• Title/Summary/Keyword: Experiments with Materials

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Optimization of Barium Titanate Slip for Tape Casting Using Design of Experiments

  • Kwon, Sung-Wook;Darsono, Nono;Yoon, Dang-Hyok
    • Journal of the Korean Ceramic Society
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    • v.43 no.9 s.292
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    • pp.519-526
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    • 2006
  • A full-factorial design of experiments with three input factors and two levels for each factor including center points was utilized for the preparation and characterization of twelve types of $BaTiO_3$ slips for tape casting. Ceramic powders with different particle sizes, different milling methods such as high energy milling and conventional ball milling, and two types of dispersant with different polymeric species were chosen as input factors in order to investigate their effects on slip and on green tape properties. Tape casting, a small rectangular-shaped K-square preparation, characterization and quantitative data analysis using statistical software were followed. Ceramic powder was the most significant among three input factors for the output responses of slip viscosity and green tape density, showing more favorable results with large particles than with very fine ones. In addition, high energy milling for only 30 min was more efficient than 24h of conventional ball milling in terms of powder dispersion and milling. The optimum condition based on the experimental results was a slip exposed to high energy milling with large ceramic particles along with a methylethyl acetate dispersant.

Self-adaptive and Bidirectional Dynamic Subset Selection Algorithm for Digital Image Correlation

  • Zhang, Wenzhuo;Zhou, Rong;Zou, Yuanwen
    • Journal of Information Processing Systems
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    • v.13 no.2
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    • pp.305-320
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    • 2017
  • The selection of subset size is of great importance to the accuracy of digital image correlation (DIC). In the traditional DIC, a constant subset size is used for computing the entire image, which overlooks the differences among local speckle patterns of the image. Besides, it is very laborious to find the optimal global subset size of a speckle image. In this paper, a self-adaptive and bidirectional dynamic subset selection (SBDSS) algorithm is proposed to make the subset sizes vary according to their local speckle patterns, which ensures that every subset size is suitable and optimal. The sum of subset intensity variation (${\eta}$) is defined as the assessment criterion to quantify the subset information. Both the threshold and initial guess of subset size in the SBDSS algorithm are self-adaptive to different images. To analyze the performance of the proposed algorithm, both numerical and laboratory experiments were performed. In the numerical experiments, images with different speckle distribution, different deformation and noise were calculated by both the traditional DIC and the proposed algorithm. The results demonstrate that the proposed algorithm achieves higher accuracy than the traditional DIC. Laboratory experiments performed on a substrate also demonstrate that the proposed algorithm is effective in selecting appropriate subset size for each point.

The Effects of Parka on Subject Wear Sensation as to Thermal Resistance (파카의 보온성에 따른 착용감에 관한 연구)

  • Lee Yoon-Jung;Lee Soon-Won
    • Journal of the Korean Society of Clothing and Textiles
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    • v.13 no.3 s.31
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    • pp.295-303
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    • 1989
  • This study is to measure the thermal resistance of 7 types of Parka of different materials with thermal manikin and to compare their effects on physiological responses & subjective wear sensations. Following are the results obtained from the experiments 1) From the thermal manikin experiment, i) As an outer layer, although not significant, water proof fabric was warmer than water proof-vapor permeable fabric. ii) In case of insulating material, down was better for thermal resistance than polyester wadding of the same thickness. Moreover, as the down was thicker, it had more efficiency in thermal resistance. However, the marginal efficiency of thickness was found to be decreasing. 2) From the male-subject experiments, i) Chest temperature, mean skin temperature & microclimate temperature showed the same results on thermal resistance as those of the thermal manikin experiment. ii) Only during rest periods, there was a significant difference among 5 insulating materials in the sense of microclimate humidity. The almost same conclusion was obtained from the above experiments. Even the outer layer did not significantly affect thermal resistance & subjective wear sensation, insulating materials had a significant influence upon them. But in case of 3.5 cm down, it gave less comfortable than that of the thinner. Therefore the optional one for the best comfort & thermal resistance among 7 combinatins is the outer layer of water proff-vapor permeable & insulating material of 2.1 cm down.

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Chloride diffusion in concrete associated with single, dual and multi cation types

  • Song, Zijian;Jiang, Linhua;Zhang, Ziming
    • Computers and Concrete
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    • v.17 no.1
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    • pp.53-66
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    • 2016
  • Currently, most of the investigations on chloride diffusion were based on the experiments and simulations concerning single cation type chlorides. Chloride diffusion associated with dual or multi cation types was rarely studied. In this paper, several groups of diffusion experiments are conducted using chloride solutions containing single, dual and multi cation types. A multi-ionic model is also proposed to simulate the chloride diffusion behavior in the experimental tests. The MATLAB software is used to numerically solve the nonlinear PDEs in the multi-ionic model. The experimental and simulated results show that the chloride diffusion behavior associated with different cation types is significantly different. When the single cation type chlorides are adopted, it is found that the bound rates of chloride ions combined with divalent cations are greater than those combined with monovalent cations. When the dual/multi cation type chlorides are adopted, the chloride bound rates increase with the $Ca^{2+}/Mg^{2+}$ percentage in the source solutions. This evidence indicates that the divalent cations would markedly enhance the chloride binding capacity and reduce the chloride diffusivity. Moreover, on the basis of the analysis, it is also found that the complicated cation types in source solutions are beneficial to reducing the chloride diffusivity.

Heat Treatment Using a Laser Beam or an Electron Beam (레이저 및 전자빔을 이용한 표면 열처리)

  • 김홍준;최우천;권영각
    • Transactions of the Korean Society of Mechanical Engineers
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    • v.19 no.2
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    • pp.427-432
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    • 1995
  • Surface heat treatment using a laser beam or an electron beam is studied through numerical analyses and experiments. For the surface heat treatment process, a theoretical model is developed to predict the effects of laser beam power, travel speed and properties of a workpiece on the depth and width of the heat affected zone(HAZ). The shape of HAZ and the hardness of heat-treated surface are experimentally obtained using an electron beam. Three materials(SS41, S45C and S55C) are selected as workpiece materials. The hardness of HAZ is increased up to 3 times for materials of a low carbon content. The results of the numerical analysis are compared with those of experiments. The comparison shows that the numerical model predicts larger depths and widths.

A Review of the Optimum Feeding Rates in Olive Flounder (5 g through 525 g) Paralichthys olivaceus Fed the Commercial Feed

  • Okorie, Okorie Eme;Kim, Young Chul;Kim, Kang-Woong;An, Cheul Min;Lee, Kyeong-Jun;Bai, Sungchul C.
    • Fisheries and Aquatic Sciences
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    • v.17 no.4
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    • pp.391-401
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    • 2014
  • Ten feeding trials were conducted to determine and to make the guideline for the optimum feeding rates in olive flounder Paralichthys olivaceus fed extruded pellets at various growth stages at the optimum rearing water temperature. The entire trials were grouped into four growth stages, namely the first stage of juvenile (5 and 9 g), the second stage of juvenile (20, 30, 40 and 50 g), growing (240 and 317 g) and sub-adult (384 and 525 g) stages with 2, 4, 2 and 2 feeding trials, respectively. In the first and second experiments, results indicated that the optimum feeding rates for the first stage of juvenile olive flounder weighing 5 and 9 g could be >5.17 but <5.52% and >4.44 but <4.64% body weight (BW)/day, respectively. In the third, fourth, fifth and sixth experiments, results suggested that the optimum feeding rates for the second stage of juvenile olive flounder weighing 20, 30, 40 and 50 g could be >3.47 but <3.50, >2.85 but <3.53, >2.58 but <3.04 and >2.36 but <2.50% BW/day, respectively. In the seventh and eighth experiments, results showed the optimum feeding rates for growing olive flounder weighing 240 and 317 g to be >1.03 but <1.25 and >0.85 but <1.0 % BW/day, respectively. In the ninth and tenth experiments, the optimum feeding rates in sub-adult olive flounder weighing 384 and 525 g were shown to be >0.69 but <0.7 and >0.55 but <0.8% BW/day, respectively. We will compare these results with the previous studies done by other research groups.

Experimental Comparison of Electrohydraulic Forming of SUS430 with Free Bulging Die Depending on Wire of Electrodes (전극봉의 와이어 체결 유무에 따른 자유 벌징 금형의 액중방전성형 실험을 통한 SUS430 소재의 성형성 비교)

  • Y. H. Jang;M. S. Kim;J. Kim
    • Transactions of Materials Processing
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    • v.32 no.6
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    • pp.303-310
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    • 2023
  • Electrohydraulic forming(EHF), one of the high-speed forming method, can supplement the weak point of previous forming process such as deep-drawing and electromagnetic forming. Indeed, EHF is time-consuming process during installing wire before experiment that hard to apply to industry. In this research, applying wireless electrode, the formability of SUS430 sheet was compared through EHF experiments using wire-installed electrode and the other, wireless. Although the power was a little lacking, the advantages of the experiment using wireless electrode could be confirmed with checking the optimal location of electrodes where the plasma is generated and comparing free-bulging height depending on former and later condition of electrodes with performing several single and multistage experiments for same voltage, 6 kV.

A Study on the Analysis of Fire Mechanisms in Electronic Products due to Failure and Malfunction of Thermostats Through Fire Cases and Reproduction Experiments (화재사례 및 재현실험을 통한 온도조절장치 고장 및 오동작으로 인한 전자제품 화재 메커니즘 분석)

  • Jeong-il Lee;Jong-Hwa Im
    • Journal of the Korea Safety Management & Science
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    • v.26 no.1
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    • pp.31-38
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    • 2024
  • In this paper, as there are many cases of fires occurring due to the failure or inoperability of the thermostat of electronic products, the purpose is to test and analyze the risks and probabilities through fire cases and reproduction experiments, and suggest countermeasures. Among electronic products, water purifiers are composed of a refrigerant system with a compressor to make cold water, a heating device to make hot water, and an electric device used as an energy source. Due to the nature of the water purifier manufacturing, these devices are subject to a lot of moisture and dust. etc. exist in large quantities and use electrical energy, so there is a possibility of fire due to short circuit in the wire, electrical abnormal overheating (tracking phenomenon) in the thermostat, electronic board, starting relay, etc., and overheating of the heating device (Band Heater). there is. Therefore, in order to prevent fires from these devices, a system to remove foreign substances inside the water purifier is necessary, the use of heat-resistant (fire-resistant) wires for electrical devices is essential, and the use of non-combustible materials (semi-combustible materials) for each part is necessary to prevent fire. The risk must be eliminated through prevention and combustion expansion prevention devices.

Poisson's ratios of fabric materials in use for large-span membrane structures

  • Jianhui Hu;Wujun Chen;Chengjun Gao;Yibei Zhang;Yonglin Chen;Pujin Wang
    • Structural Engineering and Mechanics
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    • v.90 no.6
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    • pp.543-549
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    • 2024
  • The utilization of the fabric materials for lightweight building structures has attracted considerable attention due to the multiple functions and high strength-to-weight ratio. The mechanical properties of the fabric materials evolve with the loading cycle, especially for the Poisson's ratio that requires the full cyclic strain to determine the accurate values. The digital image correlation method has been justified but needs to meet the flexibility and complexity requirements of the fabric materials. This paper thus proposes a modified digital image correlation method to quantify the Poisson's ratio of fabric materials. To obtain the accurate Poisson's ratio of fabric materials in the cyclic experiments using non-contact measuring method, a speckle generation of the digital image correlation method is implemented to obtain the strain distribution and strain characteristics. The uniaxial cyclic experiments for the fabric materials are carried out in the warp, weft and 45° directions. The digital image correlation photos are taken when the material properties become stable in the cyclic loading. The results show that the strain distributions are non-uniform and dependent on the specimen directions. The reliable Poisson's ratios of the fabric materials in the warp, weft and 45° directions are 0.016, 1.2 and 2.6. The strain asymmetry at the maximum strain position is related with the weaving architecture. These observations and results are indispensable to understand the Poisson's ratios of fabric materials and to guide the proper analysis of the large-span membrane structures.

Optimization of Wet Reduction Processing for Nanosized Cobalt Powder (나노코발트 분말합성을 위한 액상환원공정의 최적화)

  • Hong, Hyun-Seon;Jung, Hang-Chul;Kim, Geon-Hong;Kang, Lee-Seung;Suk, Han-Gil
    • Journal of Powder Materials
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    • v.20 no.3
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    • pp.191-196
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    • 2013
  • Nano-sized cobalt powder was fabricated by wet chemical reduction method at room temperature. The effects of various experimental variables on the overall properties of fabricated nano-sized cobalt powders have been investigated in detail, and amount of NaOH and reducing agent and dropping speed of reducing agent have been properly selected as experimental variables in the present research. Minitab program which could find optimized conditions was adopted as a statistic analysis. 3D Scatter-Plot and DOE (Design of Experiments) conditions for synthesis of nano-sized cobalt powder were well developed using Box-Behnken DOE method. Based on the results of the DOE process, reproducibility test were performed for nano-sized cobalt powder. Spherical nano-sized cobalt powders with an average size of 70-100 nm were successfully developed and crystalline peaks for the HCP and FCC structure were observed without second phase such as $Co(OH)_2$.