• Title/Summary/Keyword: Grinding technique

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Enhancement of Dissolution Properties of Ketoprofen from Ground Mixtures with Chitin or Chitosan

  • Koh, Ik-Bae;Shin, Sang-Chul;Lee, Yong-Bok
    • Journal of Pharmaceutical Investigation
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    • v.16 no.1
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    • pp.36-41
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    • 1986
  • The ground mixtures of ketoprofen with chitin or chitosan were prepared by grinding in a ball mill to increase the dissolution rate. The ground mixture showed a faster and more enhanced dissolution rate than the physical mixture or intact ketoprofen. The X-ray diffraction peaks indicated the production of the amorphous form of ketoprofen in the ground mixture. An interaction, in the ground mixture, such as association between the functional groups of ketoprofen and chitin or chitosan might occur in the molecular level. The endothermic peak due to the fusion of ketoprofen disappeared in the ground mixture indicating the different thermal property. The co-grinding technique with chitin or chitosan provided a promising way enhancing the dissolution rate of practically insoluble drug.

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Decision of Optimum Grinding Condition by Pass Schedule Change (열간압연 스케줄변경에 따른 최적연삭조건 결정)

  • Bae, Yong-Hwan
    • Journal of the Korean Society of Safety
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    • v.23 no.6
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    • pp.7-13
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    • 2008
  • It is important to prevent roll failure in hot rolling process for reducing maintenance cost and production loss. The relationship between rolling pass schedule and the work roll wear profile will be presented. The roll wear pattern is related with roll catastrophic failure. The irregular and deep roll wear pattern should be removed by On-line Roll Grinder(ORG) for roll failure prevention. In this study, a computer roll wear prediction model under real process working condition is developed and evaluated with hot rolling pass schedule. The method of building wear calculation functions for center portion abrasion and marginal abrasion respectively was used to develop a work roll wear prediction mathematical model. The three type rolling schedule are evaluated by wear prediction model. The optimum roll grinding methods is suggested for schedule tree rolling technique.

Development of Diagnostic Expert System for Machining Process Ffailure Detection (가공공정의 이상상태진단을 위한 진단전문가시스템의 개발)

  • Yoo, Song-Min;Kim, Young-Jin
    • Journal of the Korean Society for Precision Engineering
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    • v.14 no.11
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    • pp.147-153
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    • 1997
  • Fault diagnosis technique in machining system which is one of engineering techniques absolutely necessary to automation of manufacturing system has been proposed. As a whole, diagnosis process is explained by two steps: sensor data acquisition and reasoning current state of system with the given sensor data. Flexible disk grinding process implemented in milling machine was employed in order to obtain empirical manufacturing process information. Resistance force data during machining were acquired using tool dynamometer known as sensor which is comparably accurate and reliable in operation. Tool status during the process was analyzed using influnece diagram assigning probability from the statistical analysis procedure.

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Study on the Irregular Shape Rolling Process (비대칭 형상 압연 공정에 대한 연구)

  • 김용철;김동진;김병민
    • Proceedings of the Korean Society for Technology of Plasticity Conference
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    • 1999.08a
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    • pp.98-106
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    • 1999
  • In this study cold rolling process for the irregular cross-sectional shape has been investigated. The product analyzed in present study is the steel cutter, which is frequently used to cut the desired shape on leather. Because steel cutter always has a irregular cross-section, after rolling process the workpiece is severely bended to every direction. The bending of the workpiece affects the processed performed after rolling such as heat treatment and grinding, then that of the workpiece becomes more severe. In this study, therefore, to prevent the bending of the workpiece to the left and right sides. rigid-plastic finite element method has been utilized and in order to find optimal roll geometry rapidly, one dimensional equal interval search technique has been also introduced. By using both rigid plastic finite element method and optimum technique, cold rolling process for the irregular cross-sectional shape has been successfully investigated.

Effects of different surface treatments on the shear bond strength of veneering ceramic materials to zirconia

  • Abdullah, Adil Othman;Hui, Yu;Sun, Xudong;Pollington, Sarah;Muhammed, Fenik Kaml;Liu, Yi
    • The Journal of Advanced Prosthodontics
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    • v.11 no.1
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    • pp.65-74
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    • 2019
  • PURPOSE. To evaluate and compare the effect of different materials and techniques on the shear bond strength of veneering ceramic materials to zirconia. MATERIALS AND METHODS. 136 sintered zirconia cubes were prepared and randomly divided into four study groups according to corresponding methods of surface treatment and materials: GLN (grinding followed by laser scanning using Noritake Cerabien ZR), SLN (sandblasting followed by laser scanning using Noritake Cerabien ZR), GLV (grinding followed by laser scanning using VITA VM 9), and SLV (sandblasting followed by laser scanning using VITA VM 9). Spraying technique was performed to coat the core. Profilometer, SEM, XRD, EDS, universal testing machine, and stereomicroscope were used to record surface roughness Ra, surface morphology, phase transformation, elemental compositions, shear bond strength SBS values, and failure types, respectively. Specimens were investigated in unaged (not immersed in artificial saliva) and aged (stored in artificial saliva for a month) conditions to evaluate SBS values. RESULTS. Grinding and GLN as first and second surface treatments provided satisfactory Ra values in both conditions ($1.05{\pm}0.24{\mu}m$, $1.30{\pm}0.21{\mu}m$) compared to sandblasting and other groups (P<.05). The group GLN showed the highest SBS values in both conditions ($30.97{\pm}3.12MPa$, $29.09{\pm}4.17MPa$), while group SLV recorded the lowest ($23.96{\pm}3.60MPa$, $22.95{\pm}3.68Mpa$) (P<.05). Sandblasting showed phase transformation from t-m. Mixed failure type was the commonest among all groups. CONCLUSION. GLN showed to be a reliable method which provided satisfactory bond strength between the veneer ceramic and zirconia. This method might preserve the integrity of fixed dental crowns.

Comminution-Classification of Clay-type Minerals by Fluid Energy Mill (Fluid Energy Mill에 의한 점토성 무기소재 미립화 분급기술 소고)

  • 김태욱;김만영;정필조;이주완
    • Journal of the Korean Ceramic Society
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    • v.22 no.5
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    • pp.47-53
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    • 1985
  • In view of innovated utilization of Korean clay resources conventional techniques for pulverization are reviewed in comparison with fluid energy milling processes of fluidized-bed type. Throughout experiment indigenous halloysite ores (white grade) after usual pretreatment are employed as typical sample. It is evidenced that grinding by means of porcelain ball mills has limitation in reducing clay particles to less than 10${\mu}{\textrm}{m}$ in diameter regardless of whether it is processed in dry or wet. Upon use of tungsten carbide bull mill particulation to submicron sizes could be effected with relative ease but severe coloration in grey is attended indicating metallic contamination possibly from friction of the grinding apparatus itself. In contrast the modified fluid en ergy milling enables particulation to $\leq$10${\mu}{\textrm}{m}$ in diameter with simultaneous classification int olimited ranges of particle size distributions. Since this technique is in principle based on the interparticle collisions rather than on the frictions between particles and mill surfaces minimum impurity attendance would be an additional advantage. Evidence leads to the conclusion that the fluidized-bed type milling is regarded as highly effective in puverization as well as fractionation of the clay minerals under examination. This is especially so in contemplating high-value and/or high-purity clay products.

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An Research on Ultra Precisive Polishing Manufacturing Technology of Glass for Micromini and Super Wide-Angle Aspherics Glasses Lens. (초소형 초광각 비구면 유리렌즈의 초정밀 연삭가공기술에 관한 연구)

  • Kim, Doo-Jin;Yoo, Kyung-Sun;Hyun, Dong-Hoon
    • Journal of the Korean Society of Manufacturing Technology Engineers
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    • v.19 no.2
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    • pp.275-281
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    • 2010
  • This research's goal is to process directly aspherics with big sagment and thin center thickness. If we can process directly aspherics with big sagment and thin center thickness, we think it greatly helps to reduce the time of developing optical system. We made very thin glass using diamond grinding whetstone regarding the trace of tool and the detailed drawing of tool super precisive aspherics that has 0.46mm center thickness and over $30^{\circ}$ segment, $0.1{\mu}m$ machining accuracy, 15nm surface accuracy. We think this research's result will be effective to open new market because it is applied not only cell phone optical system but also CCTV robot optical system, internet phone optical system. Also we expect to enhance the super strong brittle precisive process's possibility with super precisive processing technique that achieves 0.46mm glass center thickness as first in the world.

Enhancement of Dissolution Properties of Poorly Soluble Drugs (III) -Dissolution Enhancement of Furosemide from Ground Mixtures with Chitin or Chitosan- (난용성 약물의 용출 증가 (제 3 보) -키틴 또는 키토산과의 혼합분쇄물로부터의 푸로세미드의 용출 증가-)

  • Shin, Sang-Chul;Oh, In-Joon;Lee, Kang-Choon;Lee, Yong-Bok;Koh, Ik-Bae
    • Journal of Pharmaceutical Investigation
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    • v.17 no.4
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    • pp.175-181
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    • 1987
  • To increase the dissolution rate of furosemide, chitin and chitosan which are widely occurring biodegradable natural materials were used as drug carriers. The ground mixtures of furosemide with chitin or chitosan were prepared by grinding in a ball mill. The ground mixture showed a faster and more enhanced dissolution rate than the physical mixture or intact furosemide. The crystalline peaks of furosemide disappeared in the ground mixtures indicating the production of amorphous form. The comparison of infrared spectra of the physical mixture and the ground mixture showed an interaction such as association between the functional groups of furosemide and chitin or chitosan in the molecular level. The weight losses in TGA curves showed all the same patterns. However, the endothermic peak due to the fusion of furosemide in DTA curve disappeared in the ground mixture indicating the different thermal property. The dissolution of furosemide from ground mixtures was fast in the order of chitosan and then chitin. The co-grinding technique with chitin or chitosan provided a promising way enhancing the dissolution rate of practically insoluble drug.

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A Study on Determining Post-machining System for RP parts with Web-based Interface Tool (웹기반 쾌속조형물후가공 선정시스템 개발에 관한 연구)

  • 이상호;안대건;양화준;장태식;이일엽;정해도;이석희
    • Proceedings of the Korean Society of Precision Engineering Conference
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    • 2003.06a
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    • pp.1257-1260
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    • 2003
  • Rapid Prototyping technology has many advantages such as Rapid Tooling. However, Using the RT technique is limited by the poor surface quality of the RP part. Thus, additional post-machining is required for improving the surface roughness by the sanding, grinding and polishing etc. But, these traditional finishing techniques are time and labor cost consuming. Hence, improving and formulation the finishing technique is inevitably necessary for the RF part. A new post-machining methodology for RP part is presented by the SLS part is used for automobile components in this research. Also, a web based interface tool that user requirements are rapidly ordered for post-machining RP part is developed.

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