• Title/Summary/Keyword: Double encapsulation

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A Case Study of Paraffin Double-walled Microencapsulation Preparation Using Acrylic Polymer and Melamine Polymer for Thermal Energy Storage

  • Nguyen, Hang Vo-Minh;Kim, Chae-Hyun;Kim, Jong-Kuk
    • Journal of the Korean Solar Energy Society
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    • v.39 no.5
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    • pp.65-78
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    • 2019
  • In this study, we investigated the paraffin encapsulation using double-walled encapsulation technique. The first encapsulation used methyl methacrylic acid as the main component in acrylic polymer and the second encapsulation used melamine polymer. Particles size and distribution of the capsules were analyzed using scanning electron microscopy. In the first encapsulation, the stable capsules were obtained at 67% of phase change material ratio to methyl methacrylic acid monomer and the size of the capsule was from 0.2 to $0.3{\mu}m$. In the second encapsulation, the size of the capsules was almost the same with those capsules prepared in the first encapsulation. The particle size of single wall and double wall was about $0.3{\mu}m$. As a result of the encapsulation of paraffin using double-walled encapsulation technique, it was confirmed that the particle size was determined in the process of encapsulating using the acrylic polymer at the first wall material, and the physical and thermal stability of the capsules were imparted using melamine at the secondary wall material.

Detection and Prevention of Bypassing Attack on VLAN-Based Network Segmentation Environment (VLAN을 이용한 네트워크 분할 환경에서의 네트워크 접근 제어 우회 공격 탐지 및 방어 기법)

  • Kim, Kwang-jun;Hwang, Kyu-ho;Kim, In-kyoung;Oh, Hyung-geun;Lee, Man-hee
    • Journal of the Korea Institute of Information Security & Cryptology
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    • v.28 no.2
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    • pp.449-456
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    • 2018
  • Many organizations divide the network to manage the network in order to prevent the leakage of internal data between separate organizations / departments by sending and receiving unnecessary traffic. The most fundamental network separation method is based on physically separate equipment. However, there is a case where a network is divided and operated logically by utilizing a virtual LAN (VLAN) network access control function that can be constructed at a lower cost. In this study, we first examined the possibility of bypassing the logical network separation through VLAN ID scanning and double encapsulation VLAN hopping attack. Then, we showed and implemented a data leak scenario by utilizing the acquired VLAN ID. Furthermore, we proposed a simple and effective technique to detect and prevent the double encapsulation VLAN hopping attack, which is also implemented for validation. We hope that this study improves security of organizations that use the VLAN-based logical network separation by preventing internal data leakage or external cyber attack exploiting double encapsulation VLAN vulnerability.

Preparation of Gemcitabine-Loaded Methoxy Poly(ethylene glycol)-b-Poly(L-lactide) Microparticles Using W/O/W Double Emulsion (W/O/W 다중유화법을 이용한 젬시타빈 함유 Methoxy Poly(ethylene glycol)-b-Poly(L-lactide) 미립자 제조)

  • Ryu, Jong-Hoon;Jung, In-Il;Lee, Ji-Eun;Lim, Gio-Bin
    • KSBB Journal
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    • v.26 no.4
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    • pp.333-340
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    • 2011
  • In this study, gemcitabine-loaded methoxy poly(ethylene glycol)-b-poly(L-lactide) (MPEG-PLLA) microparticles with different PEG block lengths were prepared by a W/O/W double emulsion technique. The present study focuses on the investigation of the influence of various preparative parameters such as the ratio of internal water phase and oil phase, polymer concentration, solvent composition of organic phase and salt concentration of external water phase on the morphology and encapsulation efficiency of the microparticles. The microparticles fabricated at high volume ratios of internal water phase to oil phase and at high polymer concentrations showed a relatively high encapsulation efficiency and low porosity. When a dichloromethane/ethyl acetate mixture was used as solvent, both the encapsulation efficiency and drug loading of the microparticles decreased as the level of ethyl acetate increased. The addition of a salt (NaCl) to the external water phase significantly improved the encapsulation efficiency up to 40%, and the microparticles became more spherical with their size and porosity decreased.

Enhancement of Light Extraction in White LED by Double Molding (이중 몰딩에 의한 백색 LED의 광추출 효율 향상)

  • Jang, Min-Suk;Kim, Wan-Ho;Kang, Young-Rea;Kim, Ki-Hyun;Song, Sang-Bin;Kim, Jin-Hyuk;Kim, Jae-Pil
    • Journal of the Korean Institute of Electrical and Electronic Material Engineers
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    • v.25 no.10
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    • pp.849-856
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    • 2012
  • Chip on board type white light emitting diode on metal core printed circuit board with high thixotropy silicone is fabricated by vacuum printing encapsulation system. Encapsulant is chosen by taking into account experimental results from differential scanning calorimeter, shearing strength, and optical transmittance. We have observed that radiant flux and package efficacy are increased from 336 mW to 450 mW and from 11.9 lm/W to 36.2 lm/W as single dome diameter is varied from 2.2 mm to 2.8 mm, respectively. Double encapsulation structure with 2.8 mm of dome diameter shows further significant enhancement of radiant flux and package efficacy to 667 mW and 52.4 lm/W, which are 417 mW and 34.8 lm/W at single encapsulation structure, respectively.

Encapsulation of 2,4-Dihydroxybenzophenone into Dodecylbenzenesulfonate Modified Layered Double Hydroxide for UV Absorption Properties

  • Li, Shifeng;Shen, Yanming;Liu, Dongbin;Fan, Lihui;Wu, Keke
    • Bulletin of the Korean Chemical Society
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    • v.35 no.2
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    • pp.392-396
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    • 2014
  • New organic-inorganic composite of 2,4-dihydroxybenzophenone (BP-1) encapsulation into dodecylbenzenesulfonate (DBS) modified layered double hydroxide (LDH) was successfully prepared. The surface, structural, thermal and absorption properties of the BP-1/DBS-LDH nanohybrid was characterized by BET analysis, scanning electron microscopy (SEM), X-ray diffraction (XRD), Fourier transform infrared spectroscopy (FT-IR), thermogravimetric analysis (TG) and diffuse reflectance UV-Vis absorbance spectra (DRUV-vis). The interlayer configuration of composite and the adsorption mechanism of BP-1 on MgAl-DBS-LDH were discussed. It was suspected that DBS anions located in the form of monolayer arrangement with a $75^{\circ}$ anti parallel angle between dodecylbenzenesulfonate chain axis. The diffuse reflectance UV-Vis absorbance results revealed that the UV absorbing wavelength of BP-1/DBS-LDH evidently extends to about 400 nm, which shows that the BP-1/DBS-LDH has the potential application as a UV absorber.

Optimization of Ascorbic Acid Encapsulation in PLA Microcapsules Using Double Emulsion Process (이중유화법을 이용한 PLA 마이크로캡슐 내부로의 아스코르브산 캡슐화 공정 최적화)

  • Ji Won Yun;Young Mi Chung
    • Applied Chemistry for Engineering
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    • v.35 no.2
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    • pp.115-121
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    • 2024
  • This study analyzed the influence of process variables affecting the thermodynamic equilibrium and fluid dynamics of interfaces such as reverse micelle, salt concentration, interfacial tension, and viscosity of fluids to optimize the microencapsulation process using the W1/O/W2 double emulsion method. The process variable with the greatest impact on encapsulation efficiency was found to be the difference in osmotic pressure between the W1 and W2 phases. It was observed that increasing the salt concentration in the W2 phase or decreasing the ascorbic acid concentration in the W1 phase resulted in higher encapsulation efficiency. Additionally, a larger difference in osmotic pressure led to increased damage to the surface of the microparticles, as confirmed by SEM images. The introduction of reverse micelles, which was anticipated to increase encapsulation efficiency, either had a low contribution or even decreased encapsulation efficiency. The yield of microcapsules was expressed as a universal function, applicable to all process conditions or solution compositions. According to this universal function, no further increase in yield was observed beyond the Ca (capillary number) of approximately 20.

Ultra Thin Film Encapsulation of OLED on Plastic Substrate

  • Ko Park, Sang-Hee;Oh, Ji-Young;Hwang, Chi-Sun;Yang, Yong-Suk;Lee, Jeong-Ik;Chu, Hye-Yong
    • Journal of Information Display
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    • v.5 no.3
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    • pp.30-34
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    • 2004
  • Fabrications of barrier layer on a polyethersulfon (PES) film and OLED based on a plastic substrate by atomic layer deposition (ALD) have been carried out. Simultaneous deposition of 30 nm of $AlO_x$ film on both sides of PES film gave film MOCON value of 0.0615 g/$m^2$/day (@38$^{\circ}C$, 100 % R.H.). Moreover, the double layer of 200 urn $SiN_x$ film deposited by PECVD and 20 nm of $AlO_x$ film by ALD resulted in the MOCON value lower than the detection limit of MOCON. The OLED encapsulation performance of the double layer have been investigated using the OLED structure of ITO/MTDATA(20 nm)/NPD(40 nm)/AlQ(60 nm)/LiF(1 nm)/Al(75 nm) based on the plastic substrate. Preliminary life time to 91 % of initial luminance (1300 cd/$m^2$) was 260 hours for the OLED encapsulated with 100 nm of PECVD deposited $SiN_x$/30 nm of ALD deposited $AlO_x$.

IPv6 over IPv4 tunneling compatible with IPv4 Firewalls (IPv4 방화벽에 호환성을 갖는 IPv6 터널링)

  • Lee, Jung-Nam;Jang, Ju-Wook
    • The KIPS Transactions:PartC
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    • v.10C no.4
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    • pp.519-524
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    • 2003
  • During the period of co-existence of IPv4 and IPv6, Ipv6 over IPv4 tunneling technique is intended as a start-up transition mechanism. However, most of IPv4 firewalls do not support the IPv6 over IPv4 tunneling packet filtering. Finally, it is impossible that a user inside IPv4 firewall connects with an IPv6 host across IPv4 network. Without any additional hardware or changing the policy of IPv4 firewall, we solve this problem using proposed Double-encapsulation and applied-HTTP tunneling technique that are end-to-end solutions. This enables cheaper IPv6 migration solutions.

The study for the preparations and analyses of fragrance oil encapsulation using $\beta$-cyclodextrin and arabic gum ($\beta$-cyclodextrin과 arabic gum를 이용한 향료의 encapsulation제법과 분석에 관한 연구)

  • 류영상;윤영수
    • Journal of the Society of Cosmetic Scientists of Korea
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    • v.21 no.1
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    • pp.84-94
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    • 1995
  • Fragrance oil was encapsulated with B-Capsulation and Arabic gum for double Encapsulation to improve the demerits-cause the skin irritation, allergy and lack of odor fixative-. Powder fragrance was obtained from the paste phase using the method of spray dry. From the analyses (GC, IR, UV) and sensory teste, it was identified that frogrance was encapsulated in our reservoir.

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Ultra Thin Film Encapsulation of Organic Light Emitting Diode on a Plastic Substrate

  • Park, Sang-Hee;Oh, Ji-Young;Hwang, Chi-Sun;Lee, Jeong-Ik;Yang, Yong-Suk;Chu, Hye-Yong;Kang, Kwang-Yong
    • ETRI Journal
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    • v.27 no.5
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    • pp.545-550
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    • 2005
  • We have carried out the fabrications of a barrier layer on a polyethersulfon (PES) film and organic light emitting diode (OLED) based on a plastic substrate by means of atomic layer deposition (ALD). Simultaneous deposition of 30 nm $AlO_x$ film on both sides of the PES film gave a water vapor transition rate (WVTR) of $0.062 g/m^2/day (@38^{\circ}C,\;100%\;R.H.)$. Further, the double layer of 200 nm $SiN_x$ film deposited by plasma enhanced chemical vapor deposition (PECVD) and 20 nm $AlO_x$ film by ALD resulted in a WVTR value lower than the detection limit of MOCON. We have investigated the OLED encapsulation performance of the double layer using the OLED structure of ITO / MTDATA (20 nm) / NPD (40 nm) / AlQ (60 nm) / LiF (1 nm) / Al (75 nm) on a plastic substrate. The preliminary life time to reach 91% of the initial luminance $(1300 cd/m^2)$ was 260 hours for the OLED encapsulated with 100 nm of PECVD-deposited $SiN_x$ and 30 nm of ALD-deposited $AlO_x$.

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