• Title/Summary/Keyword: Heat treatment time

Search Result 1,452, Processing Time 0.029 seconds

The Effect of Ageing on Grain Refinement of CuAlNi Shape Memory Alloy (CuAlNi 형상기억합금의 결정립 미세화에 따른 시효효과)

  • Yang, G.S.;Park, C.S.;Jang, W.Y.
    • Journal of the Korean Society for Heat Treatment
    • /
    • v.8 no.1
    • /
    • pp.65-74
    • /
    • 1995
  • This research was performed to investigate the effect of ageing on grain refinement of 82wt%Cu-13.5wt%Al-4.5wt%Ni-0.1wt% misch metal alloy with ageing temperature and time. The results obtained in this study are as follows; The variation of transformation temperature with ageing temperature had very influence on ageing time at $300^{\circ}C$. But it had not influence on ageing time at $100^{\circ}C$. The variation of transformation temperature after second reversed transformation cycle was not occured in martensitic phase ageing, but $M_s$ point was appeared equally with third reversed transformation cycle in parent phase ageing. The variation of $M_s$ point was not nearly with ageing time at $100^{\circ}C$ ageing temperature. But it was decreasing with ageing time at $300^{\circ}C$ ageing temperature and $A_s$ point was increasing with ageing time. Structure of parent phase ageing was being M18R martensitic and N2H martensitic phase. It was found that ${\alpha}$ and ${\gamma}_2$ phase were created by ageing of long time at $300^{\circ}C$ ageing temperature.

  • PDF

Fatigue Characteristics and FEM Analysis of $18\%$Ni(200) Maraging Steel (18Ni 마르에이징강의 피로특성 및 유한요소해석)

  • Choi Byung Ki;Jang Kyeung Cheun
    • Transactions of the Korean Society of Machine Tool Engineers
    • /
    • v.14 no.2
    • /
    • pp.75-82
    • /
    • 2005
  • Recently the needs of high reliable substances of high strength and high ductility are gradually increased with the development of aerospace industry. The characteristics of maraging steel has high ductililty, formability, corrosion resistant and high temperature strength and is easy to fabricate, weld and treat with heat, and maintain an invariable size even after heat treatment. e steels are furnished in the solution annealed condition and they achieve full properties through martensitic precipitation aging a relatively simple, low temperature heat treatment. As is true of the heat treating procedures, aging is a time/temperature dependent reaction. Therefore, the objective of this stud)'was consideration of fatigue characteristics according as Nb(niobium) content and time/temperature of heat treatment change. Also the stress analysis, fatigue lift, and stress intensity factor were compared with experiment results and FEA(finite element analysis) result. The maximum ftresses of)( Y, and Z axis direction showed about $2.12\times$10$^{2}$MPa, $4.40\times$10$^{2}$MPa and $1.32\times$10$^{2}$MPa respectively. The fatigue lives showed about $7\%$ lower FEA result than experiment result showing almost invariable error every analyzed cycle. Stress intensity factor of the FEA result was lower about $3.5~ 10\%$ than that of the experiment result showing that the longer fatigue crack ten添 the hi인or error. It considered that the cause for the difference was the modeled crack tip having always the same shape and condition regardless of the crack growth.

Thermal conductivity analysis of Al/graphite composite fabricated by a mechanical alloying (기계적 합금법에 의한 Al/graphite 복합체 제조 및 열전도도 특성 분석)

  • Lee, Jung-Il;Kim, Tae Wan;Yoon, Yo Han;Cho, Hyun Su;Ryu, Jeong Ho
    • Journal of the Korean Crystal Growth and Crystal Technology
    • /
    • v.26 no.4
    • /
    • pp.155-158
    • /
    • 2016
  • Thermal conductivity is a very important factor for applicability and reliability in electrical devices. In this study, Al/graphite composite is fabricated by a mechanical alloying and heat-treatment and its physical properties are characterized. The XRD peak intensity of the $Al_4C_3$ ceramic phase observed in the heat-treated Al/graphite composite increased with heat-treatment temperature and time. The thermal conductivity of the heat-treated Al/graphite composite sample was very lower than that of the pure Al sample, and increased with heat-treatment temperature and time.

Improvement of protein extraction efficiency from defatted sesame meal with thermal and enzymatic treatments (열 처리와 효소 처리에 의한 탈지 참깨박 단백질의 추출율 향상)

  • In, Man-Jin
    • Journal of Applied Biological Chemistry
    • /
    • v.63 no.4
    • /
    • pp.291-295
    • /
    • 2020
  • In order to increase the utilization of defatted sesame meal (DSM), a by-product of sesame oil production, the conditions of extraction of insoluble proteins from DSM by enzyme treatment were investigated. As a result of comparing the treatment results of proteolytic enzymes Alcalase, Flavorzyme, Neutrase, and Protamex with control, Protamex was effective in increasing the total solid and protein content. At the reaction conditions of Protamex (50 ℃, pH 6.0), the dosage of enzymes was appropriate for 1% of DSM and 3 h of enzyme reaction time. To improve the efficiency of enzymatic treatment, the protein content extracted increased as the heat treatment temperature increased, and slightly increased above 110 ℃. As a result of investigating the effect of the combination treatment of cell lytic enzyme (Tunicase) and protease (Protamex) on protein solubilization, it was most effective to treat the cell lytic enzyme after processing the protease. After heat treatment (110 ℃, 10 min), sequential treatment of Protamex and Tunicase increased the protein content by about 3.5 times (9.85→35.58 mg/mL) of the non-heated control and 2.2 times (15.83→35.58 mg/mL) of the heat treated control.

RRA Treatment of Semi-Solid Al-Zn-Mg-Cu Al Alloy Fabricated by Cooling Plate (냉각판으로 제조된 Al-Zn-Mg-Cu계 반응고 알루미늄 합금의 RRA 처리)

  • Kim, Dae-Hwan;Shim, Sung-Yong;Kim, Young-Hwa;Lim, Su-Gun
    • Journal of Korea Foundry Society
    • /
    • v.29 no.6
    • /
    • pp.265-269
    • /
    • 2009
  • The optimum RRA heat treating conditions and SCC (stress corrosion cracking) resistance of semi-solid Al-Zn-Mg-Cu alloy fabricated by inclined cooling plate were compared with those of conventional mould cast alloys. The non-stirring method characterized by using a cooling plate can effectively eliminate dendritic structure and form a fine globular semisolid microstructure in as-cast Al-Zn-Mg-Cu alloy and the SCC resistance of semi-solid Al-Zn-Mg-Cu alloy was higher than that of conventional mold cast alloy. Also, after retrogressed treatment at RRA heat treatment of semi-solid Al-Zn-Mg-Cu alloy, retrogressed treatment time has increased more than 10 minutes at $180^{\circ}C$ to recovery the T6 heat treatment strength.

Enhancement of Hydrophobicity by a Heat Treatment of Zinc Aluminate Thin Film Deposited on Glass Substrate (글라스 기판 위에 증착된 Zin Aluminate 박막의 열처리를 통한 소수성 특성의 향상)

  • Seo, Sang-Young;Yoon, Soon-Gil
    • Journal of the Korean Institute of Electrical and Electronic Material Engineers
    • /
    • v.33 no.4
    • /
    • pp.249-254
    • /
    • 2020
  • An 80 nm thick zinc aluminate thin film was deposited on a glass substrate via radio-frequency (rf) magnetron sputtering and heat treated to analyze changes in the wetting angles due to a surface modification. The thin films were modified from hydrophilic to hydrophobic by a simple thermal treatment. The surface modification from a heat treatment increased the wetting angles up to 111°, which was explained by the relationship with the excess surface area. The wetting angles of the annealed thin films decreased with increasing exposure time under ambient conditions, which was attributed to the oxygen vacancies in the films that were introduced during deposition. The annealed thin films were treated by ionized oxygen via oxygen plasma. After the oxygen plasma treatment, the decreased wetting angles were maintained at ~95° for 11 days.

A Study on the Allergenicity of Egg Protein (달걀 단백질의 Allergenicity에 관한 연구)

  • 정은자
    • The Korean Journal of Food And Nutrition
    • /
    • v.11 no.2
    • /
    • pp.228-236
    • /
    • 1998
  • Egg is an important foods containing many good proteins. But it is well known that egg protein has a lot of allergenicity. The purpose of this study is to develop the methods to reduce the allergenicity of egg. I tried various experimental methods ; For example, heat treatment, irradiation with ultraviolet and microwaves, treatment with polyphosphate, enzyme hydrolysis and PCA inhibition test using guinea pigs and degrees of hydrolysis. The results obtained were as follows ; 1. Heat treatment reduced allergenicity of egg protein. The longer the heat time, the better the effect. 2. Irradiating with ultraviolet and microwave increased both the degree of protein hydrolysis and PCA inhibition reduced the allergenicity. Ultraviolet was more effective than microwaves on egg protein. Fertilized eggs did not reduce allergenicity. 3. Enzyme treatment increased the degree of hydrolysis and PCA inhibition, and reduced allergenicity considerably. Alcalase was more effective than neutrase. 4. Adding polyphosphate did not induced protein hydrolysis, but increased PCA inhibition and reduced allergenicity. 5. The picture of various treatments of egg gel by SEM showed a light surface which indicated that protein was desolved. Neutrase was lighter than alcalase, and the longer the heating time, the lighter the surface became. 6. Measurements of the hardness of egg gel by Instron showed that the longer the reaction time with enzyme, the softer it became.

  • PDF

Formation of Indole Glucosinolates Breakdown Products during Processing Treatment in Cruciferous Vegetables (십자화과 채소의 가공처리 중 Indole Glucosinolate의 분해산물 형성)

  • Shim, Ki-Hwan;Kang, Kap-Suk;Sung, Nack-Kie;Seo, Kwon-Il;Moon, Ju-Seok
    • Journal of the Korean Society of Food Science and Nutrition
    • /
    • v.21 no.1
    • /
    • pp.49-53
    • /
    • 1992
  • The released amount of thiocyanate ion in Cruciferous vegetables treated by wet heat, increased as the reaction time goes by and was maximum value after treatment for 30min, but it was not changed by dry heat treatment. When samples were autolyzed by myrosinase, the amount of thiocyanate ion increased gradually as time goes by, was maximum value after 3hrs and much higher than those in the sample treated by wet. The released amount of thiocyanate ion in each sample showed much in cabbage, Chinese cabbage, radish, kale and mustard in the order. The generated amount of indoleacetonitrile by heat treatment increased as time goes by and the generated amount in each sample determined was high in the order of cabbage, Chinese cabbage and radish.

  • PDF

Study on the Mechanical Properties of Mo Series High Speed Tool Steel Austempered (Mo계 고속도 공구강의 오스템퍼렁에 따른 기계적 성질에 관한 연구)

  • Choi, M.S.;Lee, H.W.;Rho, Y.S.;Kim, Y.H.;Kim, H.G.;Lee, S.Y.
    • Journal of the Korean Society for Heat Treatment
    • /
    • v.4 no.1
    • /
    • pp.1-12
    • /
    • 1991
  • This study has been performed to find out the effect of austenitizing temperature, austempering temperature and its holding time, and tempering cycle on the mechanical properties such as impact resistance, hardness etc. of AISI $M_2$ Mo series high speed tool steel austempered or tempered after austempering treatment. The results obtained from the experiment are as follows ; (1) Optical micrograph has revealed that the transformation rate of bainite is delayed as the austenitizing temperature increases and that bainite is most apparently transformed at an austempering temperature of $290^{\circ}C$. (2) The amount of retained austenite during austempering has been analysed to be increased by the X-ray diffraction technique as the transformation product of bainite is increased. It has also been shown that the longer the holding time of austempering, the more the transformation quantity of bainite is formed, exhibiting, however, that the rate of bainitic transformation is considerably retarded after a certain period of holding time elapses. (3) Hardness measurement has shown that hardness values obtained after austempering increase with decreasing the amount of retained austenite. (4) The austempering and then tempering cycle has been formed to give hardness values which are more greatly improved as austenitizing temperature is increased. (5) The mechanical property of the specimen primary-tempered for 1 hour at $550^{\circ}C$ after austempering for 2 hours at $290^{\circ}C$ from the austenitizing temperature range of $1180^{\circ}C$ to $1210^{\circ}C$ have been estimated to be good values.

  • PDF

Study on the Surface Temperature and Laser Heat Conduction by the Computer Algorithm (컴퓨터 알고리즘에 의한 표면온도와 레이저 열전도에 관한 연구)

  • Lee, Young-Wook
    • The Journal of Information Technology
    • /
    • v.9 no.3
    • /
    • pp.67-75
    • /
    • 2006
  • This study deals with the computing the temperature change of surface to the increment of time and diffusivity, the heat flux during irradiation of laser. In addition, the computer algorithm for computing the penetration change of the corresponding surface irradiated is developed. The result of this study shows the possibility to treatment of cancer, abnormal cell and biological tissue during irradiation of laser.

  • PDF