• 제목/요약/키워드: Electron-beam evaporation

검색결과 217건 처리시간 0.022초

유기 EL 보호층으로 적용하기 위한 무기 복합 박막의 투습율 특성 연구 (Study on the Water Vapor Permeation Properties of the Inorganic Thin Composite Film for the Passivation Layer in the OLED)

  • 김광호;이주원;김영철;주병권;김재경
    • 한국전기전자재료학회논문지
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    • 제17권4호
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    • pp.432-438
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    • 2004
  • In this study, we investigated the WVTRs Properties of inorganic thin composite films(ITCFs) to be newly adopted as the passivation layer of the OLED to replace the inorganic compound material Because we thought that inorganic compound materials were limited to enhance the barrier property of thin film. So, ITCFs were fabricated by mixing the cooperated material with the base material. And then, ITCFs were deposited onto the plastic substrate using the electron beam evaporation system and the water vapor transmission rates(WVTRs) were measured using the Mocon equipment. As a result of the WVTR measurement, we could analyze the WVTR values for various ITCFs. ITCFs had a remarkably lower value than the inorganic compound film. Through the analysis of thin film, we can understand the crystal structure and mixed amount. Therefore, ITCFs can be used as the inorganic passivation layers of OLED with the inorganic compound film.

Fe2O3 첨가에 따른 AC PDP 보호막용 MgO 박막의 광학적.전기적 특성 (Effects of Fe2O3 Addition on Optical and Electrical Properties of MgO Films as a Protective Layer for AC PDPs)

  • 김창일;정영훈;이영진;백종후;최은하;정석;김정석
    • 한국전기전자재료학회논문지
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    • 제22권9호
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    • pp.760-765
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    • 2009
  • The effects of $Fe_2O_3$ addition on optical and electrical properties of MgO films as a protective layer for AC plasma display panels were investigated. Doped MgO films prepared by the e-beam evaporation have a higher ${\gamma}$ (secondary electron emission coefficient) than pure MgO protective layer. Roughness increased with amount of $Fe_2O_3$ up to 100 ppm and then decreased further addition. These results showed that discharge properties and optical properties of MgO protective layers seemed to be closely related with microstructure factors such as roughness. Good optical and electrical properties of ${\gamma}$ of 0.120, surface roughness of 14.1 nm and optical transmittance of 94.55% were obtained for the MgO + 100 ppm $Fe_2O_3$ protective layer sintered at $1700^{\circ}C$ for 5 hrs.

Optical and Electrical Properties of Thin Film Electroluminescent Devices with SrS:Cu, Ag Phosphor Layer

  • Chang, Ho-Jung;Park, Jun-Seo;Chang, Young-Chul
    • 마이크로전자및패키징학회지
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    • 제9권1호
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    • pp.29-33
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    • 2002
  • The SrS:Cu, Ag thin film electroluminescient devices were fabricated on $AlTiO_3$/ITO/glass substrates by electron-beam evaporation. The emission spectrum of the device was about 460 nm with $\chi$=0.20, y=0.29 in the CIE color coordinator. It was found that the emission spectrum was saturated to pure blue color when Ag sensitizer was doped in SrS:CuCl phosphors. The luminance of the device was increased by increasing the sulfur pressure. The measured luminance was saturated with 430 cd/$m^2$at the applied voltage of 90 V and the maximum luminance was 580 cd/$m^2$at 110V. The polarization charge and conduction charge of the devices were found to be found to be about $3.5\mu$C/$\textrm{cm}^2$ and $7.4\mu$C/$\textrm{cm}^2$, respectively.

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Gd2O3 첨가에 따른 AC PDP 보호막용 MgO 박막의 광학적.전기적 특성 (Effects of Gd2O3 Addition on Optical and Electrical Properties of MgO Films as a Protective Layer for AC PDPs)

  • 김창일;임은경;박용준;이영진;백종후;최은하;정석;김정석
    • 한국전기전자재료학회논문지
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    • 제20권7호
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    • pp.620-625
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    • 2007
  • The effects of $Gd_2O_3$ addition and sintering condition on optical and electrical properties of MgO films as a protective layer for AC plasma display panels were investigated. Doped MgO films prepared by the e-beam evaporation have a higher ${\Upsilon}$ (secondary electron emission coefficient) than pure MgO protective layer. Relative density and grain size increased with amount of $Gd_2O_3$ up to 100 ppm and then decreased further addition. These results showed that discharge properties and optical properties of MgO protective layers seemed to be closely related with microstructure factors such as relative density and grain size. Good optical and electrical properties of ${\Upsilon}$ of 0.138, surface roughness of 5.77 nm and optical transmittance of 95.76 % were obtained for the MgO+100 ppm $Gd_2O_3$ protective layer sintered at $1700^{\circ}C$ for 5 hrs.

전자빔 증착법으로 제작한 Cu 박막의 부착력과 저항율 특성 (The Resistivity Properties and Adhesive Strength of Cu Thin firms Fabricated by EBE Method)

  • 백상봉;신중홍
    • 한국전기전자재료학회:학술대회논문집
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    • 한국전기전자재료학회 2003년도 추계학술대회 논문집 Vol.16
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    • pp.422-426
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    • 2003
  • Cu thin films of $6000{\AA}$ thickness were deposited by Electron Beam Evaporation(EBE) method on the glass. The resistivity properties and adhesion of Cu thin films were investigated by various annealing and substrate temperature. Cu thin films were annealed in the air and vacuum condition for 10 min after the deposition. The resistivity and adhesion(the force required to separate films from substrates) was measured by 4-point probe and scratch testing. The resistivity of non-annealing Cu thin films was distinguished more substrate temperature loot than substrate temperature R.T, $200^{\circ}C$. In the case of air condition annealing, as heating temperature was increased, the resistivity was decreased. In the case of vacuum condition annealing, the resistivity was increased at heating temperature $200^{\circ}C$. The best resistivity($1.72\;{\mu}{\Omega}{\cdot}cm$) of Cu thin films was obtained by the air condition heating temperature $200^{\circ}C$ at the substrate heating temperature $100^{\circ}C$. As a result of scratch testing, adhesion was increased by annealing. And maximum adhesion had 600 gf.

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승화법에 의한 CdSe 성장과 특성 (Growth and characterites for CdSe single crystal grown by using sublimation method)

  • 홍광준;백승남;;김도선
    • 한국전기전자재료학회:학술대회논문집
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    • 한국전기전자재료학회 2006년도 하계학술대회 논문집 Vol.7
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    • pp.180-181
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    • 2006
  • CdSe single crystal was grown by sublimation method in the two-step vertical electric furnace. This CdSe single crustal had hexagonal structure whose lattice constants of $a_0$ and $c_0$ were measured $4.299\;{\AA}$ and $7.009\;{\AA}$ by extrapolation method, respectively. CdSe single crystal was n-type semiconductor values were measured from Hall data by Van der Pauw method in the room temperature. Mobility tends to increase in proportion to $T^{3/2}$ from 33K to 130K due to impurity scattering. but mobility tends to decrease in proprtion to $T^{-3/2}$ from 130K to 293K due to lattice scattering. CdSe thin film was made by electron beam evaporation technique had also hexagonal structure. The grain size of this thin film was grown to $1{\mu}m$ as a result of annealing in the vapor of Ar or Cd. Annealde CdSe thin film was n-type semiconductor whose carrier density had about $7{\times}10^{12}cm^{-3}$ and its mobility had about $1.6{\times}10^3cm^2/V$ sec at room temperature.

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Raman scattering spectroscopy as a characterization method of coated conductors

  • Um, Y.M.;Jo, W.
    • 한국초전도ㆍ저온공학회논문지
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    • 제9권4호
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    • pp.24-27
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    • 2007
  • The purpose of this work is to develop, integrate, and implement an optical characterization method to evaluate physical properties in coated conductors and investigate the local distribution of the causes of degraded performance. The method that we selected at this moment is Raman scattering spectroscopy, which is accompanied with measurements of local supercurrent transport, phase composition, microstructure, and epitaxy quality for coated conductors that range in size up to multi-meter-length tapes and that embrace the entire tape embodiment (substrate through cap layer). The establishment of Raman spectroscopy as an on-line process monitoring tool is our eventual goal of research, but it requires very robust and cost-effective equipments. We analyzed $YBa_2Cu_3O_7(YBCO)$ thin films grown at various substrate temperatures by using Raman spectroscopy. YBCO films were grown by a high-rate electron-beam co-evaporation method. Raman spectra of YBCO films with lower-transport properties exhibit additional phonon modes at ${\sim}300cm^{-1}$, ${\sim}600cm^{-1}$ and ${\sim}630cm^{-1}$, which are related to second-phases such as $Ba_2Cu_3O_{5.9}$ and $BaCuO_2$. We propose a new method to characterize Raman spectra of coated conductors for an in-line quality control.

터빈블레이드 형상 mock-up의 기하학적 배치조건에 따른 전자빔 물리기상증착법으로 제조된 7 wt% YSZ 열차폐 코팅의 코팅 균일성 (Deposition uniformity of 7 wt% YSZ as a thermal barrier coating with different configurational arrangement for turbine blade shape mock-up by electron beam physical vapor deposition)

  • 오윤석;채정민;류호림;한윤수;안종기;손명숙;김홍규
    • 한국결정성장학회지
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    • 제29권6호
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    • pp.308-316
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    • 2019
  • 전자빔 물리기상증착기술(EBPVD)은 주상형 성장거동과 같이 고온에서의 구조 안정성에 기여할 수 있는 특성으로 인해 터빈블레이드 등과 같은 항공기 엔진 고온부품의 열차폐 코팅(TBC) 제조기술로 개발되어 상용화된 기술이다. 전자빔 증착으로 열·기계적 특성이 상용화 가능한 수준에 만족하는 고품질 열차폐 코팅제조를 위해서는 성장거동, 균일두께형성 등과 같은 구조적 요소의 제어가 반드시 수반되어야 한다. 본 연구에서는 실품형상에 근사한 터빈 블레이드 mock-up에 대한 기하학적 코팅인자 조건에 따른 7YSZ(7 wt% 이트리아 안정화 지르코니아) 열차폐 코팅의 성장거동과 구조변화를 고찰하였으며, 전산모사 기법을 활용한 기하학적 코팅인자 조건에 따른 코팅성장거동 모델링을 수행하여 실제 코팅결과와 비교하였다.

광학적 방법을 통한 마이크로 역학 소자의 공진주파수 측정법과 이를 이용한 마이크로 캔티레버 공진기의 질량 변화 연구 (Detection of Resonance Frequency of Micro Mechanical Devices Using Optical Method and Their Application for Mass Detection)

  • 김학성;이상욱
    • 한국진공학회지
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    • 제21권1호
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    • pp.36-40
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    • 2012
  • 마이크로미터 크기의 역학적 공진기의 제작과 그 공진 주파수 변화를 이용하여 질량 변화량을 측정하는 방법에 대해 연구 하였다. 공진기의 공진 주파수를 측정하기 위해서 레이저의 간섭효과를 이용한 광학적 측정법을 사용하였는데 이 방법은 나노미터 스케일의 변위까지 감지할 수 있을 정도로 매우 감도가 높은 측정법이다. 공진기는 압전 세라믹(piezo ceramic) 위에 원자현미경(atomic force microscope)의 캔티레버를 붙여서 만들었는데 이 방법은 압전판이 캔티레버의 공진 주파수로 진동할 때 캔티레버의 변위가 가장 크게 변화됨을 이용한 것이다. 또한, 전자 빔 증착기(e-beam evaporation system)를 사용하여 금을 캔티레버 위에 증착하여 질량을 변화시킨 후에 질량 변화량에 따른 공진주파수의 변화량을 측정하였다. 이 공진기는 질량센서의 역할을 수행할 수 있으며 수 마이크로그램을 감지할 수 있는 감도를 가짐을 확인하였다.

Polynorbornene 기판 위에 증착된 IZO 필름의 전기 및 광학적 특성연구 (Electrical and Optical Properties of IZO Films Deposited on Polynorbornene Substrate)

  • 박성환;하기룡
    • 공업화학
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    • 제20권6호
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    • pp.612-616
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    • 2009
  • Transparent conducting oxide (TCO) 박막은 평판 디스플레이 산업에 널리 사용되고 있다. 화학적으로 우수한 투명전도성 indium zinc oxide (IZO) 필름은 현재 널리 사용되고 있는 indium tin oxide (ITO) 필름의 대체 물질로 관심을 끌고있다. 본 연구에서는 ITO에 비해 낮은 증착 온도에서도 낮은 비저항과 높은 투과율을 가지는 IZO 박막을 전자빔 증착법을 사용하여 polynorbornene (PNB) 기판(Tg = $330^{\circ}C$) 위에 증착하는 조건에 대하여 연구하였다. 90 : 10 wt%의 $In_2O_3$와 ZnO를 혼합하여 만든 타겟으로 전자빔 증착법을 이용하여 PNB 기판 위에 IZO 박막을 제조하여, 기판온도와 산소도입 속도에 따른 IZO 필름의 전기 광학적 특성을 연구하였다. 그 결과 4 sccm의 $O_2$, $150^{\circ}C$의 기판온도, 증착속도 $2{\AA}$/sec 및 $1000{\AA}$ 두께로 증착된 IZO 필름에서 우수한 전기 광학적 성질인 $5.446{\times}10^2{\Omega}/{\boxempty}$ 면저항 및 87.4% 광투과율을 얻을 수 있었다.