• Bulletin of the Korean Chemical Society
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• v.10 no.5
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• pp.411-414
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• 1989

A new sensitive fluorimetric method for the determination of N-methylcarbamates, a class of well known insecticides, based on the derivatization with 7-chloro-4-nitrosobenz-2-oxa-1,3-diazole (NBD-Cl) has been developed. Unreacted NBD-Cl was eluted ahead of derivatized carbamates from C-18 bonded column. An argon ion laser was used as an excitation source of chromatographic eluents and its fluorescence signal was monitored with optical multichannel analyzer. The detection limits of various carbamates were about 100 pg range and the working curves were linear to $10^4-10^5$ nanogram ranges.

• Proceedings of the Korean Radioactive Waste Society Conference
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• 2004.06a
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• pp.137-146
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• 2004

Laser Induced Breakdown Spectroscopy(LIBS) system is being developed as an in-situ analysis system for the radioactive waste glass in the cold crucible melter. In order to complete the LIBS system, a spectrometer, a detector, and a laser were structured. An ESA 3000 (LLA Instruments GmbH, Germany) including a calibrated Kodak KAF-1001 CCD detector was selected as the spectrometer. A Q-switched Nd-YAG Brilliant(Quantel, France) laser was selected as an energy source. As the first research stage, the excitation temperatures of Fe(I) as a function of the detector's delay intervals(500, 1000, 1500, 2000ns) were evaluated using the Einstein-Boltzmann equation. The optimized excitation temperature of Fe (I) was 7820k at the delay time of 1500㎱ using the 532nm Nd-YAG laser pulse. This LIBS system will be optimized under the real environment vitrification facility in the near future and then used to be in-situ analyzed the glass compositions in the melter qualitatively.

• The KSFM Journal of Fluid Machinery
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• v.16 no.3
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• pp.18-25
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• 2013

Recently the requirement of long-term mobile energy source for mobile robot or small-sized unmanned vehicle is highly increased, and the micro turbine generator(MTG) which is known to have high energy and power density is under development. MTG is designed to have air foil bearing and high speed rotor of which operating speed is 400,000rpm. In the development stage of high speed rotor and bearing, stability analysis for the full operational speed range is essential and the dynamic coefficients such as stiffness and damping coefficients of bearing depending on the rotational speed are required for that. Although perturbation method is usually used to identify the dynamic coefficients, it's not easy to give the perturbation to the high speed rotating rotor. In this study, we present the dynamic coefficients measurement system for air foil bearing which consists of electromagnets, gap sensors, high speed motor and controller. This measurement system can exert the sine sweep force to the rotor-bearing, measure the displacement of rotor and get FRF(Frequency response function) of rotor-bearing. The least square estimation method is applied to identify the dynamic coefficients of bearing from the measured frequency response at the different rpm and the identified dynamic coefficients for the wide rotational speed range are presented.

• Journal of KSNVE
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• v.8 no.6
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• pp.1158-1165
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• 1998

Low frequency interior noise in cars is mainly due to structure-borne excitations which are related with road excitation and component vibrations such as suspension and engine mounts. In order to analyze the annoying interior noise. a technique (Transfer Path Analysis) is introduced to find a noise source and the path of that noise. In this study, TPA is reviewed theoretically and applied to investigate the case when the low frequency interior noise at front seat due to road excitations needs to be optimized. The subjective and objective appraisal was performed under the conditions that a testing vehicle traveled on asphalt at 30 km/h. so that the low frequency to be eliminated was detected. The related vibration and noise data for TPA were measured on running and static vehicle. The results reveal that the noise contribution along the z-direction of trailing arm is prominent to low frequency interior noise.

• Journal of the Korea Academia-Industrial cooperation Society
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• v.12 no.3
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• pp.1117-1121
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• 2011

The movable bracket structure, which is an apparatus for supplying electric power to a running electric locomotive, is applied by a repeated load during the passage of the electric locomotive. Such a repeated load becomes an excitation source that causes screws constituting the movable bracket structure to be loosened. This study was conducted on the causes and countermeasures of the bolt loosening caused by the repeated vibration using a computer simulation. As the result, a simulation model was constructed to enable the dynamic analysis of the movable bracket structure. It could be found that the principal excitation frequency range for the bolt loosening of the movable bracket structure was less than 200 Hz. In addition, the bolts are prevented from being loosened by increasing stiffness of H beams. The vibration mode of a lower band bracket is found to be triggered in a frequency range between 300 and 600 Hz. And the increase in stiffness of the lower band bracket exhibits the effect to avoid the bolt loosening at a frequency range of 200 Hz or more.

• The Transactions of the Korean Institute of Power Electronics
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• v.6 no.3
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• pp.250-257
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• 2001

SRM drives generate large vibration and acoustic noise because it is rotated by step pulse mmf and switching commutation mechanism. The main vibration source of SRM drive is generated by rapidly variation of radial force when phase winding current is extinguished for commutation action. So the rapidly variation of radial force is repressed firstly to reduce vibrating force of SRM drive. This paper suggests an SRM excitation scheme using unidirect-short compensation winding to reduce vibration of the motor. The motor is excited by a two stage commutation method during commutation period. This paper suggests an SRM excitation scheme using unidirect-short compensation winding to reduce vibration of the motor. The motor is excited by a tow stage commutation method during commutation period. This reduction effect of vibration is verified with the result obtained in the test of prototype machine.

• Journal of Advanced Marine Engineering and Technology
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• v.36 no.2
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• pp.267-275
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• 2012

In this study, normal wind load and blast wind load are modeled mathematical. And the periodical torque and bending moments transmitted to the main shaft of wind turbine are investigated. A normal wind model assumed, of which the wind velocity is increased according to the height from ground. The average values and the harmonic terms of the transmitted moments are studied on the wind direction of range $-45^{\circ}{\sim}45^{\circ}$ and the bending moment characteristics are examined, which is regarded as the main source of the misalignment of gear train. In normal wind load case, excitation frequency is 3X (X : Rotor speed). When the wind direction is $+22.5^{\circ}$, the horizontal axis of bending moment occur the 50% of main torque. This result leads to edge contact of gear teeth by shaft elastic deformation. In blast wind load case, excitation frequency are 3X,6X,9X. Additional, in the (+) direction of wind load, relative harmonic percentage is increase.

• Ceramist
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• v.22 no.3
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• pp.281-300
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• 2019

Surface enhanced Raman scattering (SERS) was first discovered in 1974 by an unexpected Raman signal increase from Pyridine adsorbed on rough Ag electrode surfaces by the M. Fleishmann group. M. Moskovits group suggested that this phenomenon could be caused by surface plasmon resonance (SPR), which is a collective oscillation of free electrons at the surface of metal nanostructures by an external light source. After about 40 years, the SERS study has attracted great attention as a biomolecule analysis technology, and more than 2500 new papers and 500 review papers related to SERS topic have been published each year in recently. The advantages of biomaterials analysis using SERS are as follows; ① Molecular level analysis is possible based on unique fingerprint information of biomolecule, ② There is no photo-bleaching effect of the Raman reporters, allowing long-term monitoring of biomaterials compared to fluorescence microscopy, ③ SERS peak bandwidth is approximately 10 to 100 times narrower than fluorescence emission from organic phosphor or quantum dot, resulting in higher analysis accuracy, ④ Single excitation wavelength allows analysis of various biomaterials, ⑤ By utilizing near-infrared (NIR) SERS-activated nanostructures and NIR excitation lasers, auto-fluorescence noise in the visible wavelength range can be avoided from in vivo experiment and light damage in living cells can be minimized compared to visible lasers, ⑥ The weak Raman signal of the water molecule makes it easy to analyze biomaterials in aqueous solutions. For this reason, SERS is attracting attention as a next-generation non-invasive medical diagnostic device as well as substance analysis. In this review, the principles of SERS and various biomaterial analysis principles using SERS analysis will be introduced through recent research papers.

• Journal of the Korean Society of Fisheries and Ocean Technology
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• v.27 no.3
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• pp.193-210
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• 1991

For the deckhouse or superstructure, attention is directed to the reduction of vibration from a human susceptibility point of view. The two basic requirements for obtaining a low vibration level in the accommodation are to ensure that excitation forces from propeller and/or main engine are small and to avoid resonance excitation of the hull and superstructure. In recent years increased attention has been directed towards the problems of vibration and noise in deckhouse, which have caused major problems with regard to the environmental quality in the living quarters for crews. Accordingly, in this paper, the characteristic of the vibration of deckhouse of fishing boat, of which the length/height ratio is also relatively high, are studied systematically with regard to the shape and modelling of deckhouse based on finite element method of 1-dimensional, 2-dimensional and 3-dimensional model. This study is divided into 4-part. 1st part is the global deckhouse vibration, 2nd part is the local deckhouse vibration, 3rd part consists of the estimation for stiffness of foundational support and 4th part is the application to TUNA LONG LINER of 416 ton class. For the global vibration analysis, the severity of the vibration depends on the longitudinal shear and bending stiffness of the deckhouse, on the vertical deckhouse support(fore, aft and sides). However, even if the design is technically sound, vibration problems may arise due to vertical or longitudinal hull girder or afterbody resonances. Author applied the method of this study to the analysis of, deep-sea fishing vessel of G.T. 416 ton class with relatively low height and long deckhouse, and investigated the vibrational characteristic of the fishing vessel with earlier structural feature. According to this investigation, the vibration, response of above vessel was confirmed of which main hull and deckhouse behave as one body. It is at the bottom of vibrational trouble which a accommodation part of the fishing vessel is raised, that is the local vibration for side wall, fore-aft wall and deck plate of deckhouse rather than thief fect of fore-aft vibration of deckhouse for above fishing vessel. and the resonance of main hull, deckhouse and driving system such as the main engine, propeller in exciting source is mainly brought up as the trouble.

• Korean Journal of Materials Research
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• v.13 no.8
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• pp.537-542
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• 2003

($Y_{l-x}$ $Gd_{x}$ )$O_2$$_3$: $Eu^{ 3＋}$ red phosphors were prepared with the solvothermal synthesis using the 2-methoxy-ethanol solvents and the emission intensity was investigated that applied with the 254 nm wavelength and the maximum excitation wavelength for energy source. The used solvents for the solvothermal synthesis were made of nitrate salt solutions of Y, Gd and Eu. These solutions dropped in autoclave have be reacted with the solvothermal synthesis at $200^{\circ}C$ for 5hrs and the red phosphors prepared here in were showed the pure cubic phase after annealing at $1000∼1200^{\circ}C$. The brightness of ($Y_{l-x}$ $Gd_{x}$)$_2$$O_3$: $Eu^{3＋}$ phosphors particles was increased as an increase of Gd ratio. The maximum excitation wavelengths of ($Y_{l-x}$ $Gd_{x}$ )$_2$$O_3$: $Eu^{3＋}$ / phosphors particles were increased according to increasing Gd ratio from 253 nm to 259 nm wavelength. The maximum emission intensity of $Gd_2$$O_3$: $Eu^{3＋}$ (Y/Gd = 1/0) phosphors particles under UV 259 nm was found to be higher than the commercial product of $Y_2$$O_3$: $Eu^{3＋}$ phosphors.