• Title/Summary/Keyword: High isostatic pressure

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Structure and field emission properties of carbon-nitrogen (CN) nanofibers obtained by hot isostatic pressure (Hot isostatic pressure을 이용한 CN nanofiber의 구조 및 전계방출 특성)

  • Lee, Yang-Doo;Blank, V.D.;Batov, D.V.;Buga, S.G;Nahm, Sahn;Lee, Yun-Hi;Ju, Byeong-Kwon
    • Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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    • 2003.04a
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    • pp.84-87
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    • 2003
  • Carbon-nitrogen (CN) nanofibers have been produced using a water cooled hot isostatic pressure (HIP) apparatus. The CN nanofibers were grown in random with the diameter of about 100-150nm and length over $10{\mu}m$. Emission properties of CN nanofibers were investigated for spacing, between anode and cathode, variation. Then turn-on fields about $1.4V/{\mu}m$. The time reliability and light emission test were carried out for above 100 hours. We suggest that CN nanofibers can be possibly applied to high brightness flat lamp because of low turn-on field and time reliability.

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Analyses of Sever Plastic Deformation Behavior of Hot Isostatic Pressed Ni-base Superalloy during High Pressure Torsion Process (열간정수압성형공정으로 제조된 니켈기 초내열합금의 고압비틀림 공정을 통한 강소성 변형거동 분석)

  • Lee, D.J.;Lee, Y.;Kim, H.-K.;Kwon, Y.-N.;Kim, H.S.;Yoon, E.Y.
    • Transactions of Materials Processing
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    • v.25 no.4
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    • pp.254-260
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    • 2016
  • In this study, hot isostatic pressed Ni-base superalloy was subjected by high-pressure torsion process to improve the dispersion of gamma prime phase, mechanical properties and remove prior particle boundaries. The resulting microstructural size decreases and prior particle boundaries removed with increasing strain by high-pressure torsion process. Moreover, the microhardness values and room temperature tensile strength were enhanced. However, the tensile elongation was decreased as increasing strain due to fast crack propagation along the refined and well dispersed gamma prime particles.

Tribological Properties of Ti(C,N)-based Cermet after Hot Isostatic Pressing at High Nitrogen Pressure

  • Xiong, Wei-hao;Zheng, Li-yun;Yan, Xian-mei
    • Proceedings of the Korean Powder Metallurgy Institute Conference
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    • 2006.09a
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    • pp.663-664
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    • 2006
  • Sintered Ti(C,N)-based cermets were treated with hot isostatic pressing (HIP) at different nitrogen pressures. The tribological properties of the treated cermets have been evaluated. The results show that a hard near-surface area rich in TiN formed after HIP treatment. The cermets treated at higher pressure had a relatively lower friction coefficient and specific wear rate. In all cases the microhardness of treated cermets is higher than that without HIP natridation. The wear mechanisms of cermets were hard particle flaking-off and ploughing. It was also found that the HIP natridation is well-suited for improving the tribological properties of cermets.

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Structure and Electron Emission Properties of CN Nanostructures Obtained by HIP Apparatus (HIP에 의해 합성된 CN nanostructures의 구조 및 전계방출 특성)

  • 오정근;이양두;문승일;양석현;이윤희;김남수;주병권
    • Journal of the Korean Institute of Electrical and Electronic Material Engineers
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    • v.16 no.8
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    • pp.723-730
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    • 2003
  • The CN(carbon nitrogen) nanofibers were formed by HIP(high isostatic pressure) process. From the field emission measurement, CN nanofibers shows an excellent characteristics of emitter, better than CNTs and carbon nanofibers. The structures obtained can be divided into three groups : bamboo-like fibers, corrugated structures and bead necklace-like fib res. Emission properties of CN nanofibers were investigated for spacing, between anode and cathode, variation. Turn-on fields was 1.4 v/$\mu\textrm{m}$. The time reliability and light emission test were carried out for about 100 hours. We suggest that CN nanofibers can be possibly applied to the high brightness flat lamp because of low turn-on field and time reliability

Cold Isostatic Pressing and Sintering Behavior of (Al +12.5%Cu)3Zr Nanocrystalline Intermetallic Compound Synthesized by Mechanical Alloying (기계적합금화한 (Al +12.5%Cu)3Zr 초미립 금속간화합물의 CIP 성형 및 소결 거동)

  • Moon, H.G.;Hong, K.T.;Kim, S.J.
    • Korean Journal of Materials Research
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    • v.12 no.8
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    • pp.634-640
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    • 2002
  • To improve the ductility of mTEX>$(Al +12.5%Cu)<_3$Zr intermetallics, which are the potential high temperature structural materials, the mechanical alloying behavior, the effect of pressure and temperature on the $Ll_2$, phase formation and the behavior of the cold isostatic press and sintering were investigated. However mechanically alloyed A1$_3$Zr alloy have been known to have high mechanical strength even at high temperature, its workability was poor. A method of solution is refined grain size and phase transformation from $DO_{23}$ to $Ll_2$.$ Ll_2$ structure TEX>$(Al+12.5%Cu)<_3$Zr with nanocrystalline microstructure intermetallic powders where were prepared by mechanical alloying of elemental powders. Grain sizes of the as milled powders were less than 10nm (from transmission electron microscopy, TEM). Thermal analyses showed that $Ll_2$ structure was stable up to$ 800^{\circ}C$ for 1hour $(Al+ 12.5%Cu)<_3$Zr. $(Al+12.5%Cu)<_3$Zr has been consolidated by cold isostatic pressing (CIP 138, 207, 276, 414MPa) at room temperature and subsequent heat treatment at high temperatures where $Ll_2$ structure was stable under vacuum atmosphere. The results showed that 94.2% density of Ll$_2$ compacts was obtained for the (Al +12.5%Cu)$_3$Zr by sintering at 80$0^{\circ}C$ for 1hour (under CIPed 207MPa). This compact of the grain size was 40nm.

High Temperature Densification Forming Process of Tool Steel Powder Compact (공구강 분말 성형체의 고온 치밀화 성형공정)

  • Choi, Hak-Hyeon;Jeon, Yun-Cheol;Kim, Gi-Tae
    • Transactions of the Korean Society of Mechanical Engineers A
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    • v.20 no.7
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    • pp.2182-2195
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    • 1996
  • Densification characteristics and behavior of tool steel powder compact during high temperature forming processes were investigated under pressure less sintering, sinter forging and hot isostastic pressing. In pressureless sintering, full density was obtained at a closely controlled temperature near the solidus of the material. Finite element calculations from constitutive model for densification by power law creep and diffusional flow were compared with experimental data. Agreements between theoretical calculations and experimental data were good in hot isostatic pressing but not as good in sinter forging.

Effect of Organic Additive Composition on Isostatic Thermocompression Behavior of Alumina Tapes (유기물 조성에 따른 알루미나 테이프의 열간 가압 거동)

  • 이명현;박일석;김대준;이득용
    • Journal of the Korean Ceramic Society
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    • v.37 no.8
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    • pp.824-831
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    • 2000
  • Alumina tapes, having various ratios of alumina to alumina+binder+plasticizer (a/(a+o)) and binder to binder+plasticizer(b/(b+p)), were prepared by the tape casting method. The tapes were thermocompressed varying the thermocompression parameters such as temperature, pressure, and duration time. Among the parameters, the pressure was the most influential to the tape packing density. The packing density varied in two different ways depending on the a/(a+o) ratio. For the tapes having low a/(a+o) ratio, a saturation density was reached by applying very a low pressure of 1 MPa. For tapes with high a/(a+o), on the contrary, the saturation density was obtained at a relatively high pressure. These different responses to the pressure are attributed to the fact that the rearrangement of alumina particles by the pressure becomes easy as an organic content in the tapes is high.

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Overview of CSNS tantalum cladded tungsten solid Target-1 and Target-2

  • Wei, Shaohong;Zhang, Ruiqiang;Ji, Quan;Li, Changfeng;Zhou, Bin;Lu, Youlian;Xu, Jun;Zhou, Ke;Zhao, Chongguang;He, Ning;Yin, Wen;Liang, Tianjiao
    • Nuclear Engineering and Technology
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    • v.54 no.5
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    • pp.1535-1540
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    • 2022
  • A solid tungsten target was used at the China Spallation Neutron Source (CSNS) with 100 kW proton beam power. To improve the lifetime, hot isostatic pressing (HIP) process was selected to bond tantalum cladding with tungsten plates. Radioactive isotope 182Ta, an activation product of tantalum, was found in the cooling water after a period of operation, however, no radioactive isotopes of 187W was found, which shows the tantalum layer remained mostly intact. The CSNS Target-1 had been operating safely for three years and was replaced by Target-2 in August 2020.

Effect of Processing Variables on the Texture of Ni Substrate for YBCO Coated Conductor (YBCO 박막선재용 Ni 기판의 집합도에 미치는 제조공정 변수효과)

  • 지봉기;임준형;이동욱;주진호;나완수;김찬중;홍계원
    • Journal of the Korean Institute of Electrical and Electronic Material Engineers
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    • v.16 no.10
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    • pp.938-945
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    • 2003
  • We fabricated Ni-substrate for YBCO coated conductors and evaluated the effects of pressing and annealing temperature and time on texture. Ni substrate was fabricated by powder metallurgy technique and compacts were prepared by applying uniaxial or isostatic pressure. The texture of substrate made by applying cold isostatic pressure (CIP) was stronger than that by uniaxial pressure which we attribute to the fact that the CIP method provided higher density and more uniform density distribution. It was observed that the substrate annealed at 400 C showed both retained texture and recrystallized texture. On the other hand, the texture of substrate significantly improved at annealing temperature above 500 C, forming strong 4-fold symmetry, [111] II ND texture, and FWHM of 9∼10 . It is to be noted that the degree of texture was almost independent of annealing temperature (500∼1000 C) and annealing time(1∼54 min, at 1000 C). EBSD and AFM analysis indicated that 99% of grain boundaries was low angle grain boundary and RMS was approximately 3 nm, respectively. Development of strong cube texture and high fraction of low angle grain boundary of Ni-substrate made by powder metallurgy technique in our study is considered to be suitable for the application of YBCO coated conductors.

Development of New Micro Pattern Fabrication Process by U sing Isostatic Pressing (정수압을 이용한 미세 패턴 전사 신공정 개발)

  • Seol, J.W.;Joo, B.Y.;Rhim, S.H.
    • Proceedings of the Korean Society for Technology of Plasticity Conference
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    • 2009.10a
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    • pp.267-270
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    • 2009
  • In the present investigation, we are newly developing a new forming process which can fabricate micro patterns on large-area polymeric substrates for high speed mass production. The key idea of the new process is to pressurize multiple vacuum-packed substrate-mold stacks above the glass transition temperature ($T_g$) of the polymeric substrates. The new process is thought to be promising micro-pattern fabrication technique in three aspects; firstly, isostatic pressing ensures the uniform micro-pattern replicating condition regardless of the substrate area. Secondly, the control of forming condition such as temperature and pressure can realize well-defined process condition exploited in the conventional hot embossing research field. Thirdly, multiple substrates can be patterned at the same time. A prototype forming machine for the new process was developed with the design consideration realizing the present idea. With a developed machine, micro prismatic array patterns with 50 um in size were successfully made on the $380{\times}300{\times}6\;mm$ PMMA plate.

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