• 제목/요약/키워드: Fe analysis

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O/Fe(100) and MgO/Fe(100) 계의 LEED I/V curve 분석 (LEED I/V Curve Analysis of O/Fe(100) and MgO/Fe(100) System)

  • 서지근;김상현
    • 한국진공학회지
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    • 제16권1호
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    • pp.1-6
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    • 2007
  • 우리는 O/Fe(100)의 원자적 구조와 MgO/Fe(100) 표면의 계면의 구조를 LEED I/V curve를 이용하여 분석하였다. 산소를 Fe(100) 표면에 흡착시켰을 때 Fe 표면의 첫 번째 층간 간격은 약 16 % 정도 팽창하는 것을 확인하였다. 1ML MgO를 Fe(100) 표면에 성장하였을 때, MgO의 O가 Fe의 on-top 위치에 자라나는 것을 확인하였고, MgO/Fe 계면의 층간 간격이 확장되는 것을 확인하였다. AIA(average intensity mixing approximation) 계산을 사용하여 단층 MgO 성장한 Fe(100) 계의 계면구조는 MgO/FeO/Fe(100)와 MgO/Fe(100)의 계면구조를 갖는 것을 확인하였다. 이것은 확장된 FeO 층의 존재를 보이고 MgO/FeO/Fe(100)와 MgO/Fe(100) 두가지 계면 구조의 공존을 보인 EELS 실험 결과를 뒷받침 한다.

수침목제유물 보존처리에 관한 연구 -EDTA 처리에 관하여- (A study on the conservation treatment of waterlogged wood cultural properties for the subject of EDTA treatment)

  • 양석진
    • 한국문화재보존과학회:학술대회논문집
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    • 한국문화재보존과학회 2005년도 제22회 학술대회 발표 논문집
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    • pp.122-134
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    • 2005
  • XRF, EDX, IR analysis was conducted to figure the effect of Fe to blacken the waterlogged wood. The results showed that investigated soil contained more Fe than normal soil by XRF analysis and wood ash contained more sulfur and Fe than any other element by EDX analysis. C-H and C-O peaks were significantly reduced at the surface of wood where is blackened part of waterlogged wood by IR analysis. The optimum condition to remove Fe from waterlogged wood by EDTA was investigated. To do this, removed concentration of Fe was measured at various concentration of EDTA-2Na. The optimum pH of EDTA-2Na was figured to be 4.1 to 4.3 and as the concentration of EDTA was increasing, extracted concentration of Fe was also increased. In the case of 0.4 wt% of EDTA-2Na, 700ppm of Fe was eliminated and was stabilized after 48 hours time lapse. In the case of EDTA-3Na, the optimum pH was 7 to 8, and 10 ppm of Fe was eliminated at 0.4 wt% of EDTA-3Na. In the case of EDTA-4Na, the optimum pH was 10 to 11, and 120 ppm of Fe was eliminated at 0.4 wt% of EDTA-4Na.

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강성계수의 전달에 의한 평판 구조물의 구조해석 (Structural Analysis of Plate Structures by Transfer of Stiffness Coefficient)

  • 최명수
    • 동력기계공학회지
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    • 제11권1호
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    • pp.92-97
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    • 2007
  • It is important to compute the structural analysis of plate structures in structural design. In this paper, the author uses the finite element-transfer stiffness coefficient method (FE-TSCM) for the structural analysis of plate structures. The FE-TSCM is based on the concept of the successive transmission of the transfer stiffness coefficient method and the modeling technique of the finite element method (FEM). The algorithm for in-plane structural analysis of a rectangular plate structure is formulated by using the FE-TSCM. In order to confirm the validity of the FE-TSCM for structural analysis of plate structures, two numerical examples for the in-plane structural analysis of a plate with triangular elements and the bending structural analysis of a plate with rectangular elements are computed. The results of the FE-TSCM are compared with those of the FEM on a personal computer.

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유한요소법에 의한 광폭 레이저 표면경화의 잔류응력해석 (Residual Stress Analysis for Wide-band laser Heat Treatment Using Finite Element Method)

  • 김재도;맹주원
    • 한국정밀공학회지
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    • 제16권11호
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    • pp.68-73
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    • 1999
  • In this paper, the residual stresses for the wide-band laser heat treatment using a polygon mirror have been analyzed. The results of FE analysis are compared with the experimental results. ANSYS Version 5.3, a commercial FE-code, is used for the FE stress analysis. The structural analysis was performed on after thermal analysis. The residual stress distribution across the hardened area was measured by the X-ray diffraction technique. The laser hardening conditions, 2kW laser power and 2mm/s travel speed, were used for the experiment and the FE analysis. Analysis results, which is maximum tensile residual stress is about 143MPa and maximum compressive residual stress is about -380MPa. Under same parameters with the analysis, experimental results indicate that MTRS is about 152MPa and MCRS is about -312MPa. The experimental results is about 6% higher than the FE analysis. As a result, residual stress data from the experiment close well with that of the FE analysis.

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수열합성법으로 제조한 흑색 자성안료의 Fe2+/Fe3+ 몰비에 따른 특성 (Effect of Fe2+/Fe3+ Molar Ratio on the Synthesized Magnetic Black Pigment by Hydrothermal Method)

  • 정명호;장건익
    • 한국전기전자재료학회논문지
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    • 제30권12호
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    • pp.812-816
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    • 2017
  • $Fe_3O_4$ was prepared on the $TiO_2-coated$ natural mica substrate. The natural mica has an average particle size of $22{\mu}m$. The substrate was coated on $TiO_2$ thin films using hydrothermal synthesis at pH 1.5-2.5 at $75^{\circ}C$. The Fe precursor solution was prepared by mixing $FeSO_4$ (for $Fe^{2+}$ ion) and $FeCl_3$ (for $Fe^{3+}$ ions) with different molar ratios such as 1/2, 1/1, 2/1, 3/0, and $Fe_3O_4$ only. X-ray diffraction analysis shows that the crystal structure depends on the $FeCl_3-to-FeSO_4$ molar ratio. $Fe_3O_4$ crystal phase could be obtained at higher $FeSO_4$ contents.

30 kVA 초전도 발전기의 소용량 부하 인가시 운전특성 해석 (Performance Analysis of 30 kVA Super-Conducting Generator under Light Load)

  • 하경덕;황돈하;박도영;김용주
    • 대한전기학회:학술대회논문집
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    • 대한전기학회 1999년도 하계학술대회 논문집 A
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    • pp.271-273
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    • 1999
  • In this paper 30 kVA Super-Conducting Generator's test and analysis results of OCC and SCC are presented. Also the test and FE analysis results of the generator under 1.2, 2.4, and 3.6[kW] load are described. For FE analysis of the generator's performance, the external circuit is coupled with the FE region. The generator's end winding reactance is obtained based on the design data, actual dimension, preliminary FE analysis, and empirical formulas. The comparison of FE analysis coupled with external circuit to the test results shows a good agreement.

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주조 및 열간압축된 Pr, Nd-Fe-B계 영구자석의 열자기 분석과 자기적 특성 (Magnetic Properties and Thermomagnetic Analysis of Cast and Hot-Pressed Pr, Nd-Fe-B Magnets)

  • 김동엽;이동구;정원용
    • 한국자기학회지
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    • 제2권1호
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    • pp.37-43
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    • 1992
  • Pr, Nd-Fe-B계 합금을 주조 및 열간압축한 후 직류자화측정기와 진동시료형 자속계를 이용하여 자기적 특성을 측정하였다. 이 결과로부터 제 2상과 보자력과의 관계를 조사하였다. 주조시 $Pr_{17}Fe_{76.5}B_{5}Cu_{1.5}$계 합금에는 ${\alpha}-Fe$가, $Nd_{14}Dy_{1}Fe_{78.5}B_{5}Cu_{1.5}$계 합금에는 $Nd_{2}Fe_{17}$상이 각각 생성 되었다. 생성된 제 2상은 R(R=Pr, Nd)-Fe-B계 주조합금의 자기적 특성을 저하시킨다. 주조합금을 열처리하면 열자기분석 곡선에서 ${\alpha}-Fe$, $Nd_{2}Fe_{17}$상이 확인되지 않았다. 열처리 시 이와 같은 연자성상이 제거됨에 따라 열처리된 Pr, Nd-Fe-B계 주소합금의 자기적 특성은 증가하였다. Nd-Fe-B-Cu계 열간압축 자석에서의 보자력의 온도계수($\beta$)는 0.48로, 이를 Nd-Fe-B계 소결자석의 ${\beta}=0.86$, Nd-Fe-Co-B계 소결자석의 ${\beta}=0.5$와 비교해 보면 열간압축된 자석이 우수한 열적안정성을 나타냄을 알 수 있었다.

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급냉응고된 Al-(Fe, Ce) 합금에서 형성되는 석출상의 X-선적연구 (A Study on the Precipitates in Rapidly Solidified Al-(Fe, Ce) Alloys by Analysis of X-Ray Diffraction)

  • 박익민;이규한;최정철;조형호
    • 한국주조공학회지
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    • 제8권4호
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    • pp.446-452
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    • 1988
  • To obtain detailed information on the metastable and the equilibrium phases in rapidly solidified Al-(Fe,Ce) alloys, analysis of X-ray diffraction pattern has been carried out. It has been found that the metastable phase formed in Al-Fe alloys including up to 6wt%Fe is $Al_6Fe$ and the equilibrium phase is $Al_3Fe$. Any X-ray diffraction peak corresponding to the equilibrium phase $Al_{13}Fe_4$ has not been observed during aging. In Al-4wt%Fe alloy, which is ribbon shape with thickness less than $70\;{\mu}m$, aged at $400^{\circ}C$ for 1h after rapid solidification, unidentified phase has been found. In Al-4wt%Ce alloy, only X-ray diffraction peak corresponding to the equilibrium phase, $Al_4Ce$ has been observed. It has been found that the metastable phase Formed in Al-Fe-Ce alloys including up to 6wt% Fe and 4wt% Ce is $Al_6Fe$ and the equilibrium phases are $Al_3Fe$ and $Al_{10}CeFe_2$.

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유한요소해석을 이용한 Cu-10wt%Fe 합금의 압출공정 모사 (Simulation of the Extrusion Process of Cu-10wt%Fe Alloy using Finite Element Analysis)

  • 유태현;;최시훈
    • 소성∙가공
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    • 제33권1호
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    • pp.50-54
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    • 2024
  • In this paper, the process of extruding Cu-10Fe alloy using a finite element analysis (FEA) was theoretically analyzed. To achieve this, the dependence of strain rate and temperature of the alloy required for the extrusion process was secured by utilizing databases for Cu and Fe and the KHL model. For microstructure analysis, FE-SEM with EDS was used to distinguish the phases present in Cu-10Fe alloy. The mechanical characteristics of Cu-10Fe alloy were secured using the results of fitting the mechanical properties of Copper and Steel from the Deform database to the KHL model. The deformation behavior within the alloy during hot extrusion was analyzed, providing insights into effective stress, effective strain, effective strain rate, and temperature. It was observed that the strain distribution was non-uniform. These research findings contribute to an improved understanding of the hot extrusion process of Cu-10Fe alloy and can aid in predicting the mechanical properties of the material.

Aggregation multigrid method for schur complement system in FE analysis of continuum elements

  • Ko, Jin-Hwan;Lee, Byung Chai
    • Structural Engineering and Mechanics
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    • 제30권4호
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    • pp.467-480
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    • 2008
  • An aggregation multigrid method (AMM) is a leading iterative solver in solid mechanics. Recently, AMM is applied for solving Schur Complement system in the FE analysis of shell structures. In this work, an extended application of AMM for solving Schur Complement system in the FE analysis of continuum elements is presented. Further, the performance of the proposed AMM in multiple load cases, which is a challenging problem for an iterative solver, is studied. The proposed method is developed by combining the substructuring and the multigrid methods. The substructuring method avoids factorizing the full-size matrix of an original system and the multigrid method gives near-optimal convergence. This method is demonstrated for the FE analysis of several elastostatic problems. The numerical results show better performance by the proposed method as compared to the preconditioned conjugate gradient method. The smaller computational cost for the iterative procedure of the proposed method gives a good alternative to a direct solver in large systems with multiple load cases.