• Title/Summary/Keyword: High temperature stability

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Fabrication of Tantalum Nitride Thin-Film as High-temperature Strain Gauges (고온 스트레인 게이지용 질화탄탈박막의 제작)

  • 김재민;최성규;남효덕;정귀상
    • Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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    • 2001.11a
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    • pp.97-100
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    • 2001
  • This paper presents the characteristics of Ta-N thin-film strain gauges as high-temperature strain gauges, which were deposited on Si substrate by DC reactive magnetron sputtering in an argon-nitrogen atmosphere(Ar-(4∼16 %)N$_2$). These films were annealed for 1 hour in 2x10$\^$-6/ Torr vaccum furnace range 500∼1000$^{\circ}C$. The optimized conditions of Ta-N thin-film strain gauges were annealing condition(900$^{\circ}C$, 1 hr.) in 8% N$_2$ gas flow ratio deposition atmosphere. Under optimum conditions, the Ta-N thin-films for strain gauges is obtained a high resistivity, $\rho$=768.93 ${\mu}$Ω cm, a low temperature coefficient of resistance, TCR=-84 ppm/$^{\circ}C$ and a high temporal stability with a good longitudinal gauge factor, GF=4.12.

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Effects of Ca/Si Molar Ratio on the Interatomic Distance of Synthetic Calcium Silicate Hydrate (C-S-H) at Elevated Temperature (고온 가열시 Ca/Si 몰비율에 따른 합성 칼슘 실리케이트 수화물(C-S-H)의 구성 원자간 거리 변화)

  • Im, Su-Min;Bae, Sung Chul
    • Proceedings of the Korean Institute of Building Construction Conference
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    • 2021.05a
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    • pp.144-145
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    • 2021
  • Calcium silicate hydrate(C-S-H) is the principal binding phase that controls the strength and thermal stability of concrete. However, the effects of high temperature on the lattice structure and interatomic structure of C-S-H remains poorly understood due to its nanocrystallinity. This study aims to elucidate the change in interatomic distance of synthetic C-S-H with different Ca/Si molar ratios after exposure to high temperature via high energy X-ray scattering experiment which is a powerful analytical tool for amorphous materials.

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Improvement of low temperature thermal stability on PVC (PVC의 저온 열안정성 향상에 관한 연구)

  • Chung, Kwang-Bo;Jeon, In-Ki;Ahn, Sung-Hwan
    • Journal of the Korean Applied Science and Technology
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    • v.26 no.4
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    • pp.440-450
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    • 2009
  • Metal(Zinc) soap and mixed metal(Zn/Ba) soap were synthesized with good structures and characterized by IR and H-NMR. The H-NMR spectrums of the synthesized soaps were in very good accordance with the structures proposed by earlier workers. The mixed metal soaps with various costabilizers(acid or metal content effect), which added in order to investigate the thermal stabilization effect at low and high temperature, were investigated the thermal stabilization effect. The temperature effect is relation to the metal content effect than acid effect. In case of mixed metal soap, the high thermal stabilization effect improved with increasing Barium content. As the Zinc content increase the low temperature thermal stabilization effect improved, but the high temperature thermal stabilization effect showed an opposite tendency.

The Fabrication of Ceramic Thin-Film Type Pressure Sensors for High-Temperature applications (고온용 세라믹 박막형 압력센서의 제작)

  • Kim, Jae-Min;Choi, Sung-Kyu;Chung, Gwiy-Sang
    • Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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    • 2002.11a
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    • pp.456-459
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    • 2002
  • This paper describes fabrication and characteristics of ceramic pressure sensor for working at high temperature. The proposed pressure sensor consists of a Ta-N thin-film, patterned on a Wheatstone bridge configuration, sputter deposited onto thermally oxidized Si membranes with an aluminium interconnection layer. The fabricated pressure sensor presents a low temperature coefficient of resistance, high sensitivity, low non-linearity and excellent temperature stability. The sensitivity is 1.097~1.21mV/$V{\cdot}kgf/cm^2$ in the temperature range of $25{\sim}200^{\circ}C$ and the maximum non-linearity is 0.43 %FS.

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Effect of C, Mn and Al Additions on Tensile and Charpy Impact Properties of Austenitic High-manganese Steels for Cryogenic Applications (극저온용 오스테나이트계 고망간강의 인장 및 충격 특성에 미치는 C, Mn, Al 첨가의 영향)

  • Lee, Seung-Wan;Hwang, Byoungchul
    • Korean Journal of Materials Research
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    • v.29 no.3
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    • pp.189-195
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    • 2019
  • The effect of C, Mn, and Al additions on the tensile and Charpy impact properties of austenitic high-manganese steels for cryogenic applications is investigated in terms of the deformation mechanism dependent on stacking fault energy and austenite stability. The addition of the alloying elements usually increases the stacking fault energy, which is calculated using a modified thermodynamic model. Although the yield strength of austenitic high-manganese steels is increased by the addition of the alloying elements, the tensile strength is significantly affected by the deformation mechanism associated with stacking fault energy because of grain size refinement caused by deformation twinning and mobile dislocations generated during deformation-induced martensite transformation. None of the austenitic high-manganese steels exhibit clear ductile-brittle transition behavior, but their absorbed energy gradually decreases with lowering test temperature, regardless of the alloying elements. However, the combined addition of Mn and Al to the austenitic high-manganese steels suppresses the decrease in absorbed energy with a decreasing temperature by enhancing austenite stability.

Anode-supported Type SOFCs based on Novel Low Temperature Ceramic Coating Process

  • Choi, Jong-Jin;Ahn, Cheol-Woo;Kim, Jong-Woo;Ryu, Jungho;Hahn, Byung-Dong;Yoon, Woon-Ha;Park, Dong-Soo
    • Journal of the Korean Ceramic Society
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    • v.52 no.5
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    • pp.338-343
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    • 2015
  • To prevent an interfacial reaction between the anode and the electrolyte layer during the conventional high-temperature co-firing process, an anode-supported type cell with a thin-film electrolyte was fabricated by low-temperature ceramic thick film coating process. Ni-GDC cermet composite was used as the anode material and YSZ was used as the electrolyte material. Open circuit voltage and maximum power density were found to strongly depend on the surface uniformity of the anode functional layer. By optimizing the microstructure of the anode functional layer, the open circuit voltage and maximum powder density of the cell increased to 1.11 V and $1.35W/cm^2$, respectively, at $750^{\circ}C$. When a GDC barrier layer was applied between the YSZ electrolyte and the LSCF cathode, the cell showed good stability, with almost no degradation up to 100 h. Anode-supported type SOFCs with high performance and good stability were fabricated using a coating process.

Mechanical deterioration and thermal deformations of high-temperature-treated coal with evaluations by EMR

  • Biao Kong;Sixiang Zhu;Wenrui Zhang;Xiaolei Sun;Wei Lu;Yankun Ma
    • Geomechanics and Engineering
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    • v.32 no.2
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    • pp.233-244
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    • 2023
  • With the increasing amount of resources required by the society development, mining operations go deeper, which raises the requirements of studying the effects of temperature on the physical and mechanical properties of coal and adjacent rock. For now, these effects are yet to be fully revealed. In this paper, a mechanical-electromagnetic radiation (EMR) test system was established to understand the mechanical deterioration characteristics of coal by the effect of thermal treatment and its deformation and fracture characteristics under thermo-mechanical coupling conditions. The mechanical properties of high-temperature-treated coal were analyzed and recorded, based on which, reasons of coal mechanical deterioration as well as the damage parameters were obtained. Changes of the EMR time series under unconstrained conditions were further analyzed before characteristics of EMR signals under different damage conditions were obtained. The evolution process of thermal damage and deformation of coal was then analyzed through the frequency spectrum of EMR. In the end, based on the time-frequency variation characteristics of EMR, a method of determining combustion zones within the underground gasification area and combustion zones' stability level was proposed.

Recent Progress in Cathode Materials for Thermal Batteries

  • Ko, Jaehwan;Kang, Seung Ho;Cheong, Hae-Won;Yoon, Young Soo
    • Journal of the Korean Ceramic Society
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    • v.56 no.3
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    • pp.233-255
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    • 2019
  • Thermal batteries are reserve batteries with molten salts as an electrolyte, which activates at high temperature. Due to their excellent reliability, long shelf life, and mechanical robustness, thermal batteries are used in military applications. A high-performance cathode for thermal batteries should be considered in terms of its high capacity, high voltage, and high thermal stability. Research progress on cathode materials from the recent decade is reviewed in this article. The major directions of research were surface modification, compounding of existing materials, fabrication of thin film cathode, and development of new materials. In order to develop a high-performance cathode, a proper combination of these research directions is required while considering mass production and cost.

An Analytical Study on the Thermal-Structure Stability Evaluation of Mill-Turn Spindle with Curvic Coupling (커빅 커플링을 적용한 밀-턴 스핀들의 열-구조 안정성 평가에 관한 해석적 연구)

  • Lee, Choon-Man;Jeong, Ho-In
    • Journal of the Korean Society of Manufacturing Process Engineers
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    • v.19 no.1
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    • pp.100-107
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    • 2020
  • As demand for high value-added products with hard materials increases, the line center is used for producing high value-added products in many industries such as aerospace, automobile fields. The line center is a key device for smart factory automation that can improve the production efficiency and the productivity. Therefore, the development of a mill-turn line center is necessary to produce high value-added products with complex shapes flexibly. In the mill-turn process, a milling process and a turning process are combined. In particular, the turning process needs to increase the rigidity of the spindle. The purpose of this study is to analyze the thermal-structural stability through thermo-structural coupled analysis for a mill-turn spindle with a curvic coupling. The maximum temperature and thermal stability of the spindle were analyzed by thermal distribution. In addition, the thermal deformation and thermal-structural stability of the spindle were analyzed through thermo-structural coupled analysis.

Study of Structural Stability for H-section Beams Made of Fire Resistant Steels (FR 490) at High Temperatures by Analytical Method (건축용 내화강재(FR 490) 적용 H형강 보부재의 고온내력 연구)

  • Kwon, In-Kyu
    • Fire Science and Engineering
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    • v.28 no.5
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    • pp.52-57
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    • 2014
  • When structural elements of steel framed structures are exposed to fire situations, the structural stability begins to decrease due to dislocation of substantial. The increase of the beam length causes an additional stress and deflection. These can be serious factors to cause a severe failure of structures. To improve the fire resistance of beams, prevention of the heat from a fire by coating with fire protection material is essential for beams. The FR 490 was developed to enhance fire resistance compared with SM 490 steel. However, the fire resistance of FR 490 H-beams has not been evaluated by analysis method since it was developed. In this paper, materials properties in high temperature and a heat transfer and thermal stress theory were used in the evaluation of the fire resistance of FR490 H-beams. The fire resistance of FR490 steel beams was compared with that of SM490 beams. The comparison verified that the structural stability of FR490 beams at high temperature was superior to that of SM490 beams.