• 제목/요약/키워드: Curing level

검색결과 293건 처리시간 0.03초

Hydration properties of cement pastes containing high-volume mineral admixtures

  • Tang, Chao-Wei
    • Computers and Concrete
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    • 제7권1호
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    • pp.17-38
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    • 2010
  • This research aimed to investigate the influence of high-volume mineral admixtures (MAs), i.e., fly ash and slag, on the hydration characteristics and microstructures of cement pastes. Degree of cement hydration was quantified by the loss-on-ignition technique and degree of pozzolanic reaction was determined by a selective dissolution method. The influence of MAs on the pore structure of paste was measured by mercury intrusion porosimetry. The results showed that the hydration properties of the blended pastes were a function of water to binder ratio, cement replacement level by MAs, and curing age. Pastes containing fly ash exhibited strongly reduced early strength, especially for mix with 45% fly ash. Moreover, at a similar cement replacement level, slag incorporated cement paste showed higher degrees of cement hydration and pozzolanic reaction than that of fly ash incorporated cement paste. Thus, the present study demonstrates that high substitution rates of slag for cement result in better effects on the short- and long-term hydration properties of cement pastes.

동결융해 및 수침조건을 고려한 경량기포혼합토의 거동 실험 연구 (Experimental Study on behavior of the Lightweight Air-foamed Soil Considering Freezing-thawing and Soaking Conditions)

  • 강대규;신은철
    • 한국지반환경공학회 논문집
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    • 제17권5호
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    • pp.37-46
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    • 2016
  • 해성 점토를 이용한 경량기포혼합토의 동결융해 및 수침조건에 따른 환경적 변화특성을 파악하기 위하여, 시멘트 사용량을 변화시키며 경량기포혼합토의 시료를 제작하여 동절기 저온양생, 지중양생 및 실내양생 조건에서 일축압축강도를 관찰하였다. 동결융해($-9.1^{\circ}C{\sim}17.2^{\circ}C$ 온도범위)를 받는 시료는 시멘트 사용량에 상관없이 강도발현이 안되었고 지표면 아래 30cm 깊이의 지중에서 양생한 경우 시멘트 사용량이 증가할수록 압축강도는 급격히 증가되었다. 따라서 동결융해를 받는 조건에서는 경량기포혼합토 타설 후 외기로부터 차단하는 보온층 설치가 필요하다. 장기간 수침상태를 유지한 시료는 단위중량의 증가가 매우 작게 발생하였고, 시료가 건조되어 함수비가 6%로 저하되었을 때 압축강도는 급격히 감소하는 경향이 있다. 그러나 건조를 방지하고 습윤상태를 유지할 경우 압축강도 및 단위중량의 변화는 매우 작았다. 지하수위 아래에 매설되거나 피복토를 갖는 경량기포혼합토는 장기적으로 안정적인 건설재료로 평가할 수 있다.

귀비탕(歸脾湯) 및 귀비탕가자하거(歸脾湯加紫河車)가 난소적출(卵巢摘出)로 유발(誘發)된 흰쥐의 골다공증(骨多孔症)에 미치는 영향(影響) (Effects of the Guibi Tang(GT) and Guibi Tang Blended Placenta Hominis(GTPH) on Osteoporotic Rats Induced by Ovariectomy)

  • 조성희;유동열
    • 대한한방부인과학회지
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    • 제20권4호
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    • pp.24-40
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    • 2007
  • Purpose: This study was carried out to investigate the effects of Guibi Tang(GT) and Placenta Hominis blended Guibi Tang(GTPH) on the postmenopausal osteoporosis. Methods: In order to observe the potential effects of GT and GTPH on the osteoporosis induced by ovariectomy, antioxidative effects of GT and GTPH were measured. Antioxidative activity for the samples was investigated by Rancimat method. Animals were observed for 8 weeks, and vehicle and extracts of prescriptions were administered ad libitum. And we measured the variance of body weight, femoral bone weight, serum level of osteocalcin, calcium, alkaline phosphatase(ALP), estradiol, cholesterol, triglyceride, alanine aminotransferase(ALT) and creatinine. Results: As a result, GTPH showed antioxidative effect, but did not in GT. Body weight increased significantly in 6 weeks after ovariectomy, and the weight of GTPH administered group decreased significantly. GT and GTPH decreased the serum level of cholesterol and triglyceride. Administration of GTPH increased the serum level of ALP when compared with control group. Ovariectomy and GT, GTPH administration had no influence on serum level of ALT and creatinine. Conclusion: According to above results. We suggest that GT and GTPH may be used prevention and curing the postmenopausal osteoporosis.

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함수비 증가에 따른 심층혼합지반의 강도특성 (The Strength Characteristics of Deep Mixing Ground According to Increasing Water Contents)

  • 박춘식;최준삼
    • 한국지반공학회논문집
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    • 제35권3호
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    • pp.25-35
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    • 2019
  • 심층혼합지반의 강도설계를 위한 실내강도 특성을 파악하고자 점토질, 모래질, 자갈질의 20가지 지반조건, 8%, 10%, 12%, 14%의 4가지 안정재 혼합비조건, 포화도 100%에 대한 함수비와 그 때의 함수비에 10%, 20% 증가된 3가지 함수비조건에 대하여 7일 및 28일 양생기간 별로 두 개씩 총 640개의 공시체를 제작하여 일축압축강도에 대한 실내시험을 수행하였다. 점토질 지반의 경우 안정재 혼합비가 증가함에 따라 강도가 증가하지만 양생기간에는 관계없이 비슷하게 나타났으며, 심층혼합시료의 강도발현에 함수비에 대한 영향이 다른 지반에 비해 비교적 적을 것으로 판단되었다. 모래질 지반은 안정재 혼합비가 증가할수록 강도증가량이 뚜렷하게 증가하는 것으로 나타났고, 또한 함수비 증가가 강도증가 효과를 감소시키는 것으로 판단되었다. 자갈질 지반은 안정재 혼합비 14% 이상에서는 강도발현에 영향이 커서 강도증가가 크게 나타났지만 모래질 지반에 비하여 양생에 따른 강도비는 작게 나타났다.

산업부산물을 사용한 콘크리트 벽돌의 CO2 양생 후 탄산화 평가 (Carbonation Evaluation After CO2 Curing of Concrete Bricks Using Industrial by-products)

  • 문훈;이남곤;박정준;류금성;박기준;장인동
    • 한국건설순환자원학회논문집
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    • 제11권4호
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    • pp.373-380
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    • 2023
  • 본 연구에서는 발전소에서 포집된 CO2의 활용을 위해 CO2 환경에서 양생된 콘크리트 벽돌의 탄산화를 분석하였다. 전기로 환원슬래그(ERS)와 전기로 산화슬래그를 사용하여 콘크리트 벽돌 시험체를 제작하고 20% 농도의 CO2 챔버에서 콘크리트 벽돌 시험체를 3일간 양생하여 항온항습 상태에서 양생된 시험체와 탄산화 수준을 비교하였다. 콘크리트 벽돌의 무게변화, 탄산화 깊이, 휨강도, 압축강도를 측정한 결과, CO2 환경에서 양생된 시험체는 무게의 2.4 % 수준의 CO2를 흡수하는 것으로 나타났다. ERS를 사용한 시험체가 탄산화 깊이가 가장 깊었으며, KS F 4004 콘크리트 벽돌의 규준을 만족하였다. 따라서 포집된 CO2는 콘크리트 벽돌의 CO2 양생 과정에 활용할 수 있을 것으로 기대된다.

기공교육 향상을 위한 양생기공학 강의평가 분석 (Yang-Seng Gi-Gong Course Evaluation Analysis for Improving Education Gi-Gong)

  • 안훈모;나삼식
    • 대한의료기공학회지
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    • 제15권1호
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    • pp.1-22
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    • 2015
  • Objectives : The purpose of this study is to develop a Gi-Gong method instruction configured with modern motions to suit the Medical curing characteristics of Korean Medicine and improve the development and validation of educational and clinical needs. Methods : We took survey on 33 students after giving 'Yang-Seng Gi-Gong' lectures at Woosuk University School of Korean Medicine in the first semester of the year 2015. Results : 1. Reflection of training goal was 7.75±1.79, which showed that the education was overall interesting, but showed a high satisfaction with the practical rather than the theoretical lectures. 2. General difficulty level was intermediate, but the practice of Hwal-In-Shim-Bang Do-In-Beop from several formulations were evaluated relatively difficult exercise. 3. The propriety of training materials were rated as mostly adequate, but that assessment was relatively less appropriate for the linkage of theory and practice, and that of time allocation and place was a normal level. 4. For the propriety of time distribution, the class of one semester such as the current is rated appropriate by 61% of students. 5. General class participation was 6.34±2.52, then participation in practice than theory lessons were active. On the other hand, Induction training participation and participation appeared to be relatively low correlation, but overall interesting and participation in practice high correlation. Conclusions : The difficulty level of theory lessons is necessary to be adjusted and lecture form will need to continue focusing on practical lessons.

Performance of Hybrid Adhesives of Blocked-pMDI/Melamine-Urea-Formaldehyde Resins for the Surface Lamination on Plywood

  • Lubis, Muhammad Adly Rahandi;Park, Byung-Dae;Lee, Sang-Min
    • Journal of the Korean Wood Science and Technology
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    • 제47권2호
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    • pp.200-209
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    • 2019
  • To improve the water resistance of melamine-urea-formaldehyde (MUF) resins, different levels of blocked polymeric 4,4 diphenyl methane diisocyanate (B-pMDI) were blended with MUF resins to prepare B-pMDI/MUF hybrid adhesives, and their adhesion performances were evaluated for the surface lamination of fancy veneer on plywood. FT-IR spectra showed that the de-blocked -NCO groups reacted with the -OH of hydroxymethyl groups of the MUF resins to form urethane bonds at 2% B-pMDI/MUF, which was detected before and after their hydrolysis. The mass loss after the hydrolysis consistently decreased as the B-pMDI level increased, indicating an improvement in the water resistance. As the B-pMDI level increased, the activation energy of hybrid adhesives decreased, which improved the reactivity of the hybrid adhesives. Additionally, the water resistance improvement of the hybrid adhesives increased the tensile shear strength of the surface laminated plywood in semi-water proof and water-proof by 23 % and 8 %, respectively, at 2% B-pMDI level. This was likely due to the urethane linkages in the hybrid adhesives. However, the formaldehyde emission from plywood panels bonded with the hybrid adhesives increased in the dry state, indicating incomplete curing of the hybrid adhesives.

복합레진의 간헐적 광중합 방법이 변연적합도에 미치는 영향 (THE EFFECT OF INTERMITTENT COMPOSITE CURING ON MARGINAL ADAPTATION)

  • 윤용환;박성호
    • Restorative Dentistry and Endodontics
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    • 제32권3호
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    • pp.248-259
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    • 2007
  • 이 실험의 목적은 광중합복합 레진을 자체 제작한 광조사 차단 장치를 이용하여 간헐적 광중합시켜 기존의 연속 중합법과 변연적합도를 비교함으로써 간헐적 광중합의 영향을 알아 보는 것이다. 이번 실험에 사용된 재료는 Pyramid (Bisco, Schaumburg, U.S.A)와 Heliomolar (Ivoclar Vivadent, Liechtenstein)이다. 발치된 상악 소구치에 class II MOD 와동 형성 후 위 두 재료를 bulk 충전하고 다음의 중합cycle에 따라 중합시켰다: 제1군- 연속 광중합 (60초간 계속 광조사); 제2군-2초 광조사, 1초 광차단 (90초 시행); 제3군- 1초 광조사 1초 광차단 (120초 시행); 제4군- 1초 광조사, 2초 광차단 (180초 시행). 저작재현장치 (R&B, Daejeon, Korea)로 720000회의 운동횟수, 분당 120의 회전속도, $5^{\circ}C$$55^{\circ}C$의 물을 교대로 치아에 6000회 주사하면서 5.0 kg의 하중을 치아에 적용하였고 실험 전후 변연적합도를 전체와 부위별 변연으로 나누어서 $\times200$배율의 광학 현미경으로 측정하였다. 부위별 변연은 교합면, 인접면, 치은면 등 세 부위로 나누어서 법랑질 변연을 측정하였다. 전체 변연적합도에서 각 군간, 재료간, 저작 운동 전후 차이를 보기 위해 three-way ANOVA와 Duncan's multiple range test를 시행하였고, 부위별 변연적합도에서는 각 군에서 부위별 차이와 각 부위에서 군간 차이를 보기 위해 각각 one-way ANOVA와 Duncan's multiple range test를 시행하였다 (95% 유의수준). 전체 변연적합도를 보면, 저작 운동 전에는 Pyramid의 경우 3, 4군이 1,2군에 비해, Heliomolar의 경우 3.4군이 1군에 비해 전체 변연적합도가 우수하였고, 저작 운동 후에는 Pyramid. Heliomolar모두 3군이 1군에 비해 전체 변연적합도가 우수하였다 (p < 0.05). 재료간 비교에서는 저작 운동 잔에는 2군에서 Heliomolar가 Pyramid보다 변연적합도가 우수하였고 (p < 0.05) 그 외의 군에서는 유의차가 없었으며, 저작 운동 후에는 모든 군에서 재료간 유의차가 없었다. 각 부위별 변연적합도를 비교하면, 저작 운동 전 Pyramid에서는 교합면 변연에서는 4군이 2군에 비해 높은 변연적합도를 보였고 (p < 0.05), 인접면과 치은면에서는 군 간 유의차를 보이지 않았다. Heliomolar에서는 교합면 변연에서 2, 4군이 1군에 비해 높은 변연적합도를 보였고 (p < 0.05), 인접면과 치은면에서는 군간 유의차를 보이지 않았다. 저작 운동 후 Pyramid에서는 교합면 변연에서는 3군이 1, 2군에 비해 높은 변연적합도를 보였고 (p < 0.05), 인접면과 치은면에서는 군간 유의차를 보이지 않았다. Heliomolar에서는 교합면에서 2, 3, 4군이 1군에 비해 변연적합도가 높았으며 (p < 0.05), 인접면과 치은면에서는 군간 유의차를 보이지 않았다 이번 연구를 통하여 복합레진을 간헐적 광중합시킴으로써 변연적합도가 향상될 수 있음을 알 수 있었다.

Reduction of Formaldehyde Emission from Particleboardsby Bio-Scavengers

  • Eom, Young-Geun;Kim, Jong-Sung;Kim, Sumin;Kim, Jin-A;Kim, Hyun-Joong
    • Journal of the Korean Wood Science and Technology
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    • 제34권5호
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    • pp.29-41
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    • 2006
  • This study was to investigate the effect of adding additive as tannin, rice husk and charcoal, for reducing the formaldehyde emission level, on the adhesion properties of urea-formaldehyde (UF) resin for particleboard. We controlled the hot-pressing time, temperature and pressure to determine the bonding strength and formaldehyde emission. Blends of various UF resin/additives (tannin, rice husk and charcoal) compositions were prepared. To determine and compare the effect of additives (tannin, rice husk and charcoal) content, 0, 5, 10 and 15%, by weight of UF resin, were used. $NH_4Cl$ as hardener added. To determine the level of formaldehyde emission, we used the desiccator, perforator and 20 L-small chamber method. The formaldehyde emission level decreased with increased additions of additive (except rice husk). Also, increased hot-pressing time decreased formaldehyde emission level. At a charcoal replacement ratio of only 15%, the formaldehyde emission level is under F ✩ ✩ ✩ ✩ grade (emit < $0.3mg/{\ell}$). Curing of the high tannin additive content in this adhesive system indicated that the bonding strength increased. But, in the case of rice husk and charcoal, the bonding strength was much lower due to the inorganic substance. Furthermore, rice husk was poor in bonding strength as well as formaldehyde emission than tannin and charcoal.

In-situ Thermally Curable Hyper-branched 10H-butylphenothiazine

  • Jo, Mi-Young;Lim, Youn-Hee;Ahn, Byung-Hyun;Lee, Gun-Dae;Kim, Joo-Hyun
    • Bulletin of the Korean Chemical Society
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    • 제33권2호
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    • pp.492-498
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    • 2012
  • A hyper branched 10-butylphenothiazine with in-situ thermally curable methacrylate (1,3,5-tris-[$\{$10-Butyl-3-(4-(2-methyl-acryloyloxy)-phenyl)-7-yl-10H-phenothiazine$\}$]-benzene, (tris-PTMA)) was synthesized successfully. From the TGA thermogram of tris-PTMA was thermally stable up to $336^{\circ}C$. In the first heating scan of DSC thermogram, tris-PTMA showed glass transition temperature (Tg) at $140^{\circ}C$ and broad endothermic process in the region of $144-179^{\circ}C$, which is thermally curing temperature. In the second heating process, $T_g$ exhibited at $158.7^{\circ}C$ and endothermic process was not observed. Thermally cured tris-PTMA showed no big change in the UV-visible spectrum after washing with organic solvent such as methylene chloride, chloroform, toluene, indicating that thermally cured film was very good solvent resistance. Thermally cured tris-PTMA was electrochemically stable and the HOMO energy level of tris-PTMA was -5.54 eV. The maximum luminance efficiency of double layer structured polymer light-emitting diode based on in-situ thermally cured tris-PTMA was 0.685 cd/A at 16.0 V, which was higher than that of the device without thermally cured tris-PTMA (0.348 cd/A at 15.0 V).