• Carbon letters
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• 제7권4호
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• pp.271-276
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• 2006

Porous carbon materials were prepared with a thermal treatment of coal tar pitch at 550 in the Ar gas. Growth, merger, and distribution of pore were characterized with scanning electron microscopy as variation ascending temperature gradient and chamber pressure. After graphitizing at the 2600 (1 hr.), walls and connecting parts between pores were investigated with X-ray diffraction patterns. Wall thickness and pore size decreases as increasing ascending temperature gradient, and pore size becomes homogeneous. Graphite quality and thermal conductivity become higher due to the enhanced orientation of walls and connecting parts between pores.

• 한국결정성장학회지
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• 제22권6호
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• pp.269-273
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• 2012

Ammonia decomposition over titanium carbides were investigated using eight different samples which have been synthesized by TPR (temperature-programmed reduction) method of titanium oxide ($TiO_2$) with pure $CH_4$. The resulting materials which were synthesized using wo different heating rates and space velocity exhibited the different surface areas. These results indicated that the structural properties of these materials have been related to heating rates and space velocity employed. The titanium carbides prepared in this study proved to be active for ammonia decomposition, and the activity changed with the particle size/surface area. These showed the relationship between ammonia decomposition activity and the different active species. Compared to molybdenum carbide, the titanium carbides were one order of magnitude less active, suggesting the correlation between the activity difference and the degree of electron transfer between metals and carbon in metal carbides.

• 전기의세계
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• 제29권2호
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• pp.118-128
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• 1980

The properties of plasmas produced by high power glass laser were investigated with various methods of diagnostics. Electron temperature was estimated by measurement of soft X-ray, and ion temperature was estimated by measurement of the time-of-flight of ion. The measurement of incident and reflected laser light, and Schlieren and shadowgragh methods were also used. No influence of laser pulse duration on the temperature was observed in the case of durations 2, 4 and 10 nsecs. The effective heating of plasma occurred in about 2 nsec of beginning of incident laser pulse. The experimental results for fast rising laser pulse were discussed and the influence of resetime of laser pulse on the heating of plasma was described. Neutrons produced by irradiating laser beam to solid deuterium target were detected.

• 한국안전학회지
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• 제29권4호
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• pp.61-72
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• 2014

The aim of this study is to define the condition of optimal pre-treatment for preferable activated carbon fibers (ACFs), which are based on rayon fibers. This paper shows the ideal path of ACFs preparation process; implies that rayon fibers are pre-treated by various solvents with different times before the heating process. The pre-treated rayon fibers finally turned into desirable rayon fiber-based ACFs through optimal pre-treatment condition by heating processes. The thermal analysis method of pre-treated rayon fibers by thermo-gravimetry analyser (TGA) is an idealized tool, which analyzes the best thermal condition of pre-treatment process. Surface morphologies of resulting rayon fibers based ACFs were examined by scanning electron microscope(SEM). The results of TGA and SEM analyses show that the optimal pre-treatment condition for preparing ACFs was clearly defined, in terms of thermal stability and surface morphology.

• 센서학회지
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• 제24권5호
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• pp.348-352
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• 2015

Thin nickel oxide films formed on uncooled and cooled $SiO_2/Si$ substrates using a radio frequency (RF) magnetron sputter powered by 200 W in a mixed atmosphere of argon and oxygen. Grazing-incidence X-ray diffraction and field emission scanning electron microscopy are used for the structural analysis of nickel oxide films. The electrical conductivity required for better bolometric performance is estimated by means of a four-point probe system. Columnar and (200) preferred orientations are discovered in both films regardless of substrate cooling. Electric resistivity, however, is greatly influenced by the substrate cooling. Oxygen partial pressure increase during the nickel oxide deposition leads to a rapid decrease in resistivity, and the resistivity is higher in the cooled nickel oxide samples. Even when small microstructure variations are applied, lower resistivity in favor of low noise performance is acquired in the uncooled samples.

• Nuclear Engineering and Technology
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• 제41권6호
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• pp.807-812
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• 2009

An ICRF discharge cleaning and a fast wave electron heating experiment were performed. For automated operation and providing the diagnostics of the ICRF system, the ICRF local network was designed and implemented. This internal network provides monitoring, RF protection, remote control, and RF diagnostics. All the functions of the control system were realized by customized DSP units. The DSP units were tied by a local network in parallel. Owing to the distributed feature of the control system, the ICRF local control system is quite flexible to maintain. Developing the subsystem is a more effective approach compared to developing a large controller that governs the entire system. During the first experimental campaign of the KSTAR tokamak, the control system operated as expected without any major problems that would affect the tokamak operation. The transmitter was protected from harmful over-voltage events through reliable operation of the system.

• Metals and materials international
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• 제24권6호
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• pp.1293-1302
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• 2018

Nanocrystalline (NC) Ni electrodeposits (EDs) with a mean grain size of $34{\pm}12nm$ has been investigated, from room temperature to $800^{\circ}C$ under a purge gas of argon, by both non-isothermal and isothermal differential scanning calorimetry measurements, in combination with characterization of temperature-dependent microstructural evolution. A significant exothermic peak resulting from superimposition of recrystallization and surface oxidation occurs between 340 and $745^{\circ}C$ at a heating rate of $10^{\circ}C/min$ for the NC Ni EDs. The temperatures for recrystallization and oxidation increase with increasing the heating rate. In addition, recrystallization leads to a profound brittle-ductile transition of the Ni EDs in a narrow range around the peak temperature for the recrystallization.

• Journal of Information Display
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• 제2권3호
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• pp.44-47
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• 2001

The extracted field emission current can be used to controllably heat microfabricated cold field emission cathode tips. The heating can be sufficient to smooth and recrystallize the tip surface by surface self-diffusion, and at least partially clean the surface of contaminants by thermal desorption. Self-heating not only allows for the achievement and maintenance of stable emission characteristics, but can be used to make the current-voltage characteristics of microfabricated field emitter tips nearly identical to one another. The resulting improvement in emission uniformity will allow for more reliable array operation at increased electron emission current densities.

• 한국진공학회지
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• 제21권3호
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• pp.121-129
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• 2012

진공을 기초로 한 극판 전력이 인가된 유도 결합 플라즈마 소스에 관한 대부분의 연구는 자기 바이어스 효과에만 한정되어 있으며, 다양한 반도체 및 디스플레이 식각 공정에서 공정 결과와 소자 품질에 결정적인 역할을 하는 플라즈마 변수들(전자 온도, 플라즈마 밀도)과 극판 전력의 상관관계에 대한 연구는 거의 없는 실정이다. 본 연구에서는 극판 전력이 플라즈마 변수에 미치는 영향에 관한 내용을 다루고 있으며, 최근의 연구 결과에 대한 리뷰를 포함하고 있다. 플라즈마 밀도는 극판 전력 인가에 의하여 감소 또는 증가하였으며, Fluid global model에 의한 결과와 잘 일치하는 경향을 보였다. 전자 온도는 RF 바이어스에 의하여 증가하였으며, 전자 에너지 분포 측정을 통하여 전자 가열 메커니즘을 관찰하였다. 또한, 플라즈마 밀도의 공간 분포는 극판 전력에 의하여 더욱 균일해짐을 알 수 있었다. 이러한 극판 전력과 플라즈마 변수들의 상관관계와 전자 가열 메커니즘에 대한 연구는 방전 특성의 물리적 이해뿐만 아니라, 반도체 식각 공정에서 소자 품질 및 공정 개선을 위한 최적의 방전조건 도출과 외부 변수 제어에 큰 도움을 주리라 예상된다.

• 센서학회지
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• 제13권4호
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• pp.292-297
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• 2004

Carbon nanotubes (CNT) were synthesized by arc-discharge method. To fabricate CNT sensor, CNT powder was dispersed in ${\alpha}$-Terpinol($C_{10}H_{17}OH$) solution. The CNT tilms were fabricated by screen printing method on the interdigitated Pt/Pd alloy electrode. The microstructure of CNT film was observed by scanning electron microscopy (SEM) and transmission electron microscopy (TEM). In order to investigate the gas sensing characteristics of the film, the CNT film was experimented to measure NO response and recovery time. The CNT sensor with a heater was compared to that without a heater. And this sensor shows better reproductibility and faster recovery time than another CNT sensors. We suggest the possibility to utilize a CNT as new sensing materials for environmental monitoring.