• Korean Journal of Materials Research
• /
• v.21 no.4
• /
• pp.225-231
• /
• 2011

The effect of ferrous/ferric molar ratio on the formation of nano-sized magnetite particles was investigated by a co-precipitation method. Ferrous sulfate and ferric sulfate were used as iron sources and sodium hydroxide was used as a precipitant. In this experiment, the variables were the ferrous/ferric molar ratio (1.0, 1.25, 2.5 and 5.0) and the equivalent ratio (0.10, 0.25, 0.50, 0.75, 1.0, 2.0 and 3.0), while the reaction temperature ($25^{\circ}C$) and reaction time (30 min.) were fixed. Argon gas was flowed during the reactions to prevent the $Fe^{2+}$ from oxidizing in the air. Single-phase magnetite was synthesized when the equivalent ratio was above 2.0 with the ferrous/ferric molar ratios. However, goethite and magnetite were synthesized when the equivalent ratio was 1.0. The crystallinity of magnetite increased as the equivalent ratio increased up to 3.0. The crystallite size (5.6 to 11.6 nm), median particle size (15.4 to 19.5 nm), and saturation magnetization (43 to 71 $emu.g^{-1}$) changed depending on the ferrous/ferric molar ratio. The highest saturation magnetization (71 $emu.g^{-1}$) was obtained when the equivalent ratio was 3.0 and the ferrous/ferric molar ratio was 2.5.

• Journal of Pharmaceutical Investigation
• /
• v.1 no.1
• /
• pp.30-33
• /
• 1971

Comparative studies were made on the analgesic effect of salicylamide, used individually and combined with parasympatholytics (propantheline and atropine) and antihistaminics (tripelennamine, diphenhydramine) as regards the analgesic effect (in thermal contact method) were examined by its oral administration with each combined drug to mouse (three assumption cross-over test), and the following effects were found. 1. The increasing order of the parasympatholytics to the analgesic effect of salicylamide is as follows: propantheline>atropine. 2. The increasing order of the antihistaminics to the analgesic effect of salicylamide is as follows: chlorpheniramine>diphenhdramine>tri pelennamine. In the ratio '1 : 1' salicylamide to parasympatholytics and antihistaminics, the analgesic effect of salicylamide was more increase than the other ratio in this study.

• Journal of Ocean Engineering and Technology
• /
• v.12 no.1
• /
• pp.65-75
• /
• 1998

The fracture resistance curve is one of most important and design techniques employed in nuclear pressure vessel structures. This study is to evaluate the J-R curve characteristics for the SA508C-3 by the unloading compliance method and load rato analysis. The effect of strain aging for the exponential correlation of the J-R curve in this metal are investigated at room temperature, 20$0^{\circ}C$ and 30$0^{\circ}C$. The load ratio analysis method can evaluate the J-R curve by using the simple tension load-displacement curve only without the repeat of the unloading and loading. Therefore, the analysis by the proposed load ratio method has a merit, in comparison with the unloading compliance method, which can measure the crack length without the precision measurement equipment.

• Journal of ILASS-Korea
• /
• v.25 no.3
• /
• pp.111-118
• /
• 2020

This paper describes the effect of DME, biodiesel blended fuels on the macroscopic spray characteristics in a high pressure diesel injection system using Background Oriented Schlieren (BOS) method. The BOS method for visualization of impingement evaporation sprays to analyze macroscopic spray properties and evolutionary processes. In this work, the blending ratio of DME in the blended fuel are 0, 50, 100% by weight ratio. In order to investigate the macroscopic impinged spray characteristics under the various injection parameters and blending ratio. In this work, a mini-sac type single-hole nozzle injector with nozzle hole was length 0.7 mm and diameter of 0.3 mm was used. According to the result, the spray area of the collision wall increased as the DME mixing ratio increased, and the evolutionary pattern showed a stepwise increase due to the collision effect of the wall. Also, results of impinged spray area were increased according to increasing injection pressure.

• Proceedings of the Korea Concrete Institute Conference
• /
• 1999.10a
• /
• pp.479-482
• /
• 1999

The tension stiffening effect, which means the maintaining a part of stiffness after cracking of concrete in tensile, exists at a reinforced concrete member because of the concrete softening and bonding stress between cracks. It is required to consider it for precise analysis and evaluation o structural behavior, due to the possibility of discrepancy between the actual behavior and the analysis without considering the tension stiffening effect. Making and adopting a tension stiffening model is the most simple and effective way for considering it at nonlinear analysis which indicated the estimation from models and experimental results were similar each others. The comparisons on RC beam were, also performed in order to analyzed the influence of concrete strength and steel ratio into the structural behavior. They indicated that the results from analysis estimated quite closely to the test results at low steel ratio, however, overestimated at high steel ratio. The overestimation increase linearly as concrete strength or steel ratio increased.

• Journal of Power System Engineering
• /
• v.17 no.6
• /
• pp.115-121
• /
• 2013

This study was carried out to investigate the effect of hot forging on the hardness and impact value of ultra high carbon low alloy steel. With increasing hot forging ratio, thickness of the network and acicular proeutectoid cementite decreased, and than were broken up into particle shapes, when the forging ratio was 80%, the network and acicular shape of the as-cast state disappeared. Interlamellar spacing and the thickness of eutectoid cementite decreased with increasing forging ratio, and were broken up into particle shapes, which then became spheroidized. With increasing hot forging ratio, hardness, tensile strength, elongation and impact value were not changed up 50%, and then hardness rapidly decreased, while impact value rapidly increased. Hardness and impact value was greatly affected by the disappeared of network and acicular shape of proeutectoid cementite, and became particle shape than thickness reduction of proeutectoid and eutectoid cementite.

• Journal of Mechanical Science and Technology
• /
• v.16 no.10
• /
• pp.1246-1252
• /
• 2002

Ultrafine grained (UFG) low carbon (0.15 wt.% C) steel produced by equal channel angula. pressing (ECAP) was tested for investigating the effect of load ratio on the fatigue crack growth rate. Fatigue crack growth resistance and threshold of UFG steel were lower than that of asreceived coarse grained steel. It was attributed to the less tortuous crack path. The UFG steel exhibited slightly higher crack growth rates and a lower △Kth with an increase of R ratio. The R ratio effect on crack growth rates and △Kth was basically indistinguishable at lower load ratio (R >0.3), compared to other alloys, which indicates that contribution of the crack closure vanishes. The crack growth rate curve for UFG steel exhibited a longer linear extension to the lower growth rate regime than that for the coarse grained as-received steel.

• Journal of Welding and Joining
• /
• v.19 no.5
• /
• pp.486-491
• /
• 2001

The effect of S content in welding wires on spattering characteristics and droplet transfer phenomena was studied. In MAG welding using 80%Ar-$20%CO_2$ shielding gas, spattering characteristics and droplet transfer phenomena were varied with S content of wire. Sulfur addition in wire reduced surface tension of droplet and weld pool, and made arc more stable in MAG welding. With increasing S content, the spattering ratio and the ratio of large size spatter ($d{\geq}1.0mm$) were reduced in short circuit transfer mode. In spray transfer mode, spattering ratio, however was increased when sulfur was added more than 0.020wt.% because surface tension of droplets and weld pool was reduced too much even though arc stability was improved.

• Journal of Ocean Engineering and Technology
• /
• v.14 no.3
• /
• pp.84-89
• /
• 2000

The purpose of this study is to investigate the combustion emission characteristics by the effect of secondary air injection and variation of the excess air ratio in combustion field of model gas turbine combustor. For this purpose, mean temperature, CO, $CO_2$, $O_2$ and HC concentrations were measured by changing excess air ratio and secondary air injection. As a result of this study, mean temperature was decreased and CO, HC emission increased by increasing the excess air ratio of secondary air. Therefore, this results showed the secondary air injection effected strongly on the flame structure and combustion emission characteristics.

• Proceedings of the Korea Committee for Ocean Resources and Engineering Conference
• /
• 2000.04a
• /
• pp.171-176
• /
• 2000

This purpose of this study is to investigate the combustion emission characteristics on the effect of secondary air injection in combustion field of model gas turbine combustor changing excess air ratio. For this purpose, meantemperature, CO, CO2, O2 and HC concentration were measured by changing excess air ratio and secondary air injection. As a result of this study, meantemperature, CO2 emission was decreased and CO emission increased by increasing the excess air ratio of secondary air. therefore, This paper showed the effect of Secondary air injection on flame structure, combustion emission characteristics.