• Title/Summary/Keyword: Grain-size analysis

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Lattice based Microstructure Evolution Model for Monte Carlo Finite Element Analysis of Polycrystalline Materials (격자식 미세구조 성장 모델을 이용한 다결정 박막 소재의 유한 요소 해석)

  • 최재환;김한성;이준기;나경환
    • Transactions of Materials Processing
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    • v.13 no.3
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    • pp.248-252
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    • 2004
  • The mechanical properties of polycrystalline thin-films, critical for Micro-Electro-Mechanical Systems (MEMS) components, are known to have the size effect and the scatter in the length scale of microns by the numbers of intensive investigation by experiments and simulations. So, the consideration of the microstructure is essential to cover these length scale effects. The lattice based stochastic model for the microstructure evolution is used to simulate the actual microstructure, and the fast and reliable algorithm is described in this paper. The kinetics parameters, which are the key parameters for the microstructure evolution based on the nucleation and growth mechanism, are extracted from the given micrograph of a polycrystalline material by an inverse method. And the method is verified by the comparison of the quantitative measures, the number of grains and the grain size distribution, for the actual and simulated microstructures. Finite element mesh is then generated on this lattice based microstructure by the developed code. And the statistical finite element analysis is accomplished for selected microstructure.

Exploring the Applicability of Grain Size Trend Analysis to Understanding the Morphological Responses of the Deltaic Barrier Islands in the Nakdong River (낙동강 삼각주연안 사주섬의 지형변화에 대한 입도경향 분석의 활용도 탐색)

  • Kim, Sung-Hwan;Rhew, Ho-Sahng
    • Journal of the Korean association of regional geographers
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    • v.13 no.2
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    • pp.119-128
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    • 2007
  • Grain-size trend analysis is the methodology to obtain the net sediment transport pattern from the spatial trends of grain size parameters. It has the potentials to be an effective tool to address the morphological changes of the deltaic barrier islands in the Nakdoog River once we make sure net transport patterns inferred from grain size trend analysis represent the morphological evolution patterns. This research aims to investigate the applicability of the net transport patterns obtained by 'transport vector', proposed by Gao and Collins(1992), to understanding the morphological changes of the Nakdong River deltaic barrier islands. The results indicate that the net transport directions are overall in concordance with the morphological evolution patterns; however, the level of concordance is low in the island with fast growing rate. The reasons may be match or mismatch of temporal scales involved between processes represented by net transport patterns and morphological change analyzed or the rate of morphological change. Consequently, the application of grain size trend analysis in analyzing the morphological changes of deltaic barrier islands requires the careful consideration of temporal scales involved.

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Analysis of size distribution of riverbed gravel through digital image processing (영상 처리에 의한 하상자갈의 입도분포 분석)

  • Yu, Kwonkyu;Cho, Woosung
    • Journal of Korea Water Resources Association
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    • v.52 no.7
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    • pp.493-503
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    • 2019
  • This study presents a new method of estimating the size distribution of river bed gravel through image processing. The analysis was done in two steps; first the individual grain images were analyzed and then the grain particle segmentation of river-bed images were processed. In the first part of the analysis, the relationships (long axes, intermediate axes and projective areas) between grain features from images and those measured were compared. For this analysis, 240 gravel particles were collected at three river stations. All particles were measured with vernier calipers and weighed with scales. The measured data showed that river gravel had shape factors of 0.514~0.585. It was found that the weight of gravel had a stronger correlation with the projective areas than the long or intermediate axes. Using these results, we were able to establish an area-weight formula. In the second step, we calculated the projective areas of the river-bed gravels by detecting their edge lines using the ImageJ program. The projective areas of the gravels were converted to the grain-size distribution using the formula previously established. The proposed method was applied to 3 small- and medium- sized rivers in Korea. Comparisons of the analyzed size distributions with those measured showed that the proposed method could estimate the median diameter within a fair error range. However, the estimated distributions showed a slight deviation from the observed value, which is something that needs improvement in the future.

Genetic Studies on Grain Shape and Quality in Rice - I. Genetic Analysis of Grain Size, Weight and Shape (벼 입형(粒型)과 미질(米質)에 관련(關聯)된 형질(形質)의 유전연구(遺傳硏究) - I. 정조(正租)의 크기와 무게 및 모양에 대(對)한 유전분석(遺傳分析))

  • Park, Gyu Hwan;Kim, Hyun Tae;Choi, Soon Ho
    • Current Research on Agriculture and Life Sciences
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    • v.6
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    • pp.25-30
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    • 1988
  • Seven rice varieties and $42F_1$ hybrids of $7{\times}7$ diallel cross were used in genetic analysis for grain size, weight and shape. Effects of average heterosis for grain length and shape showed significantly negative values. GCA, SCA and RCA variances were significant for all characters and also additive variance was more important than dominance variance for grain length, width, thickness and weight. GCA effects of BG 2 and Arborio were highly positive for grain size and weight, and those of BG 2 and Nagdongbyeo were highly negative for grain shape. Partial dominance was observed for all characters. The direction of dominance was negative for grain length, width and shape, and ambidirections for grain thickness and weight. The effective gene number was two for grain length and shape. Both narrow and broad sense heritability were high in all characters.

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Nondestructive Evaluation for Grain Refinement of Aluminum Alloy of Equal-Channel Angular Pressing (ECAP 가공한 알루미늄합금의 결정립 미세화에 대한 비파괴평가)

  • Ahn, Seok-Hwan;Nam, Ki-Woo;Kim, Jin-Hwan;Kang, Suk-Bong
    • Journal of the Korean Society for Nondestructive Testing
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    • v.22 no.2
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    • pp.132-139
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    • 2002
  • The grain size of aluminum alloy was refined to the submicrometer level by using equal-channel angular pressing(ECAP). The effect of grain size refinement was evaluated by the tensile test, micro-hardness test, microstructure observations, ultrasonic test and acoustic emission test. The strength and the Vickers hardness were increased significantly according to grain size refinement after equal-channel angular pressed. The ultrasonic velocity was faster after equal-channel angular pressed, and the high frequency range appeared. The results of the ultrasonic velocity and the frequency range are expected to be basic data that can prove the grain size refinement

Effect of Effective Grain Size on Charpy Impact Properties of High-Strength Bainitic Steels (베이나이트계 고강도강의 샤르피 충격 특성에 미치는 유효결정립도 영향)

  • Shin, Sang Yong;Han, Seung Youb;Hwang, Byoungchul;Lee, Chang Gil;Lee, Sunghak
    • Korean Journal of Metals and Materials
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    • v.46 no.10
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    • pp.617-626
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    • 2008
  • This study is concerned with the effect of Cu and B addition on microstructure and mechanical properties of high-strength bainitic steels. Six kinds of steels were fabricated by varying alloying elements and hot-rolling conditions, and their microstructures and tensile and Charpy impact properties were investigated. Their effective grain sizes were also characterized by the electron back-scatter diffraction analysis. The tensile test results indicated that the B- or Cu-containing steels had the higher yield and tensile strengths than the B- or Cu-free steels because their volume fractions of bainitic ferrite and martensite were quite high. The B- or Cu-free steels had the higher upper shelf energy than the B- or Cu-containing steels because of their higher volume fraction of granular bainite. In the steel containing 10 ppm B without Cu, the best combination of high strengths, high upper shelf energy, and low energy transition temperature could be obtained by the decrease in the overall effective grain size due to the presence of bainitic ferrite having smaller effective grain size.

Impact Tensile Properties and Intergranular Fracture Behavior with Strain Rate Variations of Al-M g-X (X = Cr,Si) Alloy

  • Chang-Suk Han;Min-Gyu Chun;Sung-Soon Park;Seung-In Lim
    • Korean Journal of Materials Research
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    • v.34 no.7
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    • pp.330-340
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    • 2024
  • Al-Mg-Si alloys are light weight and have excellent corrosion resistance, and are attracting attention as a liner material for high-pressure hydrogen containers in hydrogen fuel cell vehicles. Because it has excellent plastic hardening properties, it is also applied to car body panel materials, but it is moderate in strength, so research to improve the strength by adding Si-rich or Cu is in progress. So far, the authors have conducted research on the intergranular fracture of alloys with excessive Si addition from the macroscopic mechanical point of view, such as specimen shape. To evaluate their impact tensile properties, the split-Hopkinson bar impact test was performed using thin plate specimens of coarse and fine grain alloys of Al-Mg-X (X = Cr,Si) alloy. The effect of the shape of the specimen on the characteristics was studied through finite element method (FEM) analysis. As a result, it was found that the intergranular fracture of the alloy with excessive Si depended on the specimen width (W)/grain size (d), which can be expressed by the specimen size and grain size. As W/d decreases, the intergranular fracture transforms into a transgranular fracture. As the strain rate increases, the fracture elongation decreases, and the fracture surface of the intergranular fracture becomes more brittle. It was confirmed that intergranular fracture occurred in the high strain rate region even in materials with small grain sizes.

Determination of Material Parameters for Microstructure Prediction Model Based on Recystallization and Grain Growth Behaviors (재결정 및 결정립 성장거동을 기초한 조직예측 모델에 대한 변수 결정방법)

  • Yeom, J.T.;Kim, J.H.;Hong, J.K.;Park, N.K.
    • Proceedings of the Korean Society for Technology of Plasticity Conference
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    • 2009.05a
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    • pp.270-273
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    • 2009
  • This work describes a method of determining material parameters included in recrystallization and grain growth models. Focus is on the recrystallization and grain growth models of Ni-Fe base superalloy, Alloy 718. High temperature compression tests at different strain, strain rate and temperature conditions were chosen to determine the material parameters of dynamic recrystallization model. The critical strain and dynamically recrystallized grain size and fraction at various process variables were quantitated with the microstructual analysis and strain-stress relationships of the compression tests. Besides, isothermal heat treatments were utilized to fit the material constants included in the grain growth model. Verification of the determined material parameters is carried out by comparing the measured data obtained from other compression tests.

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Material Properties of Ni-P-B Electrodeposits for Steam Generator Tube Repair

  • Kim, Dong Jin;Seo, Moo Hong;Kim, Joung Soo
    • Corrosion Science and Technology
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    • v.3 no.3
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    • pp.112-117
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    • 2004
  • This work investigated the material properties of Ni-P-B alloy electrodeposits obtained from a Ni sulfamate bath as a function of the contents of the P and B sources($H_3PO_3$ and dimethyl amine borane complex(DMAB), respectively) with/without additives. Chemical composition, residual stress, microstructure and micro hardness were investigated using ICP(inductively coupled plasma) mass spectrometer, flexible strip, XRD, TEM and micro Vickers hardness tester, respectively. From the results of the compositional analysis, it was observed that P and B are incorporated competitively during the electrodeposition and the sulfur from the additive is codeposited into the electrodeposit. The measured residual stress value increased in the order of Ni, Ni-P, Ni-B and Ni-P-B electrodeposits indicating that boron affects the residual tensile stress greater than phosphorus. As the contents of the alloying element sources of P and B increased, crystallinity and the grain size of the electrodeposit decreased. The effect of boron on crystallinity and grain size was also relatively larger than the phosphorus. It can be explained that the boron with a smaller atomic radius contributes to the increase of residual stress in the tensile direction and the larger restraining force against the grain growth more significantly than the phosphorus with a larger atomic radius. Introduction of an additive into the bath retarded crystallization and grain growth, which may be attributed to the change of the grain growth kinetics induced by the additive adsorbed on the substrate and electrodeposit surfaces during electrodeposition.

Dependence of fatigue crack propagation behavior on the microstructure in SM45c steel (SM45C강의 피로균열 성장에 미치는 미세조직의 영향)

  • 김현철;임병수
    • Journal of the korean Society of Automotive Engineers
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    • v.13 no.2
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    • pp.103-111
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    • 1991
  • To determine the effects of microstructure on the fatigue crack propagation behavior in SM45C steel, experimental investigations have been carried out with the specimens of different grain sizes and different spacings between the Fe$_{3}$C particles. Fatigue and tensile tests were conducted and the quantitative analysis of the relations between the threshold stress intensity range and grain size, interparticle spacing and yield stress were carried out. Some of the conclusions obtained are as follows; (1) .DELTA.K$_{th}$ was observed to increase with grain size and the spacing between the Fe3C particles. (2) In both pearlite and spheroidite microstructures, .DELTA.K$_{th}$ was increased when yield stress was decreased.sed.

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