• Journal of the Korean Society of Industry Convergence
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• v.26 no.4_2
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• pp.629-637
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• 2023

This study aimed to evaluate the effect of post-curing equipment and time on the flexural strength of 3D printing resins produced by a liquid crystal display(LCD) printer. The three 3D printing resins(DENTCA Denture Teeth, DT; C&B 5.0 hybrid, CH; C&B Permanent A2, CP) were divided into four groups according to post-curing time(10 min and 30 min) and equipment with or without vacuum treatment. For the three-point flexural strength test and biaxial strength test were prepared by method according to ISO 10477, ISO 6872, respectively. Flexural strength was measured with universal testing machine. Comparison between post-curing time of each post-curing equipment was analyzed by independent sample t-test and Mann-Whitney U test(α=.05), and comparison between groups according to each 3D printing resin was performed by Kruskal-Wallis test and post-hoc by Bonferroni-Dunn test(α=.05). The flexural strength of the resin post-curing under vacuum was higher than that of the resin post-curing in air. In the comparison according to the post-curing time, in the case of the post-curing equipment without vacuum, the 30 minute curing time showed significantly higher flexural strength than the 10 minute curing time, except for the biaxial flexural strength of CH(P<.05). In the post-curing equipment with vacuum, the three-point flexural strength of all 3D printing resins(DT, CH, and CP) showed a higher value at 30 minute curing time than at 10 minute curing time.

• Journal of the Korean Society of Safety
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• v.12 no.1
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• pp.71-76
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• 1997

In this paper, it was described results of study on curing safety of molding meterial, about the variation of phenol resin contents, wood flour contents and moisture of wood flour, under the same condition. The experimental results are summarized as follows ; 1) When the curing temperature was high, the curing time was short in the case of 4～8wt% moisture of wood flour, but in the case of more than l2wt% moisture of wood flour, the curing time was long. 2) The curing time for curing temperature was more short when 6wt% moisture of wood flour than 4wt% moisture of wood flour. 3) The more wood flour content and moisture of wood flour content, the longer curing time and the more mineral filler content, the shorter curing time. 4) When the phenol resin content of main matrix increase, the curing time was short.

• Journal of dental hygiene science
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• v.23 no.2
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• pp.123-131
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• 2023

Background: As a restorative material used to treat dental caries, the light-curing type resin is widely used, but it has the disadvantage of polymerization shrinkage. The Bulk-Fill composite resin was developed to solve these shortcomings, but the existing research mainly focused on comparing the physical properties of a composite resin and a Bulk-Fill resin. A study on the light curing time and distance of the Bulk-Fill resin itself tend to be lacking. Methods: This study compares the surface microhardness of specimens prepared by varying the light curing time and distance of smart dentin replacement (SDR) as a flowable Bulk-Fill resin and Tetric N-ceram as a packable Bulk-Fill resin, and confirms the polymerization time and distance that becomes the optimum hardness. To determine the hardness of the specimen, it was measured using the Vickers Hardness Number (Matsuzawa MMT-X, Japan). Results: In SDR, the surface microhardness decreased as the distance increased in all time groups in the change distance from the curing tip. In the change of light curing time with respect to the distance from curing tip, the surface microhardness increased as the time increased. In Tetric N-ceram, the surface microharness showed no significant difference in the change of the distance of curing tip in the group of 20 and 60 second. But in the group of 10 and 40 seconds, decreased as the distance increased. The surface microharness increased as the light curing time increased in all distance groups. Conclusion: When using SDR and Tetric N-ceram in clinical practice, it is considered that as the distance from the polymerization reactor tip increases, a longer light curing time than the polymerization time recommended by the manufacturer is required.

• Journal of Technologic Dentistry
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• v.23 no.2
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• pp.95-103
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• 2002

For this study, self curing resin and heat curing resin used for existing usual resin denture base in the denture industry were chosen by manufacturer. Curing tests for 30-minute, I-hour, 2-hour and 3-hour were conducted to know the strength of the resins and conduct analysis to get other necessary information. The results obtained are as follows: 1. Heat curing resins show a little differences among the manufacturers. However 30-minute curing resin shows great difference as shown in the fracture strength test. 2. The effect from the granularity of the resins on the fracture strength was found insignificant which means there is no difference between coherence and strength. 3. To summarize the results from each time level, the longer the time is, the more the minute cracks on the surface, which is the cause of reduced strength. From this test, it was identified that in making the denture base for patients in dental clinics, 30-minute curing is most efficient and effective in reducing discoloration and monomers, although long-time curing has been considered to be the principal.

• Proceedings of the Korean Institute of Building Construction Conference
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• v.y2004m10
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• pp.11-14
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• 2004

The object of this study is vibrating compaction and curing method in the production process of Design concrete for precast concrete(Design-PC) product. From change of vibrating compaction time and pre-curing time. curing temperature which would be factors of product quality in Design-PC concrete production. and research of optimized steam curing condition from relations between curing condition and strength development. basic data of vibrating compaction time and concrete steam curing method for Design-PC will be presented.

• Proceedings of the Korean Institute of Building Construction Conference
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• 2022.04a
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• pp.91-92
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• 2022

This study is a basic study on carbonation curing technology of concrete using supercritical CO₂, and carbonation curing was carried out by exposing concrete to supercritical CO₂ for a certain period of time. In the case of conventional carbonation curing, long-term curing was performed for several weeks by controlling the concentration of CO₂, but by using supercritical CO₂, more rapid carbonation curing was carried out using constant temperature and pressure conditions to improve durability through surface modification of concrete. This experiment was conducted with the goal of deriving the optimal carbonation curing conditions by measuring the carbonation depth by exposing concrete for a certain period of time to conditions above the supercritical level. As a result, it was confirmed that the carbonation depth increased as the curing time increased, and the curing time could be shortened compared to the carbonation curing according to the existing CO₂ concentration.

• International Journal of Highway Engineering
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• v.15 no.5
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• pp.11-20
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• 2013

PURPOSES : This study is to suggest time to spray curing compound, the amount of curing compound, and the number of times to spray curing compound based on indoor tests. METHODS : Based on the literature review, two methods are used in this study, One is test for water retention of concrete curing material and the other is test for abrasion resistance of concrete surfaces by the rotating-cutter method. Through those methods, curing compound was evaluated. RESULTS : The result of the laboratory experiment for time to spray curing compound indicates that 30 minutes after placing concrete is optimal. For the amount of curing compound, $0.5{\ell}/m^2$ is the minimum quantity for both concretes. Through test of the number of times to spray curing compound, method to spray the whole amount of curing compound in twice is more efficient than it to spray the whole amount at a time. Also, method of separately 30-50 minutes spray is better than method of separately 10-30 minutes spray. CONCLUSIONS : From the testing results, it can be proposed that optimum time to curing compound is $30{\pm}15$ minutes, $0.5{\ell}/m^2$ is efficient for spraying the whole amount of curing compound at a time, and $0.4{\ell}/m^2$ is the best for spraying the whole amount of curing compound in twice, which sprays it in 20 minutes after 30 minutes from placing concrete.

• Restorative Dentistry and Endodontics
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• v.28 no.2
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• pp.156-161
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• 2003

The purpose of this study is to evaluate the polymerization ability of three different light sources by microhardness test. Stainless steel molds of 1, 2, 3, 4 and 5 mm in thickness of 7 mm in diameter were prepared. The hybrid composite Z100 was packed into the hole of the mold and curing light was activated for designated time. Three different light sources, conventional halogen, light emitting diode, and plasma arc, were used for curing of composite. Two different curing times applied ; one is to follow the manufacturers recommendation and the other is to extend the curing time of LED and plasma arc for balancing the light energy with halogen. Immediately after curing, the Vickers hardness was measured at the bottom of specimen. The results were as follows. 1 The composite cured with LED showed equal to higher microhardnesss than halogen. 2. The composite was cured with plasma arc by manufacturers recommendation showed lowest micro-hardness at all thickness. However, when curing time was extended, microhardness was higher than the others. In conclusion, this study suggested that plasma arc needs properly extended curing time.

• Current Research on Agriculture and Life Sciences
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• v.32 no.3
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• pp.125-130
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• 2014

This study used transmission electron microscopy (TEM) to investigate the micro-morphological features of two formaldehyde to urea (F/U) mole ratio liquid urea-formaldehyde (UF) resins with three hardener levels as a function of the curing time. The micro-morphological features of the liquid UF resins were characterized after different curing times. As a result, the TEM examination revealed the presence of globular/nodular structures in both liquid UF resins, while spherical particles were only visible in the low F/U mole ratio resins. The high F/U mole ratio liquid UF resins also showed extensive particle coalescence after adding the hardener, along with the appearance of complex filamentous networks. When the resins were cured with a higher amount of hardener and longer curing time, the spherical particles disappeared. For the low mole UF resins, the particles tended to coalesce with a higher amount of hardener and longer curing time, although discrete spherical particles were still observed in some regions. This is the first report on the distinct features of the crystal structures in low F/U mole ratio UF resins cured with 5% hardener and after 0.5 h of curing time. In conclusion, the present results indicate that the crystal structures of low F/U mole ratio UF resins are formed during the curing process.

• Elastomers and Composites
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• v.52 no.4
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• pp.266-271
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• 2017

This study describes the influence of the amount of curing agent and curing temperature on the kinetics of polyurethane elastomers. The urethane prepolymer series was prepared by reacting toluene diisocyanate with polytetramethylene ether glycol at $80^{\circ}C$ for 1 h, and 4,4'-methylene bis(2-chloroaniline) was used as the curing agent. The ratio of the amine group of the curing agent to the isocyanate group of the urethane prepolymer was controlled from 0.85 to 1.05 at curing temperatures ranging from 80 to $120^{\circ}C$. The curing rate of the urethane prepolymer was monitored by observing the change in heat flow during the curing process using differential scanning calorimetry (DSC). As either the content of curing agent or the curing temperature was higher, the conversion rate to the polyurethane elastomer was high. The DSC results were compared with those obtained from using real-time FT-IR.