• Title/Summary/Keyword: Diffraction and scattering

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Transformation Behavior of Retained Austenite on Microstructure and Mechanical Properties in Fe-0.7wt%C-2.3wt%Si Steel (Fe-0.7%C-2.3%Si강의 미세조직과 기계적 성질에 미치는 잔류 오스테나이트 변태 거동)

  • Son, Je-Young;Kwon, Do-Young;Kim, Ji-Hun;Kim, Won-Bae;Kim, Hak-Jin;Ye, Byung-Joon
    • Journal of Korea Foundry Society
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    • v.32 no.3
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    • pp.138-143
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    • 2012
  • This steel has been synthesized integrating concepts from Austempering Ductile Cast Iron (ADI) technology. While ADI has excellent mechanical and physical properties, the Young's modules of ADI is approximately 20% lower than steel. In addition, the presence of graphite nodules in ADI can be sites of crack initiation, where fracture takes place at graphite matrix interface. Because of this limitations of ADI, there has been a growing interest in austempered steels as structural materials in resent years. In this investigation, a new steel with microstructure composed of ferrite and austenite and with simultaneous high tensile strength (1,150 MPa) and high ductility (33%) was developed. The goal of this investigation is to obtain a better understanding of deformation and transformation behaviour in high carbon retained austenite(${\gamma}_{HC}$) and over-saturated ferrite(${\alpha}$) during the plastic deformation. A detailed study of the microstructure of this steel was carried out by means of X-ray diffraction (XRD) and electron back scattering diffraction (EBSD) technic. In this way it was shown that BCC phase (BCC) took up the larger part of the nominal strain whereas the a part of retained austenite responded to the mechanincal load by partial martensite transformation, and misorientation change in the retained austenite after plastic strain could be attributed to the large elongation.

Fabrication of Poly Seed Layer for Silicon Based Photovoltaics by Inversed Aluminum-Induced Crystallization (역 알루미늄 유도 결정화 공정을 이용한 실리콘 태양전지 다결정 시드층 생성)

  • Choi, Seung-Ho;Park, Chan-Su;Kim, Shin-Ho;Kim, Yang-Do
    • Korean Journal of Materials Research
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    • v.22 no.4
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    • pp.190-194
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    • 2012
  • The formation of high-quality polycrystalline silicon (poly-Si) on relatively low cost substrate has been an important issue in the development of thin film solar cells. Poly-Si seed layers were fabricated by an inverse aluminum-induced crystallization (I-AIC) process and the properties of the resulting layer were characterized. The I-AIC process has an advantage of being able to continue the epitaxial growth without an Al layer removing process. An amorphous Si precursor layer was deposited on Corning glass substrates by RF magnetron sputtering system with Ar plasma. Then, Al thin film was deposited by thermal evaporation. An $SiO_2$ diffusion barrier layer was formed between Si and Al layers to control the surface orientation of seed layer. The crystallinity of the poly-Si seed layer was analyzed by Raman spectroscopy and x-ray diffraction (XRD). The grain size and orientation of the poly-Si seed layer were determined by electron back scattering diffraction (EBSD) method. The prepared poly-Si seed layer showed high volume fraction of crystalline Si and <100> orientation. The diffusion barrier layer and processing temperature significantly affected the grain size and orientation of the poly Si seed layer. The shorter oxidation time and lower processing temperature led to a better orientation of the poly-Si seed layer. This study presents the formation mechanism of a poly seed layer by inverse aluminum-induced crystallization.

Temperature dependence of Heteroeptaxial $Y_2O_3$ films grown on Si by ionized cluster beam deposition

  • Cho, M.-H.;Ko, D.-H.;Whangbo, S.W.;Kim, H.B.;Jeong, K.H.;Whang, C.N.;Choi, S.C.;Cho, S.J.
    • Journal of the Korean Vacuum Society
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    • v.7 no.s1
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    • pp.57-77
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    • 1998
  • Heteroepitaxial $Y_2O_3$ films were grown on a Si(111) substrate by ionized cluster beam deposition(ICBD) in ultra high vacuum, and its qualities such as crystllitnity, film stress, and morphological characteristics were investigated using the various measurement methods. The crystallinity was investigated by x-ray diffraction (XRD) and reflection high energy electron diffraction (RHEED). Interface crystallinity was also examined by Rutherford backscattering spectroscopy(RBS) channeling, transmission electron microscopy(TEM). The stress of the films was measured by RBS channeling and XRD. Surface and interface morphological characteristics were investigated by atomic force microscopy (AFM) and x-ray scattering method. Comparing the interface with the surface characteristics, we can conclude that many defects at the interface region were generated by interface reaction between the yttrium metal and SiO2 layer and by ion beam characteristic such as shallow implantation, so that they influenced the film qualities. The film quality was dominantly depended on the characteristic temperature range. In the temperature range from $500^{\circ}C$ to $600^{\circ}C$, the crystallinity was mainly improved and the surface roughness was drastically decreased. On the other hand, in the temperature range from $600^{\circ}C$ to $700^{\circ}C$, the compressive stress and film density were dominantly increased, and the island size was more decreased. Also the surface morphological shape was transformed from elliptical shape to triangular. The film stress existed dominantly at the interface region due to the defects generation.

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Development of Microstructures and Mechanical Properties in Differential Speed Rolled Ni-30Cr Alloy (이주속압연된 Ni-30Cr 합금의 미세조직과 기계적 특성 발달)

  • Im, Yong-Deok;Park, Hyung-Ki;Song, Kuk-Hyun
    • Korean Journal of Materials Research
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    • v.25 no.3
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    • pp.149-154
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    • 2015
  • We evaluated the developed microstructures and mechanical properties of a severely plastically deformed Ni-30Cr alloy. Normal rolling and differential speed rolling were used as deformation processes, and the thicknesses of the specimens were reduced to 68 % of the original thickness after holding at $700^{\circ}C$ for 10 min and annealing at $700^{\circ}C$ for 40 min to obtain a fully recrystallized microstructure. Electron backscattering diffraction was used to analyze the characteristic distribution of the grain boundaries on the deformed and annealed specimens. Differential speed rolling was more effective for refining grains in comparison with normal rolling. The grain size was refined from 33 mm in the initial material to 8.1 mm with normal rolling and 5.5 mm with differential speed rolling. The more refined grain in the differential-speed-rolled material directly resulted in increases in the yield and tensile strengths by 68 % and 9.0%, respectively, compared to normal rolling. We systematically explain the relationship between the grain refinement and mechanical properties through a plastically deformed Ni-30Cr alloy based on the development of a deformation texture. The results of our study show that the DSR process is very effective when used to enhance the mechanical properties of a material through grain refinement.

Development of Microcellular Radio Propagation Prediction Model in the 8 GHz Bands (8 GHz 대역에서의 마이크로셀용 전파전파 예측 모델 개발)

  • Song, Ki-Hong
    • The Journal of Korean Institute of Electromagnetic Engineering and Science
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    • v.17 no.12 s.115
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    • pp.1212-1223
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    • 2006
  • Microwave(M/W) bands, though having great demand in wireless services, have been used mostly for long distance communications. As a result, the studies on their mobile radio models have been made less than on VHF/UHF. However, as the mobile communication services with M/W bands have been increasing, the development of a more accurate prediction model of the mobile radio environments has been demanded. The development of a reliable radio prediction model in the mobile radio environments requires the measurement and analysis of the characteristics of the radio waves according to reflection, diffraction and scattering of radio signals in various mobile radio environments. The proposed 8 GHz band radio prediction models have 2 different categories: (1) LOS model and (2) non-LOS model. The LOS model predicts signal strength using the analytic result with measured pathless exponents for the waves direct and reflected by ground and buildings, and the non-LOS model suggests a prediction model of received power by calculating the signal variations after diffraction.

3D Wave Propagation Loss Modeling in Mobile Communication using MLP's Function Approximation Capability (MLP의 함수근사화 능력을 이용한 이동통신 3차원 전파 손실 모델링)

  • Yang, Seo-Min;Lee, Hyeok-Jun
    • Journal of KIISE:Software and Applications
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    • v.26 no.10
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    • pp.1143-1155
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    • 1999
  • 셀룰러 방식의 이동통신 시스템에서 전파의 유효신호 도달범위를 예측하기 위해서는 전파전파 모델을 이용한 예측기법이 주로 사용된다. 그러나, 전파과정에서 주변 지형지물에 의해 발생하는 전파손실은 매우 복잡한 비선형적인 특성을 가지며 수식으로는 정확한 표현이 불가능하다. 본 논문에서는 신경회로망의 함수 근사화 능력을 이용하여 전파손실 예측모델을 생성하는 방법을 제안한다. 즉, 전파손실을 송수신 안테나간의 거리, 송신안테나의 특성, 장애물 투과영향, 회절특성, 도로, 수면에 의한 영향 등과 같은 전파환경 변수들의 함수로 가정하고, 신경회로망 학습을 통하여 함수를 근사화한다. 전파환경 변수들이 신경회로망 입력으로 사용되기 위해서는 3차원 지형도와 벡터지도를 이용하여 전파의 반사, 회절, 산란 등의 물리적인 특성이 고려된 특징 추출을 통해 정량적인 수치들을 계산한다. 이와 같이 얻어진 훈련데이타를 이용한 신경회로망 학습을 통해 전파손실 모델을 완성한다. 이 모델을 이용하여 서울 도심 지역의 실제 서비스 환경에 대한 타 모델과의 비교실험결과를 통해 제안하는 모델의 우수성을 보인다.Abstract In cellular mobile communication systems, wave propagation models are used in most cases to predict cell coverage. The amount of propagation loss induced by the obstacles in the propagation path, however, is a highly non-linear function, which cannot be easily represented mathematically. In this paper, we introduce the method of producing propagation loss prediction models by function approximation using neural networks. In this method, we assume the propagation loss is a function of the relevant parameters such as the distance from the base station antenna, the specification of the transmitter antenna, obstacle profile, diffraction effect, road, and water effect. The values of these parameters are produced from the field measurement data, 3D digital terrain maps, and vector maps as its inputs by a feature extraction process, which takes into account the physical characteristics of electromagnetic waves such as reflection, diffraction and scattering. The values produced are used as the input to the neural network, which are then trained to become the propagation loss prediction model. In the experimental study, we obtain a considerable amount of improvement over COST-231 model in the prediction accuracy using this model.

Application of nanoparticles in extending the life of oil and gas transmission pipeline

  • Yunye, Liu;Hai, Zhu;Jianfeng, Niu
    • Structural Engineering and Mechanics
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    • v.84 no.6
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    • pp.733-741
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    • 2022
  • The amount of natural gas that is used on a worldwide scale is continuously going up. Natural gas and acidic components, such as hydrogen sulfide and carbon dioxide, cause significant corrosion damage to transmission lines and equipment in various quantities. One of the fundamental processes in natural gas processing is the separation of acid gases, among which the safety and environmental needs due to the high toxicity of hydrogen sulfide and also to prevent wear and corrosion of pipelines and gas transmission and distribution equipment, the necessity of sulfide separation Hydrogen is more essential than carbon dioxide and other compounds. Given this problem's significance, this endeavor aims to extend the lifespan of the transmission lines' pipes for gas and oil. Zinc oxide nanoparticles made from the environmentally friendly source of Allium scabriscapum have been employed to accomplish this crucial purpose. This is a simple, safe and cheap synthesis method compared to other methods, especially chemical methods. The formation of zinc oxide nanoparticles was shown by forming an absorption peak at a wavelength of about 355 nm using a spectrophotometric device and an X-ray diffraction pattern. The size and morphology of synthesized nanoparticles were determined by scanning and transmission electron microscope, and the range of size changes of nanoparticles was determined by dynamic light scattering device.

Role of Radio Frequency and Microwaves in Magnetic Fusion Plasma Research

  • Park, Hyeon K.
    • Journal of electromagnetic engineering and science
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    • v.17 no.4
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    • pp.169-177
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    • 2017
  • The role of electromagnetic (EM) waves in magnetic fusion plasma-ranging from radio frequency (RF) to microwaves-has been extremely important, and understanding of EM wave propagation and related technology in this field has significantly advanced magnetic fusion plasma research. Auxiliary heating and current drive systems, aided by various forms of high-power RF and microwave sources, have contributed to achieving the required steady-state operation of plasmas with high temperatures (i.e., up to approximately 10 keV; 1 eV=10000 K) that are suitable for future fusion reactors. Here, various resonance values and cut-off characteristics of wave propagation in plasmas with a nonuniform magnetic field are used to optimize the efficiency of heating and current drive systems. In diagnostic applications, passive emissions and active sources in this frequency range are used to measure plasma parameters and dynamics; in particular, measurements of electron cyclotron emissions (ECEs) provide profile information regarding electron temperature. Recent developments in state-of-the-art 2D microwave imaging systems that measure fluctuations in electron temperature and density are largely based on ECE. The scattering process, phase delays, reflection/diffraction, and the polarization of actively launched EM waves provide us with the physics of magnetohydrodynamic instabilities and transport physics.

Growth of CdSe thin films using Hot Wall Eptaxy method and their photoconductive properties (HWE에 의한 CdSe 박막의 성장과 광전도 특성)

  • You, Sang-Ha;Hong, Kwang-Joon
    • Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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    • 2004.07a
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    • pp.344-348
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    • 2004
  • The CdSe thin films wee grown on the Si(100) wafers by a hot wall epitaxy method(HWE). The source and substrate temperature are $600^{\circ}C\;and\;430^{\circ}C$ respectively. The crystalline structure of epilayers was investigated by double crystal X-ray diffraction(DCXD). Hall effect on the sample was measured by van der Pauw method and studied on the carrier density and mobility dependence on temperature. From Hall data, the mobility was increased in the timperature range 30K to 150K by impurity scatering and decreased in the temperature range 150K to 293K by the lattice scattering. In order to explore the applicability as a photoconductive cell, we measured the sensitivity($\gamma$), the ratio of photocurrent to darkcurrent(pc/dc), maximum allowable power dissipation(MAPD), spectral response and response time. The results indicated that the photoconductive characteristic were the best for the samples annealed in Cu vapor compare with in Cd, Se, air and vacuum vapour. Then we obtained the sensitivity of 0.99, the value of pc/dc of $1.39{\times}10^7$, the MAPD of 335mV, and the rise and decay time of 10ms and 9.5ms, respectively

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Evaluation of Microstructure and Mechanical Properties of Friction Stir Lap Jointed Inconel 600/SS 400 (겹치기 마찰교반접합된 Inconel 600/SS 400 합금의 미세조직과 기계적 특성 평가)

  • Song, Kuk-Hyun;Nakata, Kazuhiro
    • Korean Journal of Materials Research
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    • v.22 no.3
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    • pp.123-129
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    • 2012
  • The microstructures and mechanical properties of friction stir welded lap joints of Inconel 600 and SS 400 were evaluated; friction stir welding was carried out at a tool rotation speed of 200 rpm and welding speed of 100 mm/min. Electron back-scattering diffraction and transmission electron microscopy were introduced to analyze the grain boundary characteristics and the precipitates, respectively. Application of friction stir welding was notably effective at reducing the grain size of the stir zone. As a result, the reduced average grain size of Inconel 600 ranged from $20{\mu}m$ in the base material to $8.5{\mu}m$ in the stir zone. The joint interface between Inconel 600 and SS 400 showed a sound weld without voids and cracks, and MC carbides with a size of around 50 nm were partially formed at the Inconel 600 area of lap joint interface. However, the intermetallic compounds that lead to mechanical property degradation of the welds were not formed at the joint interface. Also, a hook, along the Inconel 600 alloy from SS 400, was formed at the advancing side, which directly brought about an increase in the peel strength. In this study, we systematically discussed the evolution of microstructures and mechanical properties of the friction stir lap joint between Inconel 600 and SS 400.