• Title/Summary/Keyword: EDS Process

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Two Dimensional Gold Nanodot Arrays Prepared by Using Self-Organized Nanostructure

  • Jung Kyung-Han;Chang Jeong-Soo;Kwon Young-Soo
    • Journal of Electrical Engineering and Technology
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    • v.1 no.2
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    • pp.246-250
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    • 2006
  • Highly ordered gold nanodot arrays have been successfully obtained by vacuum evaporation using an anodic aluminum oxide (AAO) as a shadow mask. An AAO mask with the thickness of 300 um was prepared through an anodization process. The structure of the nanodot arrays was studied by a field- emission scanning electron microscope (FE-SEM) equipped with an energy dispersive spectrometer (EDS). A tapping mode atomic force microscope (AFM) was employed for studies of height and phase feature. The nanodot arrays were precisely reproduced corresponding to the hexagonal structure of the AAO mask in a large area. In the gold nanodot arrays, the average diameter of dots is approximately the same as the AAO pore size in the range from 70 um to 80 nm and 100 nm center-to-center spacing. EDS analysis indicated that the gold dots were almost entirely consisted of gold, a highly demanded material.

Redundancy Analysis Simulation for EDS Process (EDS 공정에서 Redundancy Analysis 시뮬레이션)

  • 서준호;한영신;이칠기
    • Proceedings of the Korea Society for Simulation Conference
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    • 2002.05a
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    • pp.151-155
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    • 2002
  • Memory의 공정기간은 2∼3개월 정도, 공정은 수백가지에 이를 정도로 많기에 defect은 존재할 수밖에 없다. 많은 defect이 있다면 어쩔 수 없겠지만 적은 defect이 발생한 경우에는 해당 die를 reject시키는 것보다는 repair해서 사용하는 것이 memory생산 업체 입장에서는 보다 효율적이고 원가 절감 차원에서 필수적이다. 이와 같은 이유로 laser repair라는 공정이 필요하고 laser repair공정의 정확한 target을 설정하기 위해 redundancy analysis가 필요하게 되었다. 지금까지 redundancy analysis는 장비 개발 업체에서 제공하는 경우가 대부분 이었고 각 장비 제조 업체별로 redundancy analysis algorithm을 개발하여 제공하여왔기에 동일한 defect 유형에 분석하는 redundancy analysis time이 각 장비 업체 별로 다른 경우가 대부분이었다. 이에 본 연구에서는 기존의 redundancy analysis algorithm의 개념에서 벗어나 defect 유형별로 simulation한 후 redundancy analysis를 진행함으로써 redundancy analysis에 소요되는 시간을 절약함으로써 원가 경쟁력 강화를 하고 correlation 개념을 업무에 적용하는데 목적이 있다

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The characteristics analyses of deteriorated PVC insulated flexible cords by over-current (과전류에 의해 열화된 비닐코드의 특성 분석)

  • Kim, Hyang-Kon;Choi, Chung-Seog;Kim, Dong-Ook;Chung, Hun-Sang
    • Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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    • 2003.07a
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    • pp.489-492
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    • 2003
  • In this paper, we experimented on the deterioration process of power supply cords and analyzed the heating temperature of each part of those cords. We also analyzed the surface states, metallurgical structures surface structures and compositions of the wire melted by over-current. In the results of the analyses, the covering began to be deteriorated from the inside. The heating temperature of extension cord was higher than that of plug body. The dendrite structures appeared at the melted wire. By the SEM and EDS analyses, the dendrite structure showed the growth of copper oxide. We found out the characteristics of PVC insulated flexible cords by over-current from the above experiments and analyses. These results may be useful data in the analyses of deterioration causes of power supply cords.

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Conservation and Chemical Composition of Temmku bowl with hare's fur markings - Applying new restoration material - (천목다완(天目茶盌)의 복원과 유약분석 - 신복원재료의 적용 -)

  • Hwang, Hyunsung;Lee, Haesoon;Kang, Hyungtae
    • Conservation Science in Museum
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    • v.7
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    • pp.33-42
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    • 2006
  • The Conservation Science Laboratory of the National Museum of Korea had drawn up the list of conservation treatment priority according to the artifact status in the collection and performed conservation treatment based on the priority list since 2006. This paper introduces the restoration process of the lost part of a black teacup(Sindo 1961) with newly developed restoration material. Part of the peeled off glaze was analyzed with LIBS and SEM-EDS analyser to find out the glaze ingredients that make the unique pattern of black teacup.

Transient-Liquid-Phase Bonding of Fe-Base MA956 ODS Alloy (Fe기 MA956 산화물분산강화합금의 천이액상확산접합에 관한 연구)

  • 강지훈
    • Journal of Powder Materials
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    • v.2 no.1
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    • pp.53-62
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    • 1995
  • TLP(Transient-Liquid-Phase) bonding of Fe-base MA956 ODS alloy was performed. As insert metal a commercially available Ni-base alloy(MBF50) and an MA956 alloy with additive elements of 7wt% Si and 1wt% B were used. To confirm the idea that a concurrent use of MA956 powder with Insert metals can enhance the homogenization of constituent elements and thereby reduce the thickness of joint interface, MA956 powder was also inserted In a form of sheet. SEM observation and EDS analysis revealed that Cr-rich phase was formed in the bonded interface in initial stage of isothermal solidification during the bonding process, irrespective of kind of insert metals. Measurement of hardeness in the region of bonded interface and EDS analysis showed that a complete homogenization of composition could not be obtained especially in case of MBF50. Joints using either BSi insert metals only or BSi insert together with MA956 powder interlayer showed, however, a remarkable improvement in a compositional homogenization, even though a rapid grain growth in the bonded interface could not be hindered.

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Physicochemical Characteristics of Particulate Matter Emitted from Aluminum Casting Process (알루미늄 주조과정에서 배출되는 입자상물질의 물리·화학적 특성)

  • Jeong-Min Suh;Jeong-Ho Park
    • Journal of Environmental Science International
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    • v.33 no.5
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    • pp.297-304
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    • 2024
  • PM (Particulate Matters) was collected from a bag filter dust collector at an aluminum foundries, and its physicochemical properties were investigated using particle size analyzer and scanning electron microscopy with energy dispersive X-ray spectrometer (SEM/EDS). The median volume diameter of the particles passing through the pretreatment dust collector of the cyclone was approximately 10 ㎛. The cyclone pretreatment dust collector was shown to significantly reduce the throughput of large particles with a particle size of 100 ㎛ or more. The chemical composition of the particles showed a high Al content, and trace amounts of Mg, Si, and Zn were detected.

Characteristics of La0.2Ca0.8MnO3 Powder and Pellet Prepared by Sol-Gel Process (졸-겔법으로 합성한 La0.2Ca0.8MnO3의 분말과 펠렛의 특성)

  • Jung, Miewon;Lee, Jiyun;Kim, Hyunjung
    • Applied Chemistry for Engineering
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    • v.16 no.1
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    • pp.150-152
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    • 2005
  • $La_{0.2}Ca_{0.8}MnO_3$ colossal magnetoresistance (CMR) powders and pellets were synthesized by sol-gel process involving a stable metal chelate complex with acetylacetone. The structural changes of reaction mixture were monitored by FT-IR spectroscopy and X-ray diffractometry. The microstructure of sintered samples and the cation composition of gel powder were studied by FE-SEM/EDS and ICP-AES. The magnetic property was investigated as a function of temperature.

Recovery of Heavy-Metallic Components from a Waste Electro-polishing Solution of 316L Steel by the Solar Cell Electricity (태양전지 전력을 이용한 316L강의 전해연마 폐액 중 중금속 성분의 회수)

  • Kim, Ki-Ho;Jang, Jung-Mok
    • Journal of the Korean institute of surface engineering
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    • v.42 no.1
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    • pp.53-57
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    • 2009
  • Recovery of heavy-metallic component from a waste solution of factory was undertaken by the solar cell electricity. The solution was obtained from an electrolytic etching process of 316L stainless steel. The electrolysis of the solution for recovery of heavy metallic components was made with platinum plated titanium mesh anode and copper plate cathode. Analysis for the solution and electro-winned materials were made by EDS, XRD and SEM. Iron, chromium, and sulfur components were recovered on the cathode from the solution. Result of EDS analysis for the electro-winned materials revealed that some metal oxide were contained in the recovered material. The recovered materials were expected to have metallic form only by the electrolysis, but metal compounds were contained because of weak solar cell power. Nickel and manganese component in the solution doesn't recovered by this electrolysis process, but they made a sludge with phosphoric acid in the solution.

Strength and Reaction Characteristic of the Hardened Blast Furnace Slag Paste using the Alkali Accelerator (알칼리 자극제를 사용한 고로슬래그 경화체의 반응 및 강도특성)

  • Kim, Yun-Mi;Park, Sun-Gyu;Lee, Sang-Soo;Song, Ha-Young
    • Proceedings of the Korean Institute of Building Construction Conference
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    • 2013.05a
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    • pp.313-314
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    • 2013
  • The study carried out the experiment with presenting as the fundamental data for developing non-cement by using red mud generated in blast furnace slag and bauxite generated in the process of manufacturing the pig iron process of manufacturing Al(OH)3/Al2O from as the binding material using the accelerator of NaOH. After fixing the thing and the NaOH adding the blast furnace slag and NaOH 10, 20, 30 (%) with 10, 20, 30 (%) substituted the red mud in the blast furnace slag and the experimental method carried out the experiment. And it measured the flexural strength and compressive strength and took a photograph EDS analysis and SEM. Consequently, the compressive strength was improved as the addition rate of the NaOH was high and the compressive strength according to the replacement ratio of the red mud was degraded. This is determined that film of the blast furnace slag is destroyed and it makes the hydration reaction condition and the intensity is revealed.

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Investigation on alkalinity of pore solution and microstructure of hardened cement-slag pastes in purified water

  • Hu, Ya-Ru;Zuo, Xiao-Bao;Li, Xiang-Nan;Jiang, Dong-Qi
    • Advances in concrete construction
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    • v.12 no.6
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    • pp.507-515
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    • 2021
  • To evaluate the influence of slag on the alkalinity of pore solution and microstructure of concrete, this paper performs a leaching experiment on hardened cement-slag pastes (HCSP) slice specimens with different slag content in purified water. The pH value of pore solution, average porosity, morphology, phase composition and Ca/Si of HCSP specimens in the leaching process are measured by solid-liquid extraction, saturated-dried weighing, scanning electron microscopy-energy dispersive spectrometry (SEM-EDS) and X-ray diffraction (XRD). Results shows that the addition of slag can mitigate an increase in porosity and a decrease in Ca/Si of HCSP in the leaching process. Besides, an appropriate slag content can improve the microstructure so as to obtain the optimum leaching resistance of HCSP, which can guarantee the suitable alkalinity of pore solution to prevent a premature corrosion of reinforced bar. The optimum slag content is 40% in HCSP with a water-binder ratio of 0.45, and an excessive slag causes a significant decrease in the alkalinity of pore solution, resulting in a loss of protection on reinforced bar in HCSP.