• Title/Summary/Keyword: Grain Texture

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VMn underlayer for CoCrPt Longitudinal Recording Media

  • Oh, S.C;Lee, T.D
    • Journal of Magnetics
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    • v.5 no.4
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    • pp.143-146
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    • 2000
  • In this study, the magnetic properties of CoCrPt films (far longditudinal recording) on a novel VMn underlayer were measured and compared with similar films on conventional Cr underlayers. It was found that the VMn film had (200) preferred orientation and the lattice constant was about 0.2967 nm, which is slightly larger than that of the Cr film, 0.2888 m. The grain size of the VMn film was 9.8 nm at 30 m thickness, about 39% smaller than that of a similarly deposited Cr. The CoCrPt/VMn films showed higher coercivity in comparison with the CoCrPt/Cr films. The coercivity increase is attributed to the increased Co (11.0) texture, improved lattice matching between Co (11.0) and VMn (200), and lower stacking fault density. V or Mn must have diffused into the CoCrPt magnetic layer uniformly rather than preferentially along grain boundaries. This reduced Ms at higher substrate temperature.

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VMn underlayer for CoCrPt Longitudinal Media

  • S. C. Oh;Lee, T. D.
    • Proceedings of the Korean Magnestics Society Conference
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    • 2000.09a
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    • pp.352-362
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    • 2000
  • In this study, effects of novel VMn underlayer on magnetic properties of CoCrPt/VMn longitudinal medium was studied and compared with those of CoCrPt/Cr medium. It was found that the VMn film had (200) preferred orientation and the lattice constant was about 0.2967 nm, which is slightly larger than that of the Cr, 0.2888 nm. The grain size of VMn film was 9.3 nm at 30 nm thickness, and this is about 38 % smaller than that of a similarly deposited Cr film. The CoCrPt/VMn films showed higher coercivity in comparison with the CoCrPt/Cr films. The coercivity increase seems to be attributed to the increased Co (11.0) texture, improved lattice matching between Co (11.0) and VMn (200), and lower stacking fault density. Mn must have diffused into the CoCrPt magnetic layer more uniformly rather than preferentially along grain boundaries this reduced Ms at higher substrate temperature

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Microscopic Investigation of the Strain Rate Hardening for Polycrystalline Metals (철강재료 변형률속도 경화의 미시적 관찰)

  • Yoon, J.H.;Park, C.G.;Kang, J.S.;Suh, J.H.;Huh, M.Y.;Kang, H.G.;Huh, H.
    • Transactions of Materials Processing
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    • v.17 no.1
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    • pp.46-51
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    • 2008
  • Polycrystalline materials such as steels(BCC) and aluminum alloys(FCC) show the strain hardening and the strain rate hardening during the plastic deformation. The strain hardening is induced by deformation resistance of dislocation glide on some crystallographic systems and increase of the dislocation density on grain boundaries or inner grain. However, the phenomenon of the strain rate hardening is not demonstrated distinctly in the rage of $10^{-2}$ to $10^2/sec$ strain rate. In this paper, tensile tests for various strain rates are performed in the rage of $10^{-2}$ to $10^2/sec$ then, specimens are extracted on the same strain position to investigate the microscopic behavior of deformed materials. The extracted specimens are investigated by using the electron backscattered diffraction(EBSD) and transmission electron microscopy(TEM) results which show the effect of texture orientation, grain size and dislocation behavior on the strain rate hardening.

Superplasticity of Magnesium Alloys and SPF Applications (마그네슘합금의 초소성 특성과 응용)

  • Shim, Jae-Dong;Byun, Ji-Young
    • Korean Journal of Materials Research
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    • v.27 no.1
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    • pp.53-61
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    • 2017
  • Magnesium alloys are of emerging interest in the automotive, aerospace and electronic industries due to their light weight, high specific strength, damping capacity, etc. However, practical applications are limited because magnesium alloys have poor formability at room temperature due to the lack of slip systems and the formation of basal texture, both of which characteristics are attributed to the hcp crystal structure. Fortunately, many magnesium alloys, even commercialized AZ or ZK series alloys, exhibit superplastic behavior and show very large tensile ductility, which means that these materials have potential application to superplastic forming (SPF) of magnesium alloy sheets. The SPF technique offers many advantages such as near net shaping, design flexibility, simple process and low die cost. Superplasticity occurs in materials having very small grain sizes of less than $10{\mu}m$ and these small grains in magnesium alloys can be achieved by thermomechanical treatment in conventional rolling or extrusion processes. Moreover, some coarse-grained magnesium alloys are reported to have superplasticity when grain refinement occurs through recrystallization during deformation in the initial stage. This report reviews the characteristics of superplastic magnesium alloys with high-strain rate and coarse grains. Finally, some examples of SPF application are suggested.

The Trial Manufacture of the Grain-Oriented Ultra-Thin Silicon Steel Ribbon using Hot-Rolled Plate (열연판을 사용한 방향성 박규소강대의 제작)

  • 강희우
    • Journal of the Korean Magnetics Society
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    • v.11 no.1
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    • pp.1-7
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    • 2001
  • We investigated to DC magnetic characteristics, the dependence of annealing temperature on the crystal grain and the crystalline orientation for grain-oriented silicon ribbon with 100 $\mu\textrm{m}$ final thickness manufactured by three times cold rolling method using the hot-rolled silicon steel plate as a raw material. The growth of (110)[001] Goss texture were almost observed in the whole area of the sample. The values of the saturation magnetic flux density B$\sub$s/ and the average ${\alpha}$ angle have 1.9 T and 4.6 degrees respectively. From this result we could be confirmed that the three times cold rolling method has a possibility of manufacture for oriented ultra-thin silicon ribbons much more simple and cheeper than the existing oriented silicon steel manufacturing method by means of more simplified producing process.

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Fatigue Behavior of Fine Grained AM60 Magnesium Alloy Produced by Severe Plastic Deformation (강소성변형된 미세립 AM60 마그네슘 합금의 피로거동)

  • You, In-Dong;Lee, Man-Suk;Kim, Ho-Kyung
    • Journal of the Korean Society of Safety
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    • v.27 no.3
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    • pp.15-19
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    • 2012
  • The fatigue behavior of AM60 magnesium alloy produced by equal channel angular pressing(ECAP) process was investigated through fatigue lifetime and fatigue crack propagation rate tests. The grain structure of the material was refined from 19.2 ${\mu}m$ to 2.3 ${\mu}m$ after 6 passes of ECAP at 493 K. The yield strength(YS) and ultimate tensile strength (UTS) increase after two passes but decrease with further pressing, although the grain size becomes finer with increasing pass number. The softening effect due to texture anisotropy overwhelmed the strengthening effect due to grain refinement after 2 passes. A large enhancement in fatigue strength was achieved after two ECAP passes. The current finding suggests that two passed material is better than the multi-passed material in view of the static strength and fatigue performance.

Enhanced Densification in Tl-1223/Ag Tapes Prepared Using Pretreated Precursors

  • Jeong, D.Y;Baek, S.M.;Kim, B.J.;Kim, Y.C.;Park, K.G.
    • Progress in Superconductivity
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    • v.3 no.2
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    • pp.198-212
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    • 2002
  • The effects of reacted precursors on phase evolution, microstructure, $J_{c}$ and junctional characteristic of the inter-granular contacts were investigated in Ag-sheathed T1-1223 tapes prepared using three kinds of reacted precursors, and compared to those in the tape prepared using an unreacted precursor The precursors were prepared by heat-treating a mixture of Sr-Ba-Ca-Cu-O, $Tl_2$$O_3$, PbO and $Bi_2$$O_3$ powders at $805^{\circ}C$ (precursor I ), $840^{\circ}C$ (precursor II ) and $905^{\circ}C$(precursor III) for 20 min. Tl-1223 phase content, grain size and J\ulcorner in the tapes appeared to increase in an order of precursors I, II and III Compared to tapes prepared using an unreacted precursor, the tapes prewar ed using precursors II and III revealed reduced pore and impurity densities and an enhanced texture. Also characteristic of inter -granular contacts and fraction of strong-links were improved. The improved properties are attributed to enhanced densification resulting from using the reacted precursors.s.

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Classification of Grain Type and Marketing Grades for Korean Rice Varieties (한국 쌀의 입형구분과 상품 품위등급 설정)

  • Kwang-Ho Kim
    • KOREAN JOURNAL OF CROP SCIENCE
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    • v.42 no.3
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    • pp.357-366
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    • 1997
  • Rice quality is considered to have two general meanings; 1) milling, cooking, and processing quality, which refer to suitability of the grain for a particular end-use; and 2) physical quality, which means cleanliness, soundness, and freedom from foreign materials. Grain type is associated with specific milling, cooking, and processing characteristics. Thus, this experiment was conducted to classify the grain type categories and marketing grades for Korean leading rice varieties. Length: width ratio of brown rice kernel ranged from 1.57 to 2.25 and most of varieties belonged to short grain except Tongil type rice varieties. Mean of length: width ratio of brown rice kernel was 1.77 and coefficient of variance was 4.79% in short grain type varieties. Grain shape could be further classified into 5 types by length:width ratio of brown rice kernel; 1 type(less than 1.75), 2 type(1.76∼1.80), 3 type(1.81∼1.90), 4 type(1.91∼2.00), and 5 type (greater than 2.00). For 1 and 2 type of varieties, woven wire sieve having 1.7mm openings showed better whole-kernel yields for special marketing grade, and sieve having 2.0mm openings for 3 and 4 type of varieties. Grain type which classified into 5 categories was not associated with physicochemical and cooking characteristics of rice grain, but sensory evaluation of cooked rice showed better score for 1 type varieties in terms of appearance, gloss, flavor, texture, stickiness, and taste.

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Enhancement of Grain Refinement and Formability of Cross-Roll-Rolled Ni-10Cr Alloy (교차롤압연된 Ni-10Cr 합금의 결정립 미세화와 성형성 향상)

  • Song, Kuk-Hyun;Kim, Won-Yong;Son, Hyun-Taek
    • Korean Journal of Materials Research
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    • v.22 no.6
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    • pp.303-308
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    • 2012
  • This study evaluated the enhancement of microstructural and mechanical properties of a cross rolled Ni-10Cr alloy, comparing with conventionally rolled material. Cold rolling was carried out to 90% thickness reduction and the specimens were subsequently annealed at $700^{\circ}C$ for 30 min to obtain a fully recrystallized microstructure. Cross roll rolling was carried out at a tilted roll mill condition of $5^{\circ}$ from the transverse direction in the RD-TD plane. In order to observe the deformed microstructures of the cold rolled materials, transmission electron microscopy was employed. For annealed materials after rolling, in order to investigate the grain boundary characteristic distributions, an electron back-scattering diffraction technique was applied. Application of cold rolling to the Ni-10Cr alloy contributed to notable grain refinement, and consequently the average grain size was refined from 135 ${\mu}m$ in the initial material to 9.4 and 4.2 ${\mu}m$ in conventionally rolled and cross rolled materials, respectively, thus showing more significantly refined grains in the cross rolled material. This refined grain size led to enhanced mechanical properties such as yield and tensile strengths, with slightly higher values in the cross rolled material. Furthermore, the <111>//ND texture in the CRR material was better developed compared to that of the CR material, which contributed to enhanced mechanical properties and formability.

Development of Microstructures and Mechanical Properties in Differential Speed Rolled Ni-30Cr Alloy (이주속압연된 Ni-30Cr 합금의 미세조직과 기계적 특성 발달)

  • Im, Yong-Deok;Park, Hyung-Ki;Song, Kuk-Hyun
    • Korean Journal of Materials Research
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    • v.25 no.3
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    • pp.149-154
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    • 2015
  • We evaluated the developed microstructures and mechanical properties of a severely plastically deformed Ni-30Cr alloy. Normal rolling and differential speed rolling were used as deformation processes, and the thicknesses of the specimens were reduced to 68 % of the original thickness after holding at $700^{\circ}C$ for 10 min and annealing at $700^{\circ}C$ for 40 min to obtain a fully recrystallized microstructure. Electron backscattering diffraction was used to analyze the characteristic distribution of the grain boundaries on the deformed and annealed specimens. Differential speed rolling was more effective for refining grains in comparison with normal rolling. The grain size was refined from 33 mm in the initial material to 8.1 mm with normal rolling and 5.5 mm with differential speed rolling. The more refined grain in the differential-speed-rolled material directly resulted in increases in the yield and tensile strengths by 68 % and 9.0%, respectively, compared to normal rolling. We systematically explain the relationship between the grain refinement and mechanical properties through a plastically deformed Ni-30Cr alloy based on the development of a deformation texture. The results of our study show that the DSR process is very effective when used to enhance the mechanical properties of a material through grain refinement.