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Studies on Characteristics of $ZnCa_2O_4$ Prepared by Glycine Nitrate Process anti S01id State Reaction for FE8 Phosphor (GNP법과 고상반응법으로 제조한 FED 형광체용 $ZnCa_2O_4$ 분말의 특성에 관한 연구)

  • Sin, Han;Park, Sung
    • Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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    • 1999.05a
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    • pp.91-95
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    • 1999
  • PED용 형광체로 사용되는 ZnCa$_2$O$_4$를 Clycine Nitrate Process로 합성하여 고상 반응법으로 합성한 ZnCa$_2$O$_4$ 분말과 비교 분석하였다. 또한 Glycine Nitrate Process로 제조시 Mn의 doping 농도를 변화시키면서 각각의 조성비에 따른 발광특성을 알아보았다. TGA 측정 결과 GNP법으로 합성된 ZnCa$_2$O$_4$ 의 경우 약 40$0^{\circ}C$ 이상에서 무게감량의 변화가 없었으며, XRD 상분석 결과 연소반응 후 이미 상형성이 이루어짐을 알 수 있었다. PL측정을 결과 GNP(GIycine Nitrate Process)로 제조된 ZnCa$_2$O$_4$분말의 발광효율이 고상 반응법으로 제조된 분말보다 우수하였으며, 균일하고 비표면적이 큰 단일상임이 관찰되었고, 더 작은 에너지와 시간으로 제조할 수 있는 장점이 있었다

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Studies on Goucoalkaloids in Plants I. High Performance Liquid Chromatographic Analysis of Glucoalkaloids in Periderm and Cortex of Potato (Solanum tuberosum var. May Queen) (식물체(植物體)의 Glucoalkaloids 에 관(關)한 연구(硏究) 제1보(第1報) 고속액체(高速液體)크로마토그래피에 의한 감자(Solanum tuberosum var. May Queen)의 피층부(皮層部) 및 수질부(髓質部)의 Glucoalkaloids 측정(測定))

  • Hwang, Chun-Sun;Lee, Sung-Woo
    • Journal of the Korean Society of Food Science and Nutrition
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    • v.11 no.3
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    • pp.1-4
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    • 1982
  • By high performance liquid chromatography, separation and quantification of glucoalkaloids $({\alpha}-chaconine$and${\alpha}-solanine)$ from potato (Solanum tuberosum, var. May Queen) was established using periderm and cortex. $Nucleosil-NH_2\;(10{\mu}m)$ was packed in two stainless steel columns ($4.0\;ID{\times}15\;cm$ and $4.0\;ID{\times}25\;cm$) which were connected in sequence and eluted with the mixture of tetrahydrofuran, phosphoric acid buffer and acetonitrile (50 : 25 : 25, v/v/v) at the flow rate of 1ml/min. and the absorbance were read at 208 nm. Retention time was 6.92 min. for ${\alpha}-chaconine$ and 10.96 min. for ${\alpha}-solanine$ with complete separation. This method took 12 min. per sample and seemed best. ${\alpha}-Chaconine$ and ${\alpha}-solanine$ were found much in periderm than in cortex.

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The Performance Analysis and Design of Selling Spectacle Lenses in Domestic Market (국내 시판 안경렌즈의 성능 분석 및 설계)

  • Kim, Se-Jin;Lim, Hyeon-Seon
    • Journal of Korean Ophthalmic Optics Society
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    • v.15 no.4
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    • pp.355-360
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    • 2010
  • Purpose: Analysis performance for spectacle lens which sales in domestic market and optimization design a spectacle lens which is corrected aberration. Methods: Measured center thickness, radius and aspherical surface coefficient for spherical and aspherical lenses which were ${\pm}$5.00D. Refractive index for every lens was 1.6 and they came from 4 different companies. I used 3 types of equipment to measure lenses. ID-F150 (Mitutoyo) : Center Thickness, FOCOVISION (SR-2, Automation Robotics) : Radius, PGI 1240S (Taylor Hobson) : Aspherical surface coefficient. Designed a lens which had 27 mm of distance from lens rear surface to center of eye, 4 mm of pupil diameter and small aberration on center vision $30^{\circ}C$. To shorten axial distance compared with the measured lens rise merits for cosmetic. Lens Design tool was CODE V (Optical Research Associates). Results: -5.00D aspherical lens had somewhat high astigmatism and distortion compared with the spherical lens. But it had a merit for cosmetic because of short axial height and decrease edge thickness. Improved a performance of distortion and ascertain merits for cosmetic due to short axial height and decrease edge thickness same as (-) lens in case of +5.00 aspherical lens. Though an optimization process front surface aspherical lens had a good performance for astigmatism and distortion and the merit for beauty compared with measured spherical lens. Conclusions: Design trend for domestic aspherical lens is decrease axial height and thickness to increase a merit for cosmetic not but increase performance of aberration. From design theory for optimization design front surface aspherical spectacle lens which has improved performance of aberration and merit for cosmetic at the same time compared with the measured lens. Expect an improved performance from design back aspherical lens compared with front aspherical lens.

Effects of Trichostatin A on In vitro Development of Porcine Embryos Derived from Somatic Cell Nuclear Transfer

  • Jeong, Yeon Ik;Park, Chi Hun;Kim, Huen Suk;Jeong, Yeon Woo;Lee, Jong Yun;Park, Sun Woo;Lee, Se Yeong;Hyun, Sang Hwan;Kim, Yeun Wook;Shin, Taeyoung;Hwang, Woo Suk
    • Asian-Australasian Journal of Animal Sciences
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    • v.26 no.12
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    • pp.1680-1688
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    • 2013
  • Many different approaches have been developed to improve the efficiency of animal cloning by somatic cell nuclear transfer (SCNT), one of which is to modify histone acetylation levels using histone deacetylase inhibitors (HDACi) such as trichostatin A (TSA). In the present study, we examined the effect of TSA on in vitro development of porcine embryos derived from SCNT. We found that TSA treatment (50 nM) for 24 h following oocyte activation improved blastocyst formation rates (to 22.0%) compared with 8.9% in the non-treatment group and total cell number of the blastocysts for determining embryo quality also increased significantly ($88.9{\rightarrow}114.4$). Changes in histone acetylation levels as a result of TSA treatment were examined using indirect immunofluorescence and confocal microscopy scanning. Results showed that the histone acetylation level in TSA-treated embryos was higher than that in controls at both acetylated histone H3 lysine 9 (AcH3K9) and acetylated histone H4 lysine 12 (AcH4K12). Next, we compared the expression patterns of seven genes (OCT4, ID1; the pluripotent genes, H19, NNAT, PEG1; the imprinting genes, cytokeratin 8 and 18; the trophoblast marker genes). The SCNT blastocysts both with and without TSA treatment showed lower levels of OCT4, ID1, cytokeratin 8 and 18 than those of the in vivo blastocysts. In the case of the imprinting genes H19 and NNAT, except PEG1, the SCNT blastocysts both with and without TSA treatment showed higher levels than those of the in vivo blastocysts. Although the gene expression patterns between cloned blastocysts and their in vivo counterparts were different regardless of TSA treatment, it appears that several genes in NT blastocysts after TSA treatment showed a slight tendency toward expression patterns of in vivo blastocysts. Our results suggest that TSA treatment may improve preimplantation porcine embryo development following SCNT.

A study on the oxidation characteristics of Polybutadiene & Polyisoprene containing various types of antioxidants by DSC (산화방지제(酸化防止劑)를 배합(配合)한 Polybutadiene과 Polyisoprene의 DSC에 의(依)한 산화특성(酸化特性) 연구(硏究))

  • Yoo, Chong-Sun;Choi, Seoi-Young;Paik, Nam-Chul
    • Elastomers and Composites
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    • v.18 no.4
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    • pp.140-147
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    • 1983
  • The purpose of this dissertation is to increase oxidation resistance for Polybutadiene & Polyisoprene, and to investigate the energetics of inhibited oxidation of Polybutadiene & Polyisoprene stabilized with various types of antioxidants using DSC. The results of the study are as fellows: 1. In the DSC SCREEN for the onset temperature of oxidation, Polybutadiene was faster than Polyisoprene for the samples containing no antioxidant in air. 2. In the DSC evaluation for Polybutadiene, Recipe BG-4 with 2.0phr compounds of antioxidant was the best effective, and Recipe BS-4 with 2.0phr compounds of antioxidant was the worst effective, and the degrees of effect of antioxidant were exhibited in the ranking of G-1, D, BHT, and SP, roughly. 3. In the DSC evaluation for the Polyisoprene, Recipe IG-4 with 2.0phr compounds of antioxidant was the best effective, and Recipe ID-4 with 2.0phr compounds of antioxidant was the worst effective, and the degrees of effect of antioxidant were exhibited in the ranking of G-1, SP, BHT, and D roughly. 4. In the study on enthalpy which depends on exothermal reaction, the enthalpy of Polyisoprene was gloater than that of Polybutadiene. However, the problem was not solved completely, and it needs further studies.

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UV-Vis Spectra of N, N'-Bis(4′-Aminophenyl)-1,4-quinonenediimine Doped With $H_{4}SiW_{12}O_{40}$

  • Jian Gong;Cui, Xiu-Jun;Chen, Ya-Guang;Xie, Zhong-Wei;Qu, Lun-Yu
    • Macromolecular Research
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    • v.12 no.1
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    • pp.22-25
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    • 2004
  • We have synthesized aniline oligomer composites by using heteropoly acid (H$_4$SiW$_{12}$O$_{40}$ ) as a dopant. The doping and dedoping processes of the aniline oligomer composites were investigated with the aid of UV- Vis spectra. The bands of the aniline oligomer at 572 nm weakened or disappeared, and the bands at 268, 412, and 771 nm appeared, after the aniline oligomer was doped. When the solution of the aniline oligomer doped with H$_4$SiW$_{12}$O$_{40}$ was kept at lower values of pH, the aniline oligomer could not be dedoped by dilution. The turning point of doping and dedoping occurred at pH 5.5. The band at 771 nm shifted towards longer wavelengths when the aniline oligomer composites were synthesized using acetone as the solvent. This observation indicates that the molecular chain became stretched. In addition, we also investigated the change of the electronic absorption spectra of the composites with respect to the time laid up.id up.

A Study on the Considerations for Constructing RDA Application Profiles (RDA 응용 프로파일 구축시 고려사항에 관한 연구)

  • Lee, Mihwa
    • Journal of the Korean BIBLIA Society for library and Information Science
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    • v.30 no.4
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    • pp.29-50
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    • 2019
  • This study was to suggest the considerations for application profiles of 2019 revised RDA using literature reviews and case studies according to new RDA that revised in order to reflect the LRM and linked data. First, the additional elements were recommended as the contents of application profiles such as inverse element, broader element, narrow element, domain, range, alternate label name, mapping to MARC, mapping to BIBFRAME, and RDA description examples as new elements as well as element name, element ID, element URL, description method, vocabulary encoding scheme, data provenance element, data provenance value, and notes as the elements that were already suggested by previous researches. Second, RDA rules' representations in forms of flow chart and application profiles through analyzing RDA rules were suggested in order to apply the rules to RDA application profiles to structure the rules in which every element has 4 types of description method, many conditions, and options. Third, the RDA mapping to BIBFRAME was suggested in RDA application profiles because RDA and BIBFRAME are co-related in context of content standard and encoding format, and mapping BIBFRAME and RDA is necessitated for programming BIBFRAME editors with RDA as content standard. This study will contribute to find the methods for constructing RDA application profiles and BIBFRAME application profiles with RDA as content standard.

Electrical Characterization of Lateral NiO/Ga2O3 FETs with Heterojunction Gate Structure (이종접합 Gate 구조를 갖는 수평형 NiO/Ga2O3 FET의 전기적 특성 연구)

  • Geon-Hee Lee;Soo-Young Moon;Hyung-Jin Lee;Myeong-Cheol Shin;Ye-Jin Kim;Ga-Yeon Jeon;Jong-Min Oh;Weon-Ho Shin;Min-Kyung Kim;Cheol-Hwan Park;Sang-Mo Koo
    • Journal of the Korean Institute of Electrical and Electronic Material Engineers
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    • v.36 no.4
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    • pp.413-417
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    • 2023
  • Gallium Oxide (Ga2O3) is preferred as a material for next generation power semiconductors. The Ga2O3 should solve the disadvantages of low thermal resistance characteristics and difficulty in forming an inversion layer through p-type ion implantation. However, Ga2O3 is difficult to inject p-type ions, so it is being studied in a heterojunction structure using p-type oxides, such as NiO, SnO, and Cu2O. Research the lateral-type FET structure of NiO/Ga2O3 heterojunction under the Gate contact using the Sentaurus TCAD simulation. At this time, the VG-ID and VD-ID curves were identified by the thickness of the Epi-region (channel) and the doping concentration of NiO of 1×1017 to 1×1019 cm-3. The increase in Epi region thickness has a lower threshold voltage from -4.4 V to -9.3 V at ID = 1×10-8 mA/mm, as current does not flow only when the depletion of the PN junction extends to the Epi/Sub interface. As an increase of NiO doping concentration, increases the depletion area in Ga2O3 region and a high electric field distribution on PN junction, and thus the breakdown voltage increases from 512 V to 636 V at ID =1×10-3 A/mm.

The Analysis of Interdigital Bandpass Filter or K-band (Via-Hole 접지를 고려한 K-대역 인터디지트 대역통과 필터분석)

  • 심재우;이영철;김영진
    • Journal of the Korea Institute of Information and Communication Engineering
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    • v.4 no.4
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    • pp.825-834
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    • 2000
  • In this paper, we have designed a bandpass filter with via-holes ground on K-band To pass only the 25 ~30% of the bandwidth at the center frequency of 19.6GHz, we have designed a six-order interdigital bandpass filter using microstrip lines. Simulation results of optimization according to via-holes size and numbers of interdigit bandpass filter shows a excellent agreement with theoretical values on passband frequency. Experimental results of BP filters show that mesaured center frequency is 19.150Hz, insertion loss, -4.1dB, reflection coefficient, -16.7dB. It proved that the vis-holes ground size and numbers must be considered to design the bandpass filter.

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Quantitative analysis of cholesterol in infant formula by isotope dilution liquid chromatography-tandem mass spectrometry (동위원소희석 액체크로마토그래피 질량분석법에 의한 분유 내 콜레스테롤의 정량)

  • Ahn, Eun Jeong;Lee, Hwa Shim;Kim, Byung Joo;Lee, Gae Ho
    • Analytical Science and Technology
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    • v.28 no.6
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    • pp.460-466
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    • 2015
  • An isotope dilution liquid chromatography tandem mass spectrometry was developed as a primary method for the quantitative analysis of cholesterol in infant formula. Cholesterol-d4 was used as an internal standard and spiked into the infant formula sample. In order to release cholesterol out of cholesteryl ester, which is cholesterol bound to fatty acids in infant formula, saponification was carried out. Saponification conditions were optimized with heating temperature, reaction time and the concentration of KOH. The optimum conditions were as follows; heating temperature was 70 ℃, reaction time was 180 min and the concentration of KOH was 0.8 mL of 8 M KOH for about 0.1 g infant formula sample. Extraction of cholesterol out of sample solution was carried out with hexane uisng liquid-liquid extraction. Chromatographic analysis was carried out using Phenomenex Kinetex C18 column. Mobile phase was 0.1% acetic acid in methanol/water (v/v, 99/1) and flow rate was 0.3 mL/min. Cholesterol and cholesterol-d4 were monitored at mass transfer m/z 369/259 and 373/263 respectively. Reproducibility of the method was evaluated to be 0.23% of the measurement result. The expanded uncertainty of the measurement result of cholesterol in infant formula was approximately 1.9% at a 95% confidence level. NIST standard reference material having certified values of cholesterol in infant formula, was analyzed in order to verify this method. The ID-LC/MS/MS results were well agreed with the certified values of NIST SRM within the uncertainty.