• Title/Summary/Keyword: Extraction efficiency

Search Result 1,156, Processing Time 0.025 seconds

Extraction of Phenol from the Contaminated Soil Using Microwave Energy (Microwave Energy를 이용한 오염토양에서 Phenol의 추출)

  • 이기환;이태호;김윤아
    • Journal of Environmental Science International
    • /
    • v.12 no.4
    • /
    • pp.447-459
    • /
    • 2003
  • This study was carried out to develop an efficient process far the elimination of phenol pollutant from soils. An microwave-assisted process (MAP) and a conventional Soxhlet extraction method (SEM) were employed to extract phenol from two types of soils. The effects of extraction methods, aged time of the spiked soil samples, extraction solvent and extraction time on the extraction performance were compared. Our results demonstrate that the recoveries from standard soil spiked were at least 10% higher fer MAP than these f3r the conventional Soxhlet. The extraction time by MAP requires significantly shelter time (1 min) than 15 h of the conventional Soxhlet. The recoveries from non-contaminated soil spiked with phenol were also almost identical f3r above results. The reduction of the extraction times with efficiency higher than that afforded by the conventional Soxhlet technique supports the suitability of the MAP method.

A Study on the Improvement of Light-Extraction Efficiency of Organic Light-Emitting Diodes with a Use of Random-Textured Film (랜덤 택스쳐 필름을 이용한 유기 발광 소자의 광추출 효율 향상에 관한 연구)

  • Kim, Hye Sook;Hwang, Deok Hyeon;Jang, Kyeong Uk;Kim, Tae Wan
    • Journal of the Korean Institute of Electrical and Electronic Material Engineers
    • /
    • v.28 no.7
    • /
    • pp.446-449
    • /
    • 2015
  • An improvement of light-extraction efficiency of organic light-emitting diodes was studied by using random-textured films (RTF). Device was made in a structure of RTF/glass/ITO/TPD/$Alq_3$/LiF/Al. RTF mold was made by spreading PDMS solution on a sandpaper. By pressing this mold on the glass substrate pre-coated with ZPU material, the RTF was obtained. From this study, there was an improvement of external quantum efficiency by about 30% in the device with the random-textured film (RTF 40) compared to that of the reference one.

An Efficient Three-Dimensional Capacitance Extraction Based on finite Element Method Adopting Variable Division (가변 분할을 적용한 유한 요소법에 의한 3차원 모형의 효율적인 커패시턴스 추출 방법)

  • 김정학;김준희;김석윤
    • The Transactions of the Korean Institute of Electrical Engineers C
    • /
    • v.52 no.3
    • /
    • pp.116-122
    • /
    • 2003
  • This paper proposes an efficient method for computing the 3-dimensional capacitance of complex structures. The proposed method Is based on Finite Element Method(FEM) and expands the conventional FEM by adopting variable division. This method improves the extraction efficiency 50 times when compared to the conventional FEM with equal division. The proposed method can be used efficiently to extract electrical parameters of on/off-chip interconnects in VLSI systems.

The Study on Prediction of Hot Water Extraction in a Thermal Energy Storage System (축열시스템의 온수이용 예측에 관한 연구)

  • Cho, W.;Pak, E.T.
    • Solar Energy
    • /
    • v.18 no.3
    • /
    • pp.71-80
    • /
    • 1998
  • In thermal energy storage system, energy collected from many types of heat source is stored in a storage tank and then supply to load for demand. Lately, practical use of thermal energy storage system and attention to essential use of energy have been increased. From this point of view, especially, a study about the energy extraction process from a storage tank is necessary. So in this study, useful rate of hot water and hot water extraction efficiency was analysed respect to dynamic and geometric parameters dominating the hot water extraction process.

  • PDF

Optimization of Hot-water Extraction Conditions of Polyphenolic Compounds from Lipid Extracted Microalgae (탈지미세조류로부터 폴리페놀 생산 증대를 위한 열수추출 조건 최적화)

  • Choi, Kanghoon;Lee, Jihyun;Jo, Jaemin;Shin, Seulgi;Kim, JinWoo
    • Korean Chemical Engineering Research
    • /
    • v.54 no.3
    • /
    • pp.310-314
    • /
    • 2016
  • The search for natural antioxidants as alternatives to synthetic products is growing. Microalgae have emerged as a source of natural antioxidants with significant and diverse health-promoting properties. In this study, the effects of hot-water extraction conditions on total polyphenol compounds (TPC) production were investigated for lipid extracted microalgae (LEA). In order to enhance the polyphenol productivity, the extraction variables including solvents, temperature, time and ethanol concentration were optimized. The results showed hot-water extraction provided a higher extraction efficiency than the organic solvents and extraction at high temperatures showed a better extraction efficiency. While hot-water extract showed a higher extraction efficiency compared to 98% ethanol extraction, the mixture of water and ethanol (40:60 v/v) showed the highest production of polyphenols. The maximum polyphenols of 3.35 mg GAE (gallic acid equivalent)/g DM were obtained at the optimized extraction time of 10 min, $100^{\circ}C$ and 40% ethanol, respectively. Although Tetraselmis KCTC 12236BP was preprocessed by hexane to remove lipid for bio-diesel production, the results showed LEA contains relatively high level of polyphenols compared to untreated microalgae which can be used in the production of value-added materials. The predictions obtained from the developed Peleg's model were compared with the experimental data under the same operating conditions. The predicted and experimental data were consistent, indicating the reliability of the model.

An Algorithm for Scaling Parameter Optimization of Watermarking using Random Dot Images (랜덤한 점분포를 가진 영상을 사용한 워터마킹에서 스켈링 파라메타의 최적화 알고리즘)

  • Lee, In-Jung
    • The Journal of Korean Institute of Communications and Information Sciences
    • /
    • v.29 no.6C
    • /
    • pp.901-906
    • /
    • 2004
  • For a digital image watermarking some autostereograms are used such as random dot images. In there, the extraction efficiency is good and the distortion rate is low. In this paper, we shall select an optimized scaling parameter which derives low distortion rate and high extraction efficiency, when we use a random dot images as like as autostereograms into some images except for extremely biased gray level images.

A Study on the Analytical Methods Using Solid-phase Extraction for the Determination of Phenols in Water

  • Jeon, Chi-Wan;Lee, Jung-Hwa;Lee, Sang-Hak
    • Proceedings of the Korean Environmental Sciences Society Conference
    • /
    • 2003.11a
    • /
    • pp.135-138
    • /
    • 2003
  • Based on solid phase extraction, gas chromatography and mass spectrometry procedure for determining phenol and its derivatives in natural water was presented. In solid phase extraction, three types of techniques using solid phase adsorption material were treated with acid and salt, and converted second portion of acetyl derivatives. Under the these condition, extraction efficiency and detection ability dependent on extraction methods were discussed. Obtained results using optimized solid phase extraction techniques showed more convenience, simplifier and lower cost than the conventional analytical methods with holding wide dynamic range and lower detection limits.

  • PDF

Extraction Conditions of Radical Scavenging Caffeoylquinic Acids from Gomchui (Ligularia fischeri) Tea (곰취차로부터 라디칼 소거능을 갖는 Caffeoylquinic Acid류 화합물의 추출조건)

  • Kim, Sang-Min;Kang, Suk-Woo;Um, Byung-Hun
    • Journal of the Korean Society of Food Science and Nutrition
    • /
    • v.39 no.3
    • /
    • pp.399-405
    • /
    • 2010
  • After Gomchui tea was prepared from leaves of Ligularia fischeri (Ledeb.) Turcz by blanching method, the antioxidant activity of major compounds in Gomchui tea was assessed. On-line HPLC-ABTS analysis revealed that caffeoylquinic acids (chlorogenic acids), such as 5-O-caffeoylquinic acid (5-CQA), 3,4-di-O-caffeoylquinic acid (3,4-DCQA), 3,5-di-O-caffeoylquinic acid (3,5-DCQA) and 4,5-di-O-caffeoylquinic acid (4,5-DCQA), were the major antioxidant compounds in Gomchui tea. The extraction efficiency of these compounds were examined in the various conditions such as extraction temperature, time and solvent. The results demonstrated that the extraction amount with water increased in proportion to extraction time (1~10 min) and temperature ($8{\sim}80^{\circ}C$). These active compounds were also extracted with water even at $8^{\circ}C$ (60% of $80^{\circ}C$), indicating that water is very good extraction solvent for extraction of these antioxidant constituents. However, the extraction efficiency of these compounds decreased when ethanol percentage in water increased. The extraction efficiency between Gomchui powder (no blanching) and tea was significantly different, and 60% of total antioxidant compounds in tea was removed from fresh leaves into water in blanching process, especially 3,5-DCQA (over 90%). Meanwhile, the sonication method didn't affect the extraction of these compounds in all solvents. These results suggest that Gomchui tea can be a good candidate for the tea beneficial to human health.

Liquid-Liquid Extraction for Recovery of Paclitaxel from Plant Cell Cultures by Adding Inorganic Salts (식물세포배양으로부터 파클리탁셀 회수를 위한 무기염이 첨가된 액-액 추출)

  • Ha, Geon-Soo;Kim, Jin-Hyun
    • Korean Chemical Engineering Research
    • /
    • v.54 no.1
    • /
    • pp.135-139
    • /
    • 2016
  • We developed a liquid-liquid extraction method using an inorganic salt to dramatically improve the recovery efficiency of the anticancer agent paclitaxel from plant cell cultures. As a result of liquid-liquid extraction using a diverse types of inorganic salt (NaCl, KCl, $K_2HPO_4$, $NaH_2PO_4$, $NaH_2PO_4{\cdot}2H_2O$), NaCl gave the highest yield (~96%) and lowest partition coefficient (0.053) of paclitaxel. The optimal NaCl/solvent ratio, methylene chloride/MeOH ratio, and pure paclitaxel content for liquid-liquid extraction using NaCl were 1% (w/v), 26% (v/v), and 0.066% (w/v), respectively. Under the optimal conditions developed in the present method, most of the paclitaxel (~96%) was recovered from biomass by a single extraction step. In addition, this method facilitated 3-fold higher recovery efficiency of paclitaxel in a shorter extraction number than the conventional liquid-liquid extraction method.

Microwave-Assisted Extraction of Effective Constituents from Ginseng (마이크로파를 이용한 인삼으로부터 유효성분의 추출)

  • Lee, Dong-Won;Park, Young-Sin;Kim, Dok-Chan
    • Applied Chemistry for Engineering
    • /
    • v.16 no.3
    • /
    • pp.427-433
    • /
    • 2005
  • The use of the microwave-assisted process for the extraction of effective constituents from ginseng was investigated at various operating conditions. The influence of solvent (ethanol-water, 50% v/v) to ginseng ratio, particle size and applied microwave power on the efficiency of extraction was examined. The microwave extraction system used was custom manufactured so that the intensity of microwave may be varied by using anode-voltage controller. It was found that the ratio of 6 : 1 (vol/mass) gave a good extraction efficiency. Small particle size gave high yield but it caused difficulties in the separation of solvent from the sludge. The higher power was no guarantee of the efficient extraction yield. The more important factor than the employed power was the adequate temperature under sufficient contact time. Using deionized-water as swelling agent, the degree of swelling of ginseng by microwave heating and conventional heating in water-bath was also studied. It was observed that the microwave heating enhanced the swelling much more than the conventional heating. It is believed that this enhanced swelling was responsible for the rapid microwave-assisted extraction rate.