the stainless-steel- and tungsten-fiber-reinforced composites was lower than that of monolithic amorphous alloy, while that of the Ta-fiber-reinforced composite was higher. According to the microfracture observation, shear bands or cracks were initiated at the amorphous matrix, and the propagation of the initiated shear bands or cracks was effectively blocked by fibers, thereby resulting in stable crack growth which could be confirmed by the fracture resistance curve (R-curve) behavior. This increase in fracture resistance with increasing crack length improved fracture properties of the fiber-reinforced composites, and could be explained by mechanisms of formation of multiple shear bands or multiple cracks at the amorphous matrix and blocking of crack or shear band propagation and multiple necking at metallic fibers.

• Applied Microscopy
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• v.49
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• pp.3.1-3.7
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• 2019

Graphene, which is one of the most promising materials for its state-of-the-art applications, has received extensive attention because of its superior mechanical properties. However, there is little experimental evidence related to the mechanical properties of graphene at the atomic level because of the challenges associated with transferring atomically-thin two-dimensional (2D) materials onto microelectromechanical systems (MEMS) devices. In this study, we show successful dry transfer with a gel material of a stable, clean, and free-standing exfoliated graphene film onto a push-to-pull (PTP) device, which is a MEMS device used for uniaxial tensile testing in in situ transmission electron microscopy (TEM). Through the results of optical microscopy, Raman spectroscopy, and TEM, we demonstrate high quality exfoliated graphene on the PTP device. Finally, the stress-strain results corresponding to propagating cracks in folded graphene were simultaneously obtained during the tensile tests in TEM. The zigzag and armchair edges of graphene confirmed that the fracture occurred in association with the hexagonal lattice structure of graphene while the tensile testing. In the wake of the results, we envision the dedicated preparation and in situ TEM tensile experiments advance the understanding of the relationship between the mechanical properties and structural characteristics of 2D materials.

• Journal of Korean Ophthalmic Optics Society
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• v.5 no.2
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• pp.207-210
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• 2000

The SiC-TiC composites materials for glasses lens cutting were fabricated by hot-pressing and annealing. The amount of TiC was 0, 10, 20, 30wt% in the mixture of ${\beta}-SiC$. The microstructure of materials for glasses lens cutting was very dependent on the TiC amount. The introduction of larger amount of TiC improved fracture toughness, optical microscope and XRD analysis of the surface of samples were carried out. An in situ-toughened microstructure, consisted of distributed elongated SiC, matrix like TiC grains was developed by using ${\beta}-SiC$. Typical hardness and fracture toughness of materials for spectacle lens cutting were 14.9 GPa and $5.7MPa{\cdot}m^{1/2}$, respectively.

• Hip & pelvis
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• v.35 no.4
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• pp.259-267
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• 2023

Purpose: Nondisplaced femoral neck fractures have traditionally been treated with in situ fixation. However, poor surgical and clinical outcomes have been reported for fractures with valgus deformity >15°, and the reduction of valgus impaction has recently been emphasized. In addition, early degenerative osteoarthritis can be caused by cam-type femoroacetabular impingement after healing of femoral neck fractures. This study was designed with the objective of confirming the difference in progression of radiographic osteoarthritis according to the severity of the valgus deformity. Materials and Methods: Patients who underwent internal fixation using multiple cannulateld screws for management of nondisplaced femoral neck fractures were divided into two groups: high valgus group (postoperative valgus angle ≥15°) and low valgus group (postoperative valgus angle <15°). Evaluation of demographic data and changes in the joint space width from the immediate postoperative period to the latest follow-up was performed. Results: A significant decrease in joint space width in both hip joints was observed in the high valgus group when compared with the low valgus group, including cases with an initial valgus angle less than 15° and those corrected to less than 15° of valgus by reduction. No complications requiring surgical treatment were observed in either group; however, two cases of avascular necrosis, one in each group, which developed in the low valgus group after reduction of the fracture, were followed for observation. Conclusion: Performing in situ fixation in cases involving a valgus deformity ≥15° in non-displaced femoral neck fractures may cause accelerated narrowing of the hip joint space.

• Clinics in Shoulder and Elbow
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• v.19 no.1
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• pp.25-32
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• 2016

Background: The goal of this study was to evaluate whether a modified fluoroscopic technique for positioning a hook plate affected the clinical results of treating Neer type II distal clavicle fractures and Rockwood type V acromioclavicular (AC) joint separations with this device. Methods: The study was a retrospective consecutive case series with data analysis. Sixty-four patients with a Neer type II distal clavicle fracture or a Rockwood type V AC joint injury treated between March 2009 and June 2013 were divided into 2 groups: traditional fluoroscopic technique (traditional view, 31 patients) or modified fluoroscopic technique ('hook' view, 33 patients). A visual analogue scale (VAS) score, the modified University of California-Los Angeles (UCLA) shoulder scale score, and radiographic osteolysis were the main outcome measures. Results: The traditional group included a significantly larger number of patients with acromial osteolysis than the hook view group: 23 patients (74.2%) vs. 11 patients (33.3%), respectively (p=0.01). Before plate removal, the hook group reported less pain and higher UCLA shoulder scale scores than the traditional group: average VAS score, 1.55 vs. 2.26, respectively; average UCLA score, 30.88 vs. 27.06, respectively. However, there was no significant difference after plate removal. Conclusions: The hook view allows more accurate bending of the hook plate around the contour of the acromion, resulting in decreased osteolysis, decreased pain, and better function with the plate in situ.

• Korean Journal of Metals and Materials
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• v.50 no.12
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• pp.939-948
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• 2012

A 3-ply clad metal consisting of aluminum and copper was fabricated by roll bonding process and the microstructures and mechanical properties of the roll-bonded and post-roll-bonding heat treated Cu/Al/Cu clad metal were investigated. A brittle interfacial reaction layer formed at the Cu/Al interfaces at and above $400^{\circ}C$. The thickness of the reaction layer increased from $12{\mu}m$ at $400^{\circ}C$ to $28{\mu}m$ at $500^{\circ}C$. The stress-strain curves demonstrated that the strength decreased and the ductility increased with heat treatment up to $400^{\circ}C$. The clad metal heat treated at $300^{\circ}C$ with no indication of a reaction layer exhibited an excellent combination of the strength and ductility and no delamination of layers up to final fracture in the tensile testing. Above $400^{\circ}C$, the ductility decreased rasxpidly with little change of strength, reflecting the brittle nature of the intermetallic interlayers. In Cu/Al/Cu clad heat treated above $400^{\circ}C$, periodic parallel cracks perpendicular to the stress axis were observed at the interfacial reaction layer. In-situ optical microscopic observation revealed that cracks were formed in the Cu layer due to the strain concentration in the vicinity of horizontal cracks in the intermetallic layer, promoting the premature fracture of Cu layer. Vertical cracks parallel to the stress axis were also formed at 15% strain at $500^{\circ}C$, leading to the delamination of the Cu and Al layers.