• Title/Summary/Keyword: Hot solution method

Search Result 200, Processing Time 0.02 seconds

Inelastic distortional buckling of hot-rolled I-section beam-columns

  • Lee, Dong-Sik
    • Steel and Composite Structures
    • /
    • v.4 no.1
    • /
    • pp.23-36
    • /
    • 2004
  • The inelastic lateral-distortional buckling of doubly-symmetric hot-rolled I-section beam-columns subjected to a concentric axial force and uniform bending with elastic restraint which produce single curvature is investigated in this paper. The numerical model adopted in this paper is an energy-based method which leads to the incremental and iterative solution of a fourth-order eigenproblem, with very rapid solutions being obtained. The elastic restraint considered in this paper is full restraint against translation, but torsional restraint is permitted at the tension flange. Hitherto, a numerical method to analyse the elastic and inelastic lateral-distortional buckling of restrained or unrestrained beam-columns is unavailable. The prediction of the inelastic lateral-distortional buckling load obtained in this study is compared with the inelastic lateral-distortional buckling of restrained beams and the inelastic lateral-torsional buckling solution, by suppressing the out-of-plane web distortion, is published elsewhere and they agree reasonable well. The method is then extended to the lateral-distortional buckling of continuously restrained doubly symmetric I-sections to illustrate the effect of web distortion.

Fabrication and Characterization of High Purity of Fine Alumina from Korean Alunite and Sulfate Salts (국산 명반석과 황산염으로부터 고순도의 미세한 알루미나의 제조 및 특성에 관한 연구)

  • 변수일;이수영;김종희
    • Journal of the Korean Ceramic Society
    • /
    • v.16 no.1
    • /
    • pp.13-20
    • /
    • 1979
  • High purity alumina has been extracted form low grade Korean alunite. Alunite ore was treated by 15% $NH_4OH$ solution, followed by 10% $H_2SO_4$ leaching and metallic impurities such as Fe and Ti were removed by solvent extraction method. Alumina prepared by the extraction process was 99.9% in purity. Hot Petroleum Drying Method has been employed for the preparation of uniformly fine alumina powder, using chemical reagent aluminum sulfate and ammonium aluminum sulfate extrated from Korea alunite. The sinterability of alumina powder prepared by Hot Petroleum Drying Method was shown to be improved in comparison with the one treated by other methods such as ball milling method, but dry pressing was difficult due to the agglomeration of calcined powder. The best slip of alumina powder prepared by Hot Petroleum Drying Method contained a lower soild content than the one treated by other methods. The alumina body formed by soild and drain casting with the former alumina powder showed a higher sintered density.

  • PDF

Preparation and Toughening of Hot-Pressed SiC-AIN Solid Solutions

  • Lim, Chang-Sung
    • The Korean Journal of Ceramics
    • /
    • v.5 no.3
    • /
    • pp.224-229
    • /
    • 1999
  • The preparation and toughening of SiC-AIN solid solution from powder mixtures of $\beta$-SiC, AIN and $\alpha$-SiC by hot-pressing were studied in the 1870 to $2030^{\circ}C$ temperature range. The reaction of AIN and $\beta$-SiC(3C) powders causing transformation to the 2H(wurtzite) structure appeared to depend on hot-pressing temperatures and an additive of $\alpha$-SiC. For the composition of 49wt% SiC with 2 wt% $\alpha$-SiC and 47.5 wt% AIN47.5wt% SiC with 5 wt % $\alpha$-SiC at 203$0^{\circ}C$ for 1 h, th complete solid solutions with a single phase of 2H could be obtained. The appreciable amount of $\alpha$-SiC could develop the columnar inter-grains of 4H phase and the stable 2H phase with the relatively uniform composition and grain size distributions. The effect of $\alpha$-SiC on the phases present and compositional microstructures with columnar inter-grains was invetigated using X-ray diffraction, scanning electron microscopy and transmission electron microscopy. The fracture toughness and Vickers hardness of the hot-pressed solid solutions wre examined by the indentation-fracture-test method.

  • PDF

Combined Effect of Salts Mixture Addition and Brining in Hot Solution on the Korean Pickle Fermentation (오이지의 발효에 미치는 염혼합물 첨가 및 열수담금의 병용효과)

  • Choi, Hee-Sook;Ku, Kyung-Hyung;Kim, Jong-Goon;Kim, Woo-Jung
    • Korean Journal of Food Science and Technology
    • /
    • v.22 no.7
    • /
    • pp.865-870
    • /
    • 1990
  • Four different fermentation methods of Korean cucumber pickles were compared with conventional method, pickling in 10% NaCl solution at $25^{\circ}C$, in order to improve the storage stability. The methods studied were brining the cucumbers in hot($90^{\circ}C$) 10% NaCl solution(method A), addition of KCl and $CaCl_2$ into the hot salt solution(method B) addition of a sodium salts mixture of phosphates, nitrite and citrate into half fermented pickles prepared by method B(method C), substituted nitrite and citrate with KCl in method C(method D). It was found from results that the method C and D reduced the decreasing rate of pH very significantly by more than 3 fold and method B also showed the reducing effect. However, higher total acidity was measured for method C and D, which was opposite to pH results. Changes in hardness of cucumber showed little difference to control while color of brining solution exhibited some difference in their Hunter values. Organoleptic comparison showed a clear effect of salts mixtures by receiving the significant higher scores in fresh cucumber flavor and lower values in yeast moldy and sour flavor for method C and D when those were compared to control.

  • PDF

A Study on the Development of Al Alloy for the Vehicle Connecting Rod Using Hot Forging (열간단조공법을 이용한 컨로드용 Al 합금의 개발에 관한 연구)

  • Kim, S.H.;Hwang, T.M.
    • Journal of Power System Engineering
    • /
    • v.12 no.1
    • /
    • pp.66-71
    • /
    • 2008
  • Alumium alloys hot forging process are gaining increased acceptance in the automotive and electronic industries and hot forging is one of the most efficient manufacturing method for mass product parts. It has been investigated the microstructures and mechanical properties of Al-11.7Si-0.5Mg (KNT40-T6)alloy fabricated by hot forging process for development of connecting rod in this study. The microstructure of hot forged specimen was composed of eutectic structure of alumimum solid solution and $Mg_2Si$ precipitates. The tensile strength of solutionized Al-11.7Si-0.5Mg alloy was 217MPa. This alloy showed a good corrosion resistance using electrochemical polarization test.

  • PDF

Changes in Pectic Substances of Korean Pickled Cucumbers with Different Preparation Methods (담금 방법을 달리한 오이지의 숙성 중 펙틴질의 변화)

  • 장명숙;박미원;박용곤
    • Journal of the Korean Society of Food Science and Nutrition
    • /
    • v.24 no.1
    • /
    • pp.133-140
    • /
    • 1995
  • This investigation was undertaken for the purpose of studying the changes of pectic substances in alcohol insoluble solids(AIS) extracted from cucumbers pickled in salt. The preparation methods were brining the cucumbers in 10% NaCl solution (bolied, method A), 20% NaCl solution(bolied, method B) and 20% NaCl solution(cool to $25^{\circ}C$ after boiling, method C). The composition ratio of hot water soluble pectin(HWSP) in AIS decreased during brining, while that of 0.4% sodium hexametaphosphate soluble pectin(NaSP) increased remarkably. The contents of Ca and Mg in AIS increased regardless of preparation methods used. By DEAE-cellulose chromatography, HWSP from fresh and brined cucumbers were divided into six fracitons. 0.2M peak was the main fraction in fresh cucumber, whereas 0.05M and 0.2M peak were the main fraction in pickled cucumbers. On the other hands, NaSP from fresh and brined cucumbers were divided into five fractions and 0.4M peak was the main fraction. However, the composition ratios of galacturonic acid and neutral sugar of 0.4M fraction in brined cucumbers were higher than those of fresh cucumber.

  • PDF

Carbon Particle-Doped Polymer Layers on Metals as Chemically and Mechanically Resistant Composite Electrodes for Hot Electron Electrochemistry

  • Habiba, Nur-E;Uddin, Rokon;Salminen, Kalle;Sariola, Veikko;Kulmala, Sakari
    • Journal of Electrochemical Science and Technology
    • /
    • v.13 no.1
    • /
    • pp.100-111
    • /
    • 2022
  • This paper presents a simple and inexpensive method to fabricate chemically and mechanically resistant hot electron-emitting composite electrodes on reusable substrates. In this study, the hot electron emitting composite electrodes were manufactured by doping a polymer, nylon 6,6, with few different brands of carbon particles (graphite, carbon black) and by coating metal substrates with the aforementioned composite ink layers with different carbon-polymer mass fractions. The optimal mass fractions in these composite layers allowed to fabricate composite electrodes that can inject hot electrons into aqueous electrolyte solutions and clearly generate hot electron- induced electrochemiluminescence (HECL). An aromatic terbium (III) chelate was used as a probe that is known not to be excited on the basis of traditional electrochemistry but to be efficiently electrically excited in the presence of hydrated electrons and during injection of hot electrons into aqueous solution. Thus, the presence of hot, pre-hydrated or hydrated electrons at the close vicinity of the composite electrode surface were monitored by HECL. The study shows that the extreme pH conditions could not damage the present composite electrodes. These low-cost, simplified and robust composite electrodes thus demonstrate that they can be used in HECL bioaffinity assays and other applications of hot electron electrochemistry.

Development of Nutrient Solution Cooling System in Hydroponic Greenhouse (수경재배 온실의 양액냉각시스템 개발)

  • 남상운;김문기
    • Magazine of the Korean Society of Agricultural Engineers
    • /
    • v.36 no.3
    • /
    • pp.113-121
    • /
    • 1994
  • Since it is difficult to expect the normal production of plants in greenhouses during hot summer season in Korea, certain provisions on the control of extreme environmental factors in summer should be considered for the year-round cultivation in greenhouses. This study was carried out to find a method to suppress the temperature rising of nutrient solution by cooling, which is able to contribute to the improvement of the plant growth environment in hydroponic greenhouse during hot summer season. A mechanical cooling system using the counter flow type with double pipe was developed for cooling the nutrient solution efficiently. Also the heat transfer characteristics of the system was analysed experimentally and theoretically, and compared with the existing cooling systems of nutrient solution. The cooling capacities of three different Systems, which used polyethylene tube in solution tank, stainless tube in solution tank, and the counter flow type with double pipe, were evaluated. The performance of each cooling system was about 41 %, 70% and 81 % of design cooling load in hydroponic greenhouse of 1 ,000m$^2$ on the conditions that the flow rate of ground water was 2m$^3$/hr and the temperature difference between two liquids was 10 ˚C According to the results analysed as above, the cooling system was found to have a satisfactory cooling capability for regions where ground water supply is available. Fer the other regions where ground water supply is restricted, more efficient cooling System should be developed.

  • PDF

Effects of Hot Water and Chilling Treatments of Bulblets Propagated by Tissue Culture on Sprouting and Bulb Development in Korean Native Lilies (조직배양 유래 자생나리 소인경의 온탕 및 저온처리가 맹아 및 비대에 미치는 효과)

  • Kim, Min-Hui;Lim, Young-Hee;Oh, Wook;Yun, Hae-Keun;Kim, Kiu-Weon
    • Horticultural Science & Technology
    • /
    • v.29 no.2
    • /
    • pp.87-94
    • /
    • 2011
  • This study was carried out to investigate the effects of hot solution soaking and chilling treatment on sprouting and enlargement of bulblets obtained through in vitro culture in Korean native lilies with ornamental values. In vitro bulblets of Lilium cernuum, L. hansonii, L. hansonii for. mutatum, L. leichtlinii, and L. tsingtauense were soaked in distilled water or 100 $mg{\cdot}L^{-1}$ $GA_3$ and $GA_{4+7}$ solution maintained at $35^{\circ}C$ for two hours (hot water treatment) and/or exposed at $4^{\circ}C$ for 0, 4, or 8 weeks (chilling treatment) and then planted in plastic trays filled with media and grown in a greenhouse at $20^{\circ}C$ and under 16 h photoperiod. In all species, no bulblet propagated by tissue culture sprouted without chilling or hot water treatment due to dormancy. For dormancy breaking, $GA_{4+7}$ hot solution treatment increasing sprouting by 55-96%, whereas distilled water or GA was not effective in sprouting. Chilling treatment for 4 weeks induced sprouting by 50-70% in L. cernuum and L. leichtlinii, whereas 8 weeks was needed for sprouting of L. hansonii and L. hansonii for. mutatum. Combined treatment of hot water and chilling treatments synergistically promoted sprouting. Especially, in L. cernuum and L. hansonii, $GA_{4+7}$ hot solution soaking prior to chilling for 4 weeks promoted sprouting by 35-45% compared with the reverse order. Enlargement of bulblets resulted from increase in fresh weight and diameter was promoted by the treatments that increased the sprouting percentage of bulblets. Only in L. cernuum, shoots emerged from bulblets soaked in hot $GA_{4+7}$ solution or chilled at $4^{\circ}C$ and shoot emergence rate was highest in bulblets soaked in hot $GA_{4+7}$ solution and then chilled for 8 weeks. From these results, the most effective method for bulblet sprouting and enlargement was to soak in hot $GA_{4+7}$ solution and then chill for 4 weeks in L. hansonii, hansonii for. mutatum, and leichtlinii, and to soak in hot $GA_{4+7}$ solution and then chill for 4 weeks in L. cernuum and tsingtauense.

Manufacturing and Characterization evaluation of mulberry concentrate for food additive (식품첨가제용 뽕잎 농축액의 제조 및 특성평가)

  • Kim, Hyun-Bok;Seok, Young-Seek
    • Journal of Sericultural and Entomological Science
    • /
    • v.51 no.2
    • /
    • pp.180-184
    • /
    • 2013
  • Study on extraction and concentration of mulberry leaf were performed to increase utilization as new source of food additives. We analyzed extraction method in EtOH, sugar and hot water solution. The desirable method was 70% alcoholic extraction. Color of concentrate was comparatively stable in 70% alcoholic extraction solution and sugar solution. But hot water extraction was showed color change with brown. By filtering of concentrate in 70% alcoholic extraction and sugar extraction, we removed a deposits. Also, we investigated characteristics of the concentrate from mulberry leaf.