• Title/Summary/Keyword: Extruder screw

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Processing and Mechanical, Thermal and Morphological Properties of Poly(lactic acid)/Poly(butylene succinate) Blends (폴리유산/폴리부틸렌숙시네이트 블랜드의 가공 및 기계적, 열적, 형태학적 특성)

  • Kim, Dae Keun;Cho, Donghwan
    • Journal of Adhesion and Interface
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    • v.15 no.1
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    • pp.14-21
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    • 2014
  • In the present work, PLA/PBS blends with poly(lactic acid) (PLA) and poly(butylene succinate) (PBS) at different contents were processed by using a twin-screw extruder and an injection molding machine, and then their mechanical, thermal and morphological properties were investigated. The mechanical properties such as flexural strength, flexural modulus, tensile strength and tensile modulus and thermal properties such as melting behavior, dynamic mechanical thermal properties and thermal stability significantly depended on the contents of PLA and PBS. However, the heat deflection temperature of the blends was not significantly influenced by the contents of PLA and PBS. Also, the fracture surfaces of PLA/PBS blends were changed from a brittle pattern to a ductile pattern with increasing the PBS contents.

Morphology, Thermal and Mechanical Properties of Poly(lactic acid)/Poly(butylene adipate-co-terephthalate)/CMPS Blends (Poly(lactic acid)/Poly(butylene adipate-co-terephthalate)/CMPS 블렌드의 형태학, 열적 및 기계적 특성)

  • Kang, Kyoung-Soo;Kim, Bong-Shik;Jang, Woo-Yeul;Shin, Boo-Young
    • Polymer(Korea)
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    • v.33 no.2
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    • pp.164-168
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    • 2009
  • The effects of chemically modified thermoplastic starch (CMPS) on the morphology, thermal and mechanical properties of the blends of poly (lactic acid)(PLA) and poly(butylene adipate-co-terephthalate)(PBAT) were studied. Blends of PLA/PBAT with the CMPS contents of 10, 20 and 30 wt% on the basis of PLA/PBAT weight were prepared by a twin screw extruder. The morphology, thermal and mechanical properties of the blends were examined by using scanning electron microscope (SEM), differential scanning calorimeter (DSC) and a tensile tester. The DSC study revealed that PLA/PBAT blends are thermodynamically immiscible, while the compatibility was much improved by addition of the CMPS.

Reflectance and Flexural Modulus of ABS/TiO2 Composite Sheets (ABS/TiO2 복합체 쉬트의 반사율과 굴곡 탄성률)

  • Kim, Jun Hong;Yoon, Kwan Han
    • Polymer(Korea)
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    • v.38 no.1
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    • pp.103-107
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    • 2014
  • Poly(acrylonitrile-butadiene-styrene) (ABS) composite sheets containing titanium dioxide ($TiO_2$), barium sulfate ($BaSO_4$), calcium carbonate ($CaCO_3$) were prepared by using a co-rotating twin screw extruder, and the reflectance and flexural modulus of the composite sheets were measured. The fillers were well dispersed in ABS matrix. The reflectance of composite sheet was increased with increasing $TiO_2$ and $BaSO_4$ content. Sheet having $TiO_2$ 20 wt% composition, with 5~20 wt% $BaSO_4$ resulted in more than 95% of reflectance. The flexural modulus of composite sheet was increased from 1864 MPa for $ABS/TiO_2/BaSO_4$ 85/10/5 (w/w/w) to 3134 MPa for $ABS/TiO_2/BaSO_4$ 55/20/25 (w/w/w).

Preparation and Characterization of Antimicrobial Composite Film Containing Calcined Oyster Shell Powder (굴 패각 분말을 함유한 항균성 복합 필름의 제조 및 특성 연구)

  • Park, Kitae;Kambiz, Sadeghi;Seo, Jongchul
    • KOREAN JOURNAL OF PACKAGING SCIENCE & TECHNOLOGY
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    • v.27 no.1
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    • pp.41-48
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    • 2021
  • In this study, ethylene vinyl acetate (EVA) and low density polyethylene (LDPE) composite films (EVA/LDPE-OSP) containing calcined oyster shell powder (OSP) were prepared using twin-screw extruder as an antimicrobial packaging material. The OSP composite was initially prepared and then incorporated into an EVA/LDPE blend at different ratios (0, 1, 3 and 5%) to develop the EVA/LDPE-OSP composite films. The as-prepared EVA/LDPE-OSP composites films were evaluated using FT-IR, DSC, TGA, OTR, WVTR, SEM and UTM as well as antimicrobial activity was examined using JIS Z 2801:2000 standard. OPS endowed the antimicrobial potency to the composite films against Gram-positive (Staphylococcus aureus) and Gram-negative (Escherichia coli) bacteria. In addition, the incorporation of OSP remarkably enhanced the thermal stability. OSP as a natural biocidal agent can be used as a multifunctional additive in packaging industry such as improving the thermomechanical properties and preventing the microbial contamination of packaged products.

Preparation and Characterizations of Wood Plastic Composite Panel Fabricated with Chamaecyparis obtusa Wood Flour (편백나무 목분을 첨가한 합성목재 패널의 제조 및 특성 평가)

  • Kim, Soo-Jong
    • Journal of Convergence for Information Technology
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    • v.12 no.5
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    • pp.126-132
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    • 2022
  • Wood Plastic Composite(WPC) has been mostly used for outdoor purposes such as deck materials and trails so far. In this study, WPC panels with improved antibacterial properties, total volatile organic compound emissions (TVOC), and flame retardant were manufactured to use Wood Plastic Compound as interior materials for indoor use. WPC compound was prepared by mixing Chamaecyparis obtusa wood flour with high density polyethylene(HDPE). The prepared WPC compound exhibited excellent antibacterial and antifungal properties, and the total volatile organic compound emission(TVOC) was 0.062 mg/m2·h. The WPC panel(303mm×606mm×10mm) manufactured by a twin screw extruder with the manufactured compound achieved the flame retardant grade 2 standard of KS F 2271.

PBAT Compound Films with Improved Hydrolysis Resistance and its Application (내가수분해성이 향상 된 PBAT의 컴파운드 필름 및 이의 응용)

  • Sim, Jae-Ho;Shim, Jae-Hoon
    • The Journal of the Convergence on Culture Technology
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    • v.8 no.5
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    • pp.553-559
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    • 2022
  • The film mulching technology is useful for controlling soil temperature and moisture by covering the soil surface, and for suppressing weeds. In this study, in order to improve the hydrolysis resistance and mechanical properties of the biodegradable mulching film, PBAT(Poly butylene adipate-co-terephthalate) and PLA(Poly lactic acid) were modified using a twin-screw extruder and then the physical and biodegradable properties of the film were investigated. After landfill the mulching film in soil, the weight reduction of the film was confirmed by period, and plant growth was observed after mulching in the dry paddy field for rice farming. Mulching films with improved hydrolysis resistance showed excellent crop growth properties, and biodegradable mulching films can offer potential as a new alternative for environmentally friendly, efficient and sustainable agricultural practices.

Effect of Master Batch and Compatibilizer on the Physical and Rheological Properties of PP/CNF Composite (PP/CNF 복합체의 물리적 성질 및 유변학적 특성에 대한 마스터배치와 상용화제의 영향)

  • San Kang;Yoo Jin Lee;Youn Cheol Kim
    • Applied Chemistry for Engineering
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    • v.35 no.5
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    • pp.418-422
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    • 2024
  • Polypropylene (PP)/CNF composites containing 3, 7, and 10 phr of cellulose nanofibers (CNF) were manufactured using a twin-screw extruder. CNF was introduced in the form of powder or master batch (MB) into ethylene-acrylic acid copolymer (EEA), and maleic anhydride grafted PP (PP-g-MAH) was used as a compatibilizer. The results of measuring the tensile strength and flexural strength showed that the degree of improvement in the mechanical properties of the PP/CNF composites applied with the compatibilizer was the greatest. This was confirmed by the morphological analysis of SEM, which was due to the increased compatibility between PP and CNF. It was confirmed that the complex viscosity of the PP/CNF composite in the low frequency range was higher than that of pure PP, but there was no significant difference in processing characteristics due to the increase in shear thinning phenomenon.

Studies on the Effects of Amylase Addition to Rice Extrusion on the Rheological Properties of the Extrudate for Weaning Food Base (압출조리를 이용한 쌀 이유식 제조에서 아밀라제 첨가가 물성변화에 미치는 효과)

  • Lee, Gang-Gweon;Kim, Ji-Yong;Lee, Cherl-Ho
    • Korean Journal of Food Science and Technology
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    • v.26 no.6
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    • pp.670-678
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    • 1994
  • The effects of amylase addition during extrusion cooking of rice on the physico-chemical properties of the extrudates were investigated in order to develop rice-based Korean style weaning food products. A laboratory-built single screw extruder was used, the enzymes used were Termamyl 120LS(amylase from Bacillus licheniformis, NOVO Co.), BAN 240L(amylase from Bacillus amylolichuefaciens, NOVO Co.) and malt powder. By the addition of enzymes, the water soluble index of the extrudates increased by 3 times compared to that of the extrudates without enzyme and the concentration of reducing sugar in the extrudates increased drastically at 28 feed moisture. The gel permeation chromatographic pattern showed that the large molecular starch fractions diminished by the addition of enzyme during extrusion and the low molecular fraction increased. The residual enzyme activity in the extrudate were 27% for the most thermo-resistance enzyme by treating at $140^{\circ}C$ in the metering section of the extruder. The sediment volume of the extrudate dispersion increased as the metering section temperature increased to $140^{\circ}C$ . By the addition of enzymes the viscosity of extrudate dispersion was redused $1/4{\sim}1/200$ of that of the extrudates without enzyme. It allowed to use 1.8 times of solid material to the weaning food formulation to attain the same level of consistency as the commercial products. It proves that the addition of amylase during rice extrusion is effective to increase the energy density of weaning food by starch degradation, which results in the increases of water solubility, reducing sugar content, dispersibility and fluidability.

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Physicohemical Properties of Extruded Rice Flours and a Wheat Flour Substitute for Cookie Application (압출쌀가루의 이화학적 특성 및 밀가루 대체 쿠키 특성)

  • We, Gyoung Jin;Lee, Inae;Kang, Tae-Young;Min, Joo-Hong;Kang, Wie-Soo;Ko, Sanghoon
    • Food Engineering Progress
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    • v.15 no.4
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    • pp.404-412
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    • 2011
  • The purpose of this study is to prepare extruded rice flours suitable for baking rice cookies. The extruded rice flours were prepared at 100 and 130$^{\circ}C$ temperature and 25 and 27% moisture content in a co-rotating twin screw extruder. The rice extrudates were dried at 100$^{\circ}C$ for 18 hr and subsequently ground into the fine flour. Characteristics of the extruded rice flours were examined by rapid visco analysis, hydration property analysis, differential scanning calorimetry (DSC), and in vitro digestion test. Water absorption, solubility, and swelling power of all extruded rice flours were higher than those of native rice flour. DSC analysis showed that native rice flour had a peak at about 65$^{\circ}C$ while all extruded rice flours did not show any peaks since they were already gelatinized during the extrusion proess. Viscosity of the extruded rice flours decreased with increasing temperature and lowering moisture content in the extrusion proess. The extruded rice flours prepared at 130$^{\circ}C$ exhibited lower viscosity than those prepared at 100$^{\circ}C$. The operating temperature of the extrusion proess was critical for the starch digestion in vitro. The extruded rice flours prepared at 130$^{\circ}C$ showed a rapid decrease in digestible starch content while an increased level of slowly digestible starch content was observed compared to those treated at 100$^{\circ}C$ in the extruder. Cookies were prepared with a mixture of wheat flour and extruded rice flours at the ratio of 7 to 3. The cookies made with the extruded rice flours had lower spread factor and darker yellow color than those prepared with wheat flour only. Hardness of the extruded rice flour-added cookies was similar to that of the wheat flour cookie whereas their overall acceptance was better. Therefore the rice cookies partially supplemented with extruded rice flours may have a potential as early childhood foods which require soft texture and allergy reduction.

Effect of the Compatibilizer on Physical Properties of Polypropylene (PP)/Bamboo Fiber (BF) Composites (폴리프로필렌/대나무 섬유 복합체의 물성에 대한 상용화제의 영향)

  • Lee, Jong Won;Ku, Sun Gyo;Lee, Beom Hee;Lee, Ki-Woong;Kim, Cheol Woo;Kim, Ki Sung;Kim, Youn Cheol
    • Applied Chemistry for Engineering
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    • v.26 no.5
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    • pp.615-620
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    • 2015
  • Polypropylene (PP)/bamboo fiber (BF) composites were fabricated by twin screw extruder in order to investigate effects of the compatibilizer on physical properties of PP/BF composites. The content of BF changed from 10 to 25 wt% and that of the compatibilizer was fixed at 3 wt%. Maleic anhydride grafted PP (PP-g-MAH) was used to increase the compatibility between PP and BF as a compatibilizer. Chemical structures of the composites were confirmed by the existence of carbonyl group (C=O) stretching peak at $1,700cm^{-1}$ in FT-IR spectrum. Considering the degradation and mechanical properties, the optimum extrusion conditions were selected to be $210^{\circ}C$ and 100 rpm, respectively. There was no distinct changes in melting temperature of the composites, but the crystallization temperature increased by $10-20^{\circ}C$ owing to the heterogeneous nuclei of BF. It was checked that the optimum BF content was in the range of 15-20 wt% from the results of tensile and flexural properties of the composites. The effect of the compatibilizer on mechanical properties was confirmed by SEM images of fractured surface and contact angles.