• 제목/요약/키워드: Grain-size distribution

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Floating zone법에 의한 $LiNbO_3$ 단결정 성장을 위한 최적 원료분말 합성 및 소결 조건 (The optimum condition of the powder synthesis and sintering for the floatign zone crystal growth of $LiNbO_3$)

  • 조현;심광보;오근호
    • 한국결정성장학회지
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    • 제6권2호
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    • pp.121-128
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    • 1996
  • Floating zone법으로 $LiNbO_3$ 단결정올 육성하는데 있어서 원료분말 합성과 원료봉 소결 과정의 최척의 조건을 설험적으로 조사하였다. 원료분말 합성사 낮은 고상반응 온도(700, $800^{\circ}C$)에서는 미량의 $Li_2CO_3$$Nb_2O_5$가 미반응상태로 남아있고, 고상반응 온도가 높을 때 ($1000^{\circ}C$)에는 입자성장이 일어나 후속공정인 원료봉 소결에 악영향을 미침이 확인되었다. $950^{\circ}C$에서 12시간 고상반응시킨 원료분말이 $LiNbO_3$의 결정상을 가지면서 미세한 결정립 크기와 균일한 크기분포를 보여 $950^{\circ}C$, 12시간이 최적의 원료분말 합성조건이었다. 원료봉 소결시 소 결온도가 높아질수록, 또 소결시간이 늘어날수록 치밀도가 증가하고 업자성장 양상이 급격히 증가함을 알 수 었었다. $1100^{\circ}C$에서 2시간 동안 소결한 원료봉이 치밀하고, 작은 결정립 크기 와 균얼한 크기분포를 나타내어 floating zone법에 의한 $LiNbO_3$ 단결정성장에 가장 적합한 최적 의 소결 조건은 $1100^{\circ}C$, 2시간엄이 확인되었다.

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고파랑 해안 침식폭 예측모델을 이용한 침식한계선(ECL) 설정 (Erosion Control Line (ECL) Establishment Using Coastal Erosion Width Prediction Model by High Wave Height)

  • 박승민;박설화;이정렬;김태곤
    • 한국해양공학회지
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    • 제33권6호
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    • pp.526-534
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    • 2019
  • The average coastline and the erosion control line introduced as the management coastline, and the average shoreline (MSL) was established from the observed coastline. Also, the median grain size and the wave height of 30-years return period were applied. The erosion control line (ECL) was established through the model, HaeSaBeeN. These two lines set the coastline for evaluation. Based on the observed monitoring data along the coastline, the 1-day variation according to the normal distribution was used to estimate the regional variation, and the width of the erosion was calculated by applying the median grain size (D50) and the wave height of 30-years return period through the high-wave coastal erosion width model, i.e., HaeSaBeeN.

감입곡류 지형과 암질 차이가 하상 퇴적물 입경 및 형상에 미친 영향: 공릉천 중상류 구간을 사례로 (The Effects of Incised Meandering Valley and Lithological Differences on the Grain Size and Shape of Channel Bed Materials: A Case Study of the Upper and Middle Reaches of Gongneungcheon River)

  • 진훈;김종욱;한민;변종민
    • 한국지형학회지
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    • 제26권1호
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    • pp.15-26
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    • 2019
  • In this study, we investigated the grain size, lithological type, and shape of coarse bed materials in the upper and middle reaches of Gongneungcheon River. For this purpose, 11 sampling points were selected along the river. For 100 samples of the coarse bed materials at each point, three axes (long, intermediate, and short) of samples were measured, and their lithological types were also identified. By measuring grain size, the sphericity and flatness of samples were calculated. Finally, every particle was classified into four shape categories: sphere, disc, blade and rod. We found that the grain size in incised meandering reach is the largest. This is mainly due to the supply of coarse materials from steep valley sides along the meandering channel. According to the lithological analysis, all samples were identified as granite, gneiss and schist, and quartz. The proportion of granite decreased, whereas the proportion of gneiss and schist increased downstream. These patterns indicate that the bedrock distribution within the study area accounts for the downstream lithological variation of coarse bed materials. With regard to the grain shape, sphericity gradually decreased while flatness gradually increased downstream. In the case of the shape classification, unlike the general downstream pattern of grain shape, the proportion of the sphere type decreased and the proportion of the blade type increased downstream. Such a reversal change in the downstream direction turns out to be determined by the lithology (such as foliation, bedding and the pattern of weathering) of coarse bed materials.

열 CVD법으로 증착된 SnO2 박막의 미세구조와 전기적 특성 (Microstructure and Electrical Properties of SnO2 Thin Films Grown by Thermal CVD Method)

  • 정진;최승평;신동찬;구재본;송호준;박진성
    • 한국전기전자재료학회논문지
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    • 제16권5호
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    • pp.441-447
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    • 2003
  • When a SnO$_2$ thin film was deposited by thermal CVD, two different types of growth behavior that were dependent on the deposition temperature were observed. The film grown at 475$^{\circ}C$ had a wide grain size distribution and a faceted surface shape. On the other hand, the film grown at 5$25^{\circ}C$ had a relatively narrow grain size distribution and a rounded sulfate shape. The aspects of grain shape and growth behavior agree well with the theory of gram growth and a roughening transition. The charge tarrier density decreased with deposition time. According to photoluminescence measurements, the peak intensity of the spectra occurred at approximately 2.5 eV, which is related to oxygen vacancies, and decreased with increasing of deposition time. These measurement results suggest that the number of oxygen vacancies, which is related to the electrical conductivity, decrease with deposition time.

입도 분포 특성을 이용한 동해 남한국대지 시추 퇴적물 중 화산재와 황사의 구분 (Discrimination of Volcanic Ash and Asian Dust (Hwangsa) in Core Sediments from the South Korea Plateau (East Sea) Using Characteristics of Grain-size Distributions)

  • 이홍원;장준호;박장준
    • 한국해양학회지:바다
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    • 제26권2호
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    • pp.135-144
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    • 2021
  • 동해 남한국대지 IODP Site U1430 시추 퇴적물 쇄설성 성분의 입도 자료에 대한 구성 성분 분해 결과 황사 입자와 화산재 입자를 대표하는 4개 구성 입도 집단이 구별되었다. 이 중 화산재 입자를 대표하는 2개 구성 입도 집단은 다양한 형태의 세립 및 조립 유리질 샤드들로 이루어져 있으며, 전체 입도 분포에서 0-82% 범위의 비율을 차지하고 있다. 분석된 입도 자료 중 화산재 유입 영향을 받은 자료를 제거하고 황사 입경 변화의 경향을 추출하기 위한 기준으로 화산재 구성 입도 집단 비율 33%가 적정한 것으로 판단된다.

MgO-C벽돌에 있어서 MgO Clinker의 특성이 침식에 미치는 영향 (The Effect of MgO Clinker s Properties on Corrosion of MgO-C Brick)

  • 이상완;김의훈;이석근
    • 한국세라믹학회지
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    • 제25권6호
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    • pp.593-600
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    • 1988
  • The properties of 10 kinds of MgO clinker were investigated to know the effect of MgO clinker's porperties on corrosion of MgO-C brick. For MgO clinker, chemical composition, porosity, density, periclase grain size, and microstructure were examined, while slag corrosion resistance was examined for MgO-C brick. In MgO clinker pore size and it's distribution, periclase grain size, impurities composition and the composition of grain boundaries are more important factors to determine corrosion degree of MgO-C brick than density, potosity and MgO purity.

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EFFECT OF Al UNDERLAYER ON THE MICROSTRUCTURES OF CoCrTa/Cr FILMS

  • Chang, H.S.;Shin, K.H.;Lee, T.D.;Park, J.K.
    • 한국자기학회지
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    • 제5권5호
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    • pp.614-617
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    • 1995
  • Thin CoCrTa/Cr films were deposited on glass substrates at $280^{\circ}C$ with or without Al underlayer. The coercivity of CoCrTa increased considerably by introducing an Al underlayer. The grain size of Cr thin film deposited on Al underlayer became smaller than that of Cr thin film deposited on glass substrate. The grain size of CoCrTa thin film was determined by Cr grain size. The cause of the coercivity increase seems to be associated with the refinement and uniform distribution of CoCrTa grains.

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초극저탄소 Cu강화형 자동차용 강판 변형시효에 미치는 Aluminum 및 고용질소의 영향 (Effect of Aluminum and Solute N on the Strain Aging of Extremely Low-Carbon Automotive Steel Strengthened with Cu sulfide)

  • 홍문희;양혜미;송승우;한성호
    • 대한금속재료학회지
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    • 제47권2호
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    • pp.71-78
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    • 2009
  • The precipitation behavior of solute carbon and nitrogen strongly affects the mechanical properties of low-carbon automotive panel. In the present study, the effects of aluminum and solute nitrogen on the bake hardenability and strain aging of extremely low-carbon steel with carbon content below 15 ppm has been investigated. The ferrite grain size and distribution of precipitates were varied with the amount of aluminum content of 0.003 to ~ 0.100 wt% in a constant solute carbon and nitrogen. With increasing the aluminum content, the ferrite grain size is increased and strain aging is delayed. The strain aging is also delayed by increasing the annealing temperature, although the ferrite grain size is not much changed.

자갈하상하천의 bar지형 발달에 관한 연구 -골지천을 사례로- (Bar Development in Gravel-bed River)

  • 양희경
    • 대한지리학회지
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    • 제32권4호
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    • pp.435-444
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    • 1997
  • bar는 하상의 기복중에서 가장 대표적인 충적지형으로 어느 하천에서나 쉽게 발견된다. 본 연구의 목적은 이러한 bar의 지형적 특성을 구명하는 것이다. 연구지역은 골지천 하류뷰이며, 총 6개 지점 bar를 조사하였다. 6개 bar는 모두 입경이 2mm 이상인 gravel bar이며 3, 5지점을 제외한 나머지 bar들은 유슈의 방향을 따라 길쭉한 형상을 하고 있다. bar의 력을 조사한 결과, 상류뷰에서 하류뷰로 가면서 입경이 감소하며 원마도는 증가하였다. bar의 형상은 수위변도, 하도경사, 형상계수 등에 따라 국지적으로 다르게 변화한다.

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ZnO 바리스터의 미세구조와 전기적특성에 미치는 ${ZnAl_2}{O_4}$의 영향 (Effects of ${ZnAl_2}{O_4}$ on the Microstructure and Electrical Properties of ZnO Varistor)

  • 손세구;김경남;한상목
    • 한국세라믹학회지
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    • 제37권4호
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    • pp.314-319
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    • 2000
  • Microstructueral development and electrical properties in ZnO-Bi2O3-ZnAl2O4 system were investigated with ZnAl2O4 content(0.1~1.0 mol%). The shrinakge of specimens started around $700^{\circ}C$ and finished at 110$0^{\circ}C$, reaching a maximum shrinkage rate at 80$0^{\circ}C$. The shrinkage rate is strongly related to the fromation of a Bi-rich liquid. The increase of the ZnAl2O4 content inhibited the grain growth of ZnO. Most of ZnAl2O4 particles located at the grain boundaries were about 2~3${\mu}{\textrm}{m}$. ZnO grain size changed little up to 110$0^{\circ}C$, but increased markedly above 115$0^{\circ}C$, especially at lower ZnAl2O4 content. Drastic decreasing in breakdown voltage(Vb) with increasing temperature is expected to be dependent on the ZnO grain size and the distribution of the largest grains between the electrode. The nonlinear I-V characteristic was significantly influenced by the ZnAl2O4 content, which exhibited a maximum value at about 15${\mu}{\textrm}{m}$ of ZnO grain size.

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